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2014-2015
École Na! onale Supérieure de Chimie de LilleAvenue Mendeleïv - BP 90108 - Bât. C7
Cité Scien� fi que
59652 Villeneuve d’Ascq cedex
FRANCE
Contact : interna� onal@ensc-lille.fr
www.ensc-lille.fr
Programme of studyNa! onal Graduate School of Engineering Chemistry of Lille
(France)
Année 2012-2013
3rd academic year (semesters 5 and 6)
MODULE : ORGANIC AND MOLECULAR CHEMISTRY
SUBJECT:
STRUCTURE AND REACTIVITY OF ORGANIC MOLECULES
Chim
Coordinator:
Professor Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (3) 20 43 48 58
Building C1-Office 101
Compulsory
Code: CH1503
Semester: 5
Lecture: 17 Hours
Directed studies: 11 Hours
Language: French
Coefficient: 3
ECTS: 1.5
Instructor(s):
Philippe Cotelle
Learning outcomes:
Give the same basis for every student from all particular formations
The students will be able to:
Have an idea of the structural 3D representation of an organic compound
Anticipate the reactivity from the structure and the electronic properties of a molecule
Propose reasonable short synthetic route(s) for the synthesis of organic compounds
Prerequisite:
Basic competences acquired during previous formations (CPGE, CPI, DEUG, DUT, BTS, ATS).
Paul Arnaud : Cours de chimie organique, Dunod 15ème édition, 1990, ISBN 2-0401-9716-8. Nicolas
Rabasso : Chimie organique, de Boeck, 2006, ISBN 2-8041-5210-3
Contents:
Chemical bond (theory of the covalent bond, hybridization concept, molecular orbital theory…)
3D structures of small organic molecules
Reactivity in relation with the structure and the electronic properties
Additions to multiple bonds
Aliphatic Substitutions on sp3 carbon
Eliminations
Substitutions on aromatic carbons (electrophilic and nucleophilic)
Pericyclic reactions (including Diels-Alder reactions)
Aldehydes and ketones : tautomeric equilibrium (keto/enol), condensations, transpositions.
Addition on the carbonyl function, Michael addition, Robinson annulation
Additional information:
Media: powerpoint presentation
Bibliographical references: Vollhardt, Schore : Traité de chimie organique, 5ème édition,2009, ISBN 2-
8041-5884-5
Clayden, Greeves, Warren, Wothers : Organic chemistry, 1ère édition, 2001, ISBN 978-0-19-850346-0
Assessment: two written exams (the first one in november, 1 hour, the second one in january, 2 hours)
Remarks:
CI 1Y
MODULE : ORGANIC AND MOLECULAR CHEMISTRY
SUBJECT:
APPLIED MOLECULAR SPECTROSCOPIES
Chim
Coordinator:
Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
03 20 43 48 58
Building C1-Office 01
Compulsory
Code : CH1502
Semester : 5
Lecture: 15 Hours
Directed studies:
Language : French
Coefficient : 4
ECTS : 2
Instructor(s) :
Prénom(s) /Nom(s)
Learning outcomes :
(Description en termes de compétences générales ou spécifiques.)
Prerequisite:
(Exigences préalables. Indication des connaissances préalables présumées acquises au début de l'unité de cours; indication des cours requis au préalable.) Contents :
Other :
Contents :
(Présentation concise de chaque unité.)
Additional information:
Media :
Bibliographical references:
Assessment: (nature, durée, chronologie, fréquence)
Remarks:
CI 1Y
Instructor(s):
Eric BUISINE
Eric.buisine@ensc-lille.fr
Phone: 03 20 33 77 48
ENSCL - C7B
Learning outcomes:
The aim of this course is to develop fundamental knowledge necessary for a good understanding of the
main molecular spectroscopy techniques used in analytical chemistry. The course describes Micro-
Wave rotational spectroscopy, Infra-Red vibrational spectroscopy and UV/Vis electronic spectroscopy.
Prerequisite:
None
Contents:
Chapter I - Introduction: electromagnetic wave ; electromagnetic spectrum ; absorption and emission of radiation ; molecular energy states ; population of molecular states and transitions ; transition dipole moment ; transition probability ; selection rules ; measurement of the absorption mode intensities ; spectral linewidth ; spectrum sensitivity and resolution. Chapter II - MW rotational spectroscopy: moments of inertia ; molecular rotators - Diatomic and linear
polyatomic molecules: frequencies and intensities of rotational transitions ; selection rules ; centrifugal
distortion effect ; rotation-vibration coupling - Non-linear molecules.
Chapter III - IR vibrational spectroscopy - Diatomic molecule: harmonic oscillator approximation ; fundamental vibration frequency ; effect of bond strength ; effect of atomic masses ; selection rules and intensities of vibrational transitions ; rovibration spectrum ; selection rules and intensities of rovibrational transitions - Polyatomic molecules: vibrational degrees of freedom and normal modes of vibration ; bond deformation vibrations ; angular deformation vibrations ; selection rules and activity of normal modes ; intensity of vibrational transitions ; harmonic and combination spectral lines. Chapter IV - UV/Vis electronic spectroscopy - Molecular electronic states ; electron configuration and molecular spin states (doublet, triplet…) ; electronic transitions in organic molecules ; Franck-Condon principle ; selection rules and intensity of vibronic transitions ; chromophores and solvatochromism ; desexcitation mechanisms ; fluorescence and phosphorescence. Additional information:
Media : copy of PowerPoint presentations are accessible from the intranet
Bibliographical references: None
Assessment: written 2 hour exam without documents (semester 6)
Remarks:
Related directed studies are given in the course unit CH1602 (semester 6)
The exam is unique for the two course units CH1502 and CH1602
MODULE : ORGANIC AND MOLECULAR CHEMISTRY
SUBJECT:
APPLIED MOLECULAR SPECTROSCOPIES
Chim
Coordinator:
Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (3) 20 43 48 58
Building C1-Office 101
Compulsory
Code: CH1602
Semester: 6
Lecture: 13 Hours
Directed studies: 14 Hours
Language: French
Coefficient: 4
ECTS: 2
Instructor(s):
Eric BUISINE
Eric.buisine@ensc-lille.fr
Phone: 03 20 33 77 48
ENSCL - C7B
Alain MOISSETTE
(IR and UV/Vis: directed
studies)
Alain.moissette@univ-lille1.fr
Phone: 03 20 43 69 62
LASIR - C8)
Learning outcomes:
Acquiring fundamental knowledge necessary for a good understanding of the one-dimensional Nuclear
Magnetic Resonance (NMR) molecular spectroscopy applied to 1H and 13C nuclei ; determining the
potential structures of small organic molecules from their 1H and 13C 1D-NMR spectra but also from
their IR vibrational and UV/Vis electronic spectra.
Prerequisite:
Contents: course unit CH1502 (semester 5) Contents:
Chapter I - Introduction: NMR active nuclei ; energy and magnetic/spin states of nuclei in organic molecules ; spin transition and magnetic resonance frequency ; macroscopic magnetization ; basic pulsed NMR principles; the signal in pulsed NMR (FID); relaxation mechanisms ; Fourier Transform of the NMR signal ; intensity of NMR signals and quantitative analysis ; introduction to 13C NMR spectroscopy (NOE effects, 1H decoupling technique). Chapter II - Chemical Shift: definition ; shielding constant ; shielding and deshielding effects ; magnetic
anisotropy of molecules ; chemical shifts of typical 1H and 13C nuclei in organic molecules ; influence of
conformational and chemical exchanges.
Chapter III - Scalar spin-spin coupling: polarization mechanisms ; scalar coupling energy ; coupling and
chemical structure ; typical 1H-1H homonuclear coupling constants (geminal, vicinal, long-range) ;
coupling of 1H nuclei bound to heteroatoms ; chemical equivalence ; magnetic equivalence ; first- and
second-order scalar coupling systems.
Additional information:
Media: copy of PowerPoint presentations are accessible from the intranet
Bibliographical references: none
Assessment: written 2 hour exam without documents (semester 6)
Remarks:
The exam is unique for the two course units CH1502 and CH1602
With regard to directed studies, 6 hours are dedicated to interpretation of IR vibrational and UV/Vis
electronic spectra and 8 hours to interpretation of 1D-NMR 1H and 13C spectra.
CI 1Y
MODULE : ORGANIC AND MOLECULAR CHEMISTRY
SUBJECT:
ADVANCED ORGANIC CHEMISTRY
Coordinator:
Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (3)20 43 48 58
Building C1- Office 101
Compulsory
Code: CH1603
Semester: 6
Lecture: 20 Hours
Directed studies: 12 Hours
Language: French
Coefficient: 3
ECTS: 1.5
Instructor(s):
Gaëlle Fontaine
gaelle.fontaine@ensc-lille.fr
03 20 43 46 83
Bureau 2
Learning outcomes:
Synthesis and reactivity of multifunctional organic compound and heterocycles
Prerequisite:
Contents:
Carboxylic compounds and derivatives Amines Heterocycles Phosphorus, Sulfur, Selenium, Boron and Silicon based compounds
Additional information:
Bibliographical references:
Vollhardt, chimie organique, De Boeck, 1990.
Rabasso, N.: Chimie organique; généralités, études des grandes fonctions et méthodes
spectroscopiques; De Boeck, 2006.
Remarks:
CI 1Y
MODULE : ORGANIC AND MOLECULAR CHEMISTRY
SUBJECT:
INTRODUCTION TO POLYMER CHEMISTRY
Chim
Coordinator:
Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (3) 20 43 48 58
Building C1 - Office 101
Compulsory
Code: CH1604
Semester: 6
Lecture: 8 Hours
Directed studies: 4 Hours
Language: French
Coefficient: 1
ECTS: 1
Instructor(s):
Patrice WOISEL
Frédéric CAZAUX
Learning outcomes:
The purpose of this course is to introduce the basic concepts of polymer synthesis and to describe
leading features of polymers.
At the end of the module, students will be able to:
- understand what polymers are made up of, their properties, and basic polymer nomenclature
- identify the key parameters of the free radical homopolymerization
- understand the principle industrial polymerization processes work
Prerequisite:
CH1503
Contents:
- Introduction to polymer chemistry: historical and economic backgrounds
- Kinetics and thermodynamics of free redical polymerizations
- Industrial polymerization processes
Additional information:
Media: Duplicated lecture note + documents given during the courses
Bibliographical references:
- La polymérisation : Principes et applications
George ODIAN Polytechnica, 1994 ISBN 2840540282
- Chimie et physico-chimie des polymères
Michel FONTANILLE, Yves GNANOU Dunod, 2002 ISBN 2100039822
- Exercices et problèmes de chimie macromoléculaire
Thierry HAMAIDE, Michel BARTHOLIN Editions TEC & DOC, 1999 ISBN 2743003537
Assessment: 1 written exam (1H30)
Remarks:
CI 1Y
MODULE : INORGANIC CHEMISTRY
SUBJECT:
INTRODUCTION TO SOLID STATE CHEMISTRY
Coordinator:
Rose-Noelle Vannier
rose-noelle.vannier@ensc-
lille.fr
+33 (0)3 20 43 65 83 / office
208
Compulsory
Code: CH1506
Semester: 5
Lecture: 16 Hours
Directed studies: 5 Hours
Language: French
Coefficient: 2
ECTS: 1
Instructor(s):
Murielle Rivenet
murielle.rivenet@ensc-lille.fr
03 20 33 64 35 / room 228
Learning outcomes:
To know the main structure types. To quote the structure types of solids with an example. To calculate
compactness of a solid. To determine the coordination number and coordination polyhedron of an
atom or an ion in the solid. To be able to establish the relations between the lattice parameters, the
interatomic or interionic distances and the density within a solid. To describe the intermolecular forces
responsible for the solids cohesion. To analyze the nature and strength of the cohesion forces existing
in a solid. To calculate the lattice energy. To predict the structure of a solid according to Pauling’s rules
and to the calculation of the crystal field stabilization energies (Jahn-Teller effect). To explain the
electrical properties starting from the band theory. To know some physical properties of solids as for
examples: luminescence, lasers, conductivity of graphite and of graphite intercalation compounds,
lithium batteries, applications of semi-conductors. To be able to explain the relation between the
properties of materials and their solid structure.
Prerequisite:
Electronic structure of atoms according to the quantum theory – Periodic table of the elements -
Properties of the elements and their trend along the periodic table - Lewis’s chemical bonding theory –
Basis on the quantum theory of chemical bonding – Prediction of the molecular geometry according to
the Valence Shell Electron Pairs Repulsion (VSEPR).
Contents:
The first part of the lecture aims to describe the crystal structures of various materials according to
their bond types: metals, ionic structures, covalent network structures and molecular structures. The d
electron effects on transition metal compounds are considered on the basis of the crystal field theory
and on the Jahn-Teller effects. A section is devoted to the calculation of the lattice energy of ionic
crystals using either the sum of the electrostatic forces or the Born-Haber cycle and thermochemical
calculations.
The second part introduces the band model for bonding. Then, some of the physical properties of solids
are seen: electronic conductivity and optical properties. This section aims to relate the physical
properties of solids to their electronic and crystal structures. Many applications of solids are considered
in order to illustrate the factors that influence the selection of a material for a particular application.
Additional information:
Media: slides
Bibliographical references: Chimie des solides, Jean-Francis Marucco, Ed. EDP Sciences - Introduction à
la chimie du solide, Lesley Smart, Elaine Moore, Ed. Masson - Solid State Chemistry and its applications,
Anthony R. West, Ed. Wiley - Introduction à la cristallographie et à la chimie structurale, Maurice Van
Meerssche, Janine Feneau-Dupont, Ed. Peeters - Chimie inorganique, André Casalot, André Durupthy,
Ed. Hachette Supérieur
Assessment: a first written exam on prerequisite in november (1 hour of examination) and a final
written exam in January (2 hours of examination)
Remarks:
CI 1Y
MODULE : INORGANIC CHEMISTRY
SUBJECT:
CRISTALLOGRAPHY
Coordinator:
Rose-Noëlle VANNIER
rose-noelle.vannier@ensc-
lille.fr
+33 (0)3 20 43 65 83
C7 A, Office 208
Compulsory
Code: CH1507
Semester: 5
Lecture: 24 Hours
Directed studies:
Language:
French/English
Coefficient: 3
ECTS: 2
Instructor(s):
Rose-Noëlle VANNIER
Learning outcomes:
The aim of this lecture is to give the basics in crystallography to approach the field of materials science,
on one hand, and the analysis of crystalline structures of either mineral or organic compounds, on the
other hand.
Crystallographers have their own rules and language. At the end of this lecture, students should be able
to understand the description of crystalline structure (bibliography) and discuss with specialists in the
field.
They will possesses the necessary bases to approach the characterization of materials by X-ray
diffraction, a technique which is widely used for the analysis of minerals and metals, for instance in the
field of cement or materials recycling.
Prerequisite:
No prerequisite Contents :
In a first part, the lattice and symmetry in crystals are explained. Then, the international tables of
crystallography are introduced. In a second part, X-ray diffraction on single crystal and powder is
described with an emphasis on the evidence of element of symmetry in the crystalline structure.
Additional information:
Media: A copy of the necessary media to follow the lecture will be given to the student. The main part
of the lecture is available on the intranet network of the school.
References:
Eléments de radiocristallographie, R. Ouahes, Ed. Publisud,
Analyse structurale et chimique des matériaux, J.P. Eberhart, Dunod,
Les rayons X, A. Guinier, Collection "Que sais-je ?", Presses universitaires de France,
International Tables for Crystallography, Volume A, edited by Theo Hahn, by Kluwer Academic
Publishers, Dordrecht/Boston/London (1989).
Assessment:
A written exam, 2h.
Remarks:
This subject requires a personal work to master the crystallographic tools. Corrected exercises and
previous exams with their correction are available on the intranet network of the school so that the
student can train themselves.
This lecture is opened to the foreign students within the framework of the international exchanges of
the school and, if needed, it can be given in English
CI 1Y
MODULE : INORGANIC CHEMISTRY
SUBJECT :
INORGANIC AND INDUSTRIAL CHEMISTRY
Coordinator:
Rose-Noëlle VANNIER
rose-noelle.vannier@ensc-
lille.fr
03 20 43 65 83
C7 A, Office 208
Compulsory
Code: CH1606
Semester: 6
Lecture: 20 Hours
Directed studies:
Language: French
Coefficient: 2
ECTS: 1
Instructor(s):
Rose-Noëlle VANNIER
Learning outcomes:
The objective of this lecture is to get a general knowledge on the basic mineral products (halogen,
hydrogen, ammonia, nitric acid, oxygen, nitrogen) from their preparation to their use. Main points are:
electrolysis of Moissan, preparation of chlorine, methane reforming, hydrogen storage, Ni-MH battery,
fuel cells, Li-ion battery, oxygen and the nitrogen separation from air.
Prerequisite:
No prerequisite Contents:
The lecture is divided into 6 chapters: I. Halogens (preparation of fluorine (uranium enrichment), of chlorine, of bromine and iodine)
II. Hydrogen, vector of energy for future, from its production to its storage
III. Hydrides (Ni-MH battery, synthesis of ammonia, nitric acid)
IV. Fuels cells (different kind of FC: PEM, DMFC, MCFC, SOFC, defect in solids, solid state reaction, sol-
gel, shaping techniques)
V. From alkaline cells to Li-ion battery
VI. Oxygen and nitrogen from air (distillation from liquid air, PSA, VSA process)
Additional information:
Media: A copy of the necessary media to follow the lecture will be given to the student. The main part
of the lecture is available on the intranet network of the school.
Bibliographical references:
Techniques de l'Ingénieur,
Actualité chimique,
Cours de chimie minérale, Maurice Bernard, Ed. Dunod,
Chimie industrielle, Robert Perrin, Jean-Pierre Scharff, ed. Masson
Chimie Inorganique, R.B. Heslop, P.L. Robinson, Ed. Flammarion Médecine Sciences
Descriptive Chemistry, Mc Quarries, Rock, Ed. freeman and co, New-York
Assessment: A written exam, 2h.
Remarks:
Corrected exercises and previous exams with their correction are available on the intranet network of
the school...
CI 1Y
MODULE : GENERAL CHEMISTRY
SUBJECT:
THERMODYNAMICS
Coordinator:
Prof. Sergey GORYACHEV
serguei.goriatchev@ensc-
lille.fr
Tel: +33 (0)3 20 33 64 96
Building P5 -Office 221
Compulsory
Code: CH1508
Semester: 5
Lecture: 28 Hours
Directed studies: 9 Hours
Language: French
Coefficient: 4
ECTS: 2
Instructor(s) :
Prof. Sergey GORYACHEV
Prof. Charaffeddine JAMA
Learning outcomes:
Can to use the main thermodynamic functions and relations in Chemical Engineering and Material
Sciences.
Know the behavior, the equations of state and the thermodynamic diagrams of real gases, fluids and
solids.
Be able to deal with the phase transformations.
Know how to calculate a chemical equilibrium state of thermodynamic system.
Prerequisite:
Fluid mechanics. Statistical physics. General thermodynamics.
Contents:
Courses
Statistical thermodynamics. Thermodynamics quantities. Thermodynamics data. Thermodynamics
transformations. Real gases. Phase equilibrium. Solutions. Chemical reactions.
Directed studies
Thermodynamics principles. Functions of state. Chemical potential. Reaction quantities. Evolution
and equilibrium of a system. Variance. Displacement of chemical equilibrium. Binary solid-liquid and
liquid-vapor equilibrium.
Additional information:
Bibliographical references:
1. Landau L., Lifchitz E. - Physique statistique, Ellips, Paris, 1998.
2. Durupthy A. et al. - Thermodynamique chimique, 2de année PC-PC*, Cours avec exercices corrigés,
Hachette, 1996.
3. Brénon-Audat F. et al. - Thermodynamique chimique, 2de année PC-PC*, Exercices et problèmes
corrigés, Hachette, 2003.
4. I. Prigogine, D. Kondepudi - Thermodynamique : des moteurs thermiques aux structures dissipatives,
Edition Odile Jacob, Paris, 1999.
Remarks:
CI 1Y
MODULE : GENERAL CHEMISTRY
SUBJECT:
ELECTROCHEMISTRY IN SOLUTION
Coordinator:
caroline.pirovano@ensc-
lille.fr
+33 (0)3 20 43 49 73
Building C7a - Office 224
Compulsory
Code: CH1501
Semester: 5
Lecture: 9 Hours
Directed studies: 8 Hours
Language: French
Coefficient: 2
ECTS: 1
Instructor(s):
Caroline PIROVANO
Christophe VOLKRINGER
Learning outcomes:
The acquisition of the electrochemistry fundamentals in solution
Prerequisite:
● Basic knowledge acquired in preparatory years
● Complementary knowledge learnt in Practical studies of Analytical Chemistry (TP1501) Contents:
Brief plan of the course:
● Chemical Equilibrium in solution
Thermodynamics, Acid-base equilibrium, Complexation, Solubility and precipitation
● Redox Reactions
The redox potential, The electrochemical potential, Nernst equation, Diagrams of Latimer, Formal
Potential, Diagrams of Pourbaix
● Electrodes
The electrochemical chain, Redox indicator electrodes, Reference electrodes, Ion selective electrodes
● Electrochemical processes - Fundamentals notions
Principle of the production of electrochemical reactions, Faraday's law, Faradaic versus non-faradaic
processes, The electrochemical cells, Galvanic cells, Electrolytic cells, the electrochemical cell for
electroanalytical measurement: the three electrodes cell
Additional information:
Media: lecture manual and materials for tutorial classes. Additional documents are available on the
intranet (annals of the examination with corrections)
Bibliographical references:
● Électrochimie analytique et réactions en solution, B. Trémillon, tome 1 & 2, Éd. Masson (1993)
● Électrochimie, des concepts aux applications, F. Miomandre, S. Sadki, P. Audebert, R. Méallet-
Renault, Sciences Sup, Dunod (2005)
● Electrochemical Methods: Fundamentals and Applications, Allen J. Bard, Larry R. Faulkner, 2nd
edition, Éd. Wiley (2001)
Assessment: An intermediate written examination (1h30 by the end of October or beginning of
November). A final written examination (2h in January).
Remarks:
CI 1Y
MODULE : GENERAL CHEMISTRY
SUBJECT:
APPLIED THERMODYNAMICS
Coordinator :
Compulsory
Code: CH1608
Semester: 6
Lecture: 8 Hours
Directed studies:
Language: French
Coefficient: 1
ECTS: 1
Instructor(s) :
Charlotte.becquart@ensc-
lille.fr
Bâtiment C6, Office 17,
+33 (0)3 20 43 49 44
Learning outcomes:
Use of Ellingham diagramm
A good understanding of phase diagrams
Knowledge of how a blast furnace operates
Knowledge of the processing of Al
Prerequisite:
Thermodynamics (S5)
Contents:
I Processing methods of metals and alloys
II Which method should one use? ; II-1 Reminders in Thermodynamics; II-2 Ellingham Diagramms ; II-3
Oxyde reduction by hydrogen and C oxyde
III Steel processing ; III-1 small historical introduction ; III-2 Fe oxydes ; III-3 The blast furnace ; III-4
Phenomena involved in the process ; III-4 From cast iron to steel ; III-5 Electrical processing of steels ;
III-6 Casting III-7 Rolling
IV Al processing; IV-1 A bit of history IV-2 from the ore to the oxyde: beauxite to Al2O3 ; IV-3 from the
oxyde to liquid Al ; IV-4 processing of the melt ; IV-5 Al Recycling
V Thermodynamical bases for the interpretation of equilibrium diagrams
Additional information:
Bibliographical references: 1/ « précis de métallurgie », Jean Barralis et Gérard Maeder, Edition Nathan,
2005.
2/ « Métallurgie : du minerai au matériau », Jean Philibert, Alain Vignes, Yves Bréchet et Pierre
Combrade, Edition Dunod, 2002
3/ « Phase transformations in metals and alloys », David A. Porter and K.E. Easterling, Van Nostrand
Reinhold (UK) Co. Ltd 1981
4/ « Thermodynamique des matériaux, de l’élaboration des matériaux à la genèse des
microstructures », Gérard Lesoult, Traité des matériaux, Presses polytechniques et universitaires
Romandes, 2010.
Assessment: 1 hour written exam at the end of the course
Remarks:
CI 1Y
MODULE : GENERAL CHEMISTRY
SUBJECT:
KINETICS
Coordinator:
anne-sophie.mamede@ensc-
lille.fr
+33 (0)3 20 33 70 90
Building C3 - Office 106
Compulsory
Code: CH1609
Semester: 6
Lecture: 16 Hours
Directed studies: 4 Hours
Language: French
Coefficient: 3
ECTS: 1
Instructor(s):
Anne-Sophie MAMEDE
Learning outcomes:
The course is designed so that engineering students can acquire and use the concepts of chemical
kinetics: understanding patterns and reaction mechanisms, establishing rate laws and identifying the
factors influencing the rate of the chemical reaction (temperature, pressure, ionic strength in solution,
catalysts ...)
Prerequisite:
Mathematical notions including the integration of differential equations
Basic knowledge in Physical Chemistry gained in preparatory classes (CPGE, CPI, L2, DUT, BTS, ATS…)
Contents:
The first chapter contains general information on chemical transformations and their kinetic evolution
to determine the order of the reaction and its rate constant. The second chapter presents the basic
processes and concepts of rate theories (elementary theory of collisions and activated complex theory).
The third chapter is dedicated to the kinetics of chemical processes in homogeneous phase
(nucleophile substitutions and consecutive, parallel, opposed, chain reactions, etc. ...). The fourth
chapter focuses on the kinetic aspects of reactions in liquid phase with the study of the influence of
diffusion, of the dielectric permittivity of the solvent or of the ionic strength. Catalytic phenomena in
solution, including acid-base and enzymatic catalysis are also discussed. Fifth chapter deals with the
kinetics of heterogeneous catalysis with introduction to the concepts of molecular adsorption and
desorption, of Langmuir isotherm and of BET isotherm characterizing physisorption phenomenon.
Finally some mechanisms of heterogeneous catalysis are presented including the models of Langmuir-
Hinshelwood and of Eley-Rideal.
Additional information:
Media: Class and practical exercises manuals
Bibliographical references:
Introduction à la cinétique chimique, S. Logan, Dunod, 1998
Cinétique et catalyse, G. Scacchi, M. Bouchy, J.-F. Foucaut, O. Zahraa, R. Fournet, Editions Tec&Doc,
Lavoisiser, 2011
Cinétique et catalyse hétérogène, B. Gilot, R. Guiraud, Technosup, Ellipses, 2004
Assessment: Written evaluation of 2 hours with class manual
Remarks:
CI 1Y
MODULE : GENERAL CHEMISTRY
SUBJECT:
ELECTROCHEMICAL METHODS
Coordinator:
caroline.pirovano@ensc-
lille.fr
+33 (0)3 20 43 49 73
Building C7a- Office 224
Compulsory
Code: CH1601
Semester: 6
Lecture: 11 Hours
Directed studies: 12 Hours
Language: French
Coefficient: 3
ECTS: 2
Instructor(s):
Caroline PIROVANO
Christophe VOLKRINGER
Learning outcomes:
In the continuity of the course of electrochemistry in solution (CH1501), this teaching allows to deepen
the general theoretical characteristics of the electrochemical processes and to approach the main
electroanalytical methods.
Prerequisite:
● Electrochemistry in solution (CH1501) Contents:
● Mass transfert
Nernst-Planck equation, convection, migration, diffusion and Fick's laws, the Nernst diffusion layer and
steady-state conditions, the Cottrell equation
● Electrodes kinetics
Standard electrochemical rate constants, Butler-Volmer kinetics, the Tafel law, mass transfer versus
charge transfer
● Current-potential curves: examples and applications
Current-potential curves applications, sensors and biosensors, organic electrochmistry, inorganic
electrosynthesis, corrosion, etc.
● Potentiometry and amperometry
Potentiometric method (at i = 0 and i 0), amperometric method
● Voltammetry
General principle and experimental consideration, polarography and mercury electrodes, cyclic voltammetry, pulse voltammetry, (staircase voltammetry, NPV, DPV, SWV, stripping voltammetry) Additional information:
Media: lecture manual and materials for tutorial classes. Additional documents are available on the
intranet (annals of the examination with correcVolmertions)
Bibliographical references:
● Électrochimie analytique et réactions en solution, B. Trémillon, tome 1 & 2, Éd. Masson (1993)
● Électrochimie, des concepts aux applications, F. Miomandre, S. Sadki, P. Audebert, R. Méallet-
Renault, Sciences Sup, Dunod (2005)
● Electrochemical Methods: Fundamentals and Applications, Allen J. Bard, Larry R. Faulkner, 2nd
edition, Éd. Wiley (2001)
Assessment: written examination (2h in January)
Remarks:
CI 1Y
MODULE : CHEMICAL ENGINEERING
SUBJECT:
FLUID MECHANICS AND HYDRODYNAMICS
Coordinator:
Nouria.fatah@ensc-lille.fr
+33 (3)20335436
Ecole Centrale de Lille
Compulsory
Code : CH1509
Semester : 5
Lecture: 12 Hours
Directed studies: 3 Hours
Language : French
Coefficient : 2
ECTS : 1
Instructor(s):
Nouria/Fatah
Learning outcomes:
Fluid mechanics : Fluid statics, Ideal and real fluid dynamics. Basic relations. Viscosity, pressure drop
(on line and miscellaneous). Piping design and specifications. Fluid pumping, centrifugal pump
specification.
Prerequisite:
Unit operations: Elementary knowledge gained in preparatory classes (CPGE, CPI, DEUG, DUT, BTS, ATS, Licence) Contents:
Introduction-Basic definitions-Symbols and Unit-Definition of the pressure and physical flow-Properties of the liquid- Fluids Statics- Energy conservation system- fluids dynamics - pressure and fluid measurement, pumps. Additional information:
Media:
Copy of slides presentation
Bibliographical references:
-Coulson J.M., Richardson J.F. , ‘Chemical Engineering’, Pergamon Press 1990
-R.Byron Bird, Warren Stewart, et E.N. Lightfoot : “Transport phenomena”, John Wiley & Sons 2001
-Cours de Mr Acloque (site intranet de l'ENSCL)
Assessment:
Lectures: 5 sessions of course, 1h20 duration and 2 sessions of class work, 1h 20 duration.
Written exam 2h, without documents
Remarks:
CI 1Y
MODULE : CHEMICAL ENGINEERING
SUBJECT:
HEAT AND EXCHANGE TRANSFER
Coordinator:
Nouria.fatah@ensc-lille.fr
+33 (3)20335436
Ecole Centrale de Lille
/Building C
Compulsory
Code : CH1610
Semester : 6
Lecture: 10 Hours
Directed studies: 4 Hours
Language : French
Coefficient : 2
ECTS : 1
Instructor(s):
Nouria/Fatah
Learning outcomes:
General. Heat transmission by radiation, conduction. Different types of heat exchangers. General
relations for heat transfer coefficients. Design of shell and tube exchangers. Special study of
evaporators, reaction vessels - steady and unsteady operation.
The goal of this class : Analysis of heat transfer problems : méthodology
Prerequisite:
Fluid mechanics and applied thermodynamics
Contents:
-Units and dimensions -Physics origins and rate equations (conduction, convection and radiation)-conservation of Energysrequirement-Heat Exchangers (Heat exchangers types, heat exchangers analysis, heat exchangers design and performance calculations) Additional information:
Media : copy of slides presentation
Bibliographical references:
-Coulson J.M., Richardson J.F. , ‘Chemical Engineering’, Pergamon Press 1990
-R.Byron Bird, Warren Stewart, et E.N. Lightfoot : “Transport phenomena”, John Wiley & Sons 2001
-Course : A. Acloque (site intranet de l'ENSCL)
Assessment: Lectures: 6 sessions of course, 1h20 duration and 2 sessions of class work, 2h duration.
Written exam 2h, without documents,
Remarks:
CI 1Y
MODULE : CHEMICAL ENGINEERING
SUBJECT:
MASS TRANSFER AND ABSORBERS
Coordinator :
Nouria Fatah
Nouria.Fatah@ensc-lille.fr
+33 (0)3.20.33.54.36
Ecole Centrale de Lille
Building C.
Compulsory
Code: CH1611
Semester: 6
Lecture: 11 Hours
Directed studies: 4 Hours
Language: French
Coefficient: 2
ECTS: 1
Instructor(s) :
Marek Czernicki
Learning outcomes:
Main objective of this course is to give basic concepts of the absorption process. This lecture covers the
methods used to calculate the absorbers. Diffusive and convective mass transfer is presented. Different
methods to calculate mass transfer coefficients are shown
The goal of this class is that students will develop a conceptual understanding of mass transfer
processes
Prerequisite:
Topics to be covered include: Principles of mass transfer, diffusion in gas and liquid, Fick's laws of diffusion. Differential equations of mass transfer, determination of mass transfer coefficient, calculation of counter-current and co-current packed bed columns. Contents:
Topics to be covered include: Principles of mass transfer, diffusion in gas and liquid, Fick's laws of diffusion. Differential equations of mass transfer, determination of mass transfer coefficient, calculation of counter-current and co-current packed bed columns.
Additional information:
Media: copy of presentation
Bibliographical references:
Coulson J.M., Richardson J.F. , ‘Chemical Engineering’, Pergamon Press 1990
-R.Byron Bird, Warren Stewart, et E.N. Lightfoot : “Transport phenomena”, John Wiley & Sons 2001
-Lefrançois B., ‘Chimie Industrielle’, Technique et Documentation Lavoisier, Paris 1995
-Techniques de l’Ingénieur, Transfert de matière J1077, Distillation absorption colonnes garnies J2626,
Cinétique de transfert de matière entre 2 phases J1075.
- Lieto J., ‘Le Génie Chimique à l’Usage de Chimiste’, Techniques et Documentation, Lavoisier, Paris
1998
-J.L. Humphrey, G.E. Keller, ‘Procédés de séparation’, Dunod, Paris 2001
Assessment: Lectures: 8 sessions of course, 1h20 duration and 2 sessions of class work, 2h, duration.
Written exam 2h, without documents
Remarks:
Student will be able to do typical basic calculations involving mass transfer. This includes calculations of
packed bed absorption columns and mass transfer coefficients
CI 1Y
MODULE : COMPUTER SCIENCE AND APPLIED STATISTICS
SUBJECT:
APPLIED STATISTICS
Coordinator:
serguei.goriatchev@ensc-
lille.fr
+33 (0)3 20 33 64 96
Office 221
Building P5
Compulsory
Code: CH1510
Semester: 5
Lecture: 15 Hours
Directed studies:
Language: French
Coefficient: 2
ECTS: 2
Instructor(s):
Prof. Sergey GORYACHEV
Learning outcomes:
Every measure involves inevitable errors, and above all in an industrial context, it matters to be able to
evaluate their importance. In that course, practical indications are given on methods of errors
estimation.
Prerequisite:
Mathematics (Probabilities)
Contents:
Probabilities and statistics.
Sampling.
Estimation of statistical parameters.
Statistical tests.
Comparison of frequencies, means, variances and distribution functions.
Correlation.
Linear regression.
Additional information:
Bibliographical references:
F. Dress, Probabilités et Statistique (Rapppels de cours ), Dunod, Paris (1997).
F. Couty, J. Debord et D. Fredon, Probabilités et Statistiques (Résumés de cours et 157 exercices),
Dunod, Paris (1999).
R. Veysseyre, Statistique et probabilités pour l’ingénieur, Dunod, Paris (2004).
W. W. Hines, Probabilités et Statistique pour ingénieurs, Chenelère Education, Montréal (2005).
Remarks:
CI 1Y
MODULE : COMPUTER SCIENCE AND APPLIED STATISTICS
SUBJECT :
DATA SYSTEMS AND TREATMENT
Coordinator :
Ludovic.Thuinet@univ-lille1.fr
+33 (0)3 20 33 62 25
Office 232
Building C6
Compulsory
Code: CH1511
Semester: 5
Lecture:
Directed studies: 10 Hours
Language: French
Coefficient:
ECTS :
Instructor(s) :
Ludovic Thuinet
Serguei Goriatchev
Learning outcomes:
To know how to use some chosen software and numerical tools in order to deal with data.
● Optimal use of Excel to program formulas and to calculate them, to plot graphs from calculated data
in Excel or from other source files. Organization of the calculation sheet to solve a complex scientific
problem
● To know how to use a programming software, i.e. to master the syntactic rules, to know the different
types of variables. To be able to write short numerical algorithms with loops and conditional operators
Prerequisite:
None Contents:
General presentation of Excel: cell format, formulas insertion, absolute/relative references…
How to plot graphs with Excel and how to analyze the data (bars of uncertainty, linear regression…)
Use of specific tools in Excel, like Solver
General presentation of the programming language Scilab: syntactic rules, main types of variables
How to use or create input/output data with Scilab
Use of loops "for" and "while" and conditional operators (if-then-else-end)
Additional information:
Media: 2 short documents summarizing the main features of Excel and Scilab. Students are also given
User manuals for Word and Powerpoint and a document entitled "how to write a report: guide to
authors", but these are not the topic of any exercises in this module.
Bibliographical references: A complete documentation on Scilab is at the disposal of the students on
the ENSCL Intranet. Various examples of scientific problems solved with Scilab can be found on the
ENPC website: http://cermics.enpc.fr/scilab_new/site/
Assessment: Students are assessed on the knowledge taught in this module through the module
physical chemistry-practical studies (TP1502), in which they have to use these numerical tools.
Remarks:
CI 1Y
MODULE :ANALYTICAL CHEMISTRY (Practical studies)
SUBJECT:
ANALYTICAL CHEMISTRY
Chim
Coordinator:
caroline.pirovano@ensc-
lille.fr
+33 (0)3 20 43 49 73
Office 224
Building C7a
Compulsory
Code: TP1501
Semester: 5
Practical studies: 36 Hours
Project:
Language: French
Coefficient: 7
ECTS: 4.5
Instructor(s):
Teachers:
Anne-Sophie MAMEDE
Caroline PIROVANO
Fabienne SAMYN
Christophe VOLKRINGER
Technical staff:
Catherine CANDELIER
Maxence VANDEWALLE
Learning outcomes:
The objectives of this cycle of Practical class of Analytical Chemistry are:
● The acquisition of the basic notions in analytical chemistry in aqueous solution
● The acquisition of Good Laboratory Practice (GPL) through the development of care, initiative, rigour.
respect for the conditions of hygiene and safety in laboratory, writing a laboratory notebook…
● The control of all the operations to be performed during any manipulations: the preparation
(conceptions of experimental protocols), the realization and the interpretation of the results.
Prerequisite:
● Classical methods learnt in preparatory classes
● Notions of safety in laboratory (FE1501-3)
Contents:
The practical class of Analytical Chemistry begins with an initiation to the classical laboratory
techniques (Tutorial classes and preparatory practical classes). Once this preparatory cycle
accomplished in small groups, the students work then individually at fixed post, every student having
his own material, he prepares his solutions, titrates and calibrates them.
The studied titrations are:
● acid-base titration
● gravimetric titration
● complexometric titration
● redox titration
Additional information:
Media: manual of practical class of Analytical Chemistry
Bibliographical references:
● Vogel's Quantitative Chemical Analysis, 6th Ed., 2000, Pearson Education Limited
● Fundamentals of analytical chemistry, D.A. Skoog, D.M. West, F.J. Holler, eighth edition, Thomson-
Brooks/Cole, 2004
Assessment: students are evaluated on their results and the quality of manipulation, the reports. Oral
interrogations to test the preparation as well as short written examinations are possible during the
practical session.
Remarks:
CI 1Y
MODULE : PHYSICAL CHEMISTRY (Practical studies)
SUBJECT:
PHYSICAL CHEMISTRY
Chim
Coordinator:
caroline.pirovano@ensc-
lille.fr
+33 (0)3 20 43 49 73
Office 224
Building C7a
Compulsory
Code: TP1502
Semester: 5
Practical studies: 40.5 Hours
Project:
Language: French
Coefficient: 7
ECTS: 4.5
Instructor(s):
Teachers:
Charlotte BECQUART
Serguei GORIATCHEV
Anne-Sophie MAMEDE
Caroline PIROVANO
Fabienne SAMYN
Ludovic THUINET
Technical staff:
Catherine CANDELIER
Learning outcomes:
This cycle of practical works led the students to discover new experimental techniques and to check
concretely the fundamental laws, the theoretical principles and the specific methods of physical
chemistry.
The use of computing tools allows the students to acquire the control of these tools (through the
exploitation of their results, programming, modelling and the writing of reports).
Prerequisite:
● Basic knowledge acquired in preparatory years and in practical classes of Analytical Chemistry
(TP1501)
● Knowledge learnt in the courses of general chemistry: electrochemistry (CH1501), thermodynamic
(CH1508), spectroscopy (CH1502), chemical kinetics (CH1609)
● Knowledge acquired in the data systems and treatments module (CH1511)
● Notions of safety in laboratory (FE1501-3)
Contents:
In this cycle of manipulations are thus approached:
● Electrochemical methods ( potentiometry, conductimetry, polarography...)
● Chemical kinetics
● Spectroscopic methods (spectroscopy U.V. and atomic spectroscopy)
● Thermal analyses
● Modelling
Additional information:
Media: a manual of practical class of Physical Chemistry given to the students and additional
documentations are available in the laboratory during the sessions.
Bibliographical references:
● Analyse Chimique. Méthodes et techniques instrumentales modernes; F. Rouessac, A. Rouessac,
Dunod
● Fundamentals of analytical chemistry, D.A. Skoog, D.M. West, F.J. Holler, eighth edition, Thomson-
Brooks/Cole, 2004
Assessment: Reports, oral preparation test, written theorical examination possible at the end of the
practical classes
Remarks:
CI 1Y
MODULE : CHEMICAL CHEMISTRY (Practical studies)
SUBJECT:
CHEMICAL ENGINEERING
Chim
Coordinator:
Nouria.fatah@ec-lille.fr
+33 (0)3.20.33.54.36
Ecole Centrale de Lille
Building C
Compulsory
Code : TP1503
Semester : 5
Practical studies: 15 Hours
Project:
Language : French
Coefficient : 3
ECTS : 2
Instructor(s):
R. BECHARA, M. CZERNICKI, F.
DHAINAUT et N. FATAH
Learning outcomes:
Practical works of Chemical engineering program: theory, practice and calculations. The experimental training try to carry out a harmonization between the basic disciplines of the chemistry and those of Chemical engineering. The unit operations of Chemical engineering (praticals): -Hydrodynamics in a packed column, -Heat exchanger -Fluid mechanics
Prerequisite:
Elementary knowledge gained in preparatory classes (CPGE, CPI, DUT, BTS, ATS) Notions of fluid flow, mass transfer and heat transfer.
Contents:
Practical work of Chemical engineering gathers theory, practical program and numerical modelling. They try to carry out an harmonization accentuated between the basic disciplines of chemistry and those of Chemical engineering and target three objectives: - to supplement the course of the teaching of Chemical engineering. - to confront the students with semi-industrial scale pilots during a sufficient working time in order to obtain results of good quality and into practice to put the theoretical teaching exempted at the time of the courses and directed work -Numerical Modeling : The purpose of this study is to introduce the modelisation possibilities offered by Comsol. In the first part, the design of an heat exchanger allows to review the fundamental of technical drawing in 3D. Then, flows across a cylinder are modelled, in laminar state according to the Navier-Stokes equations, but also in turbulent state with the k- model. In the last part, a multiphysics phenomena, between 2 equation systems is accomplished by considering the convection and conduction phenomena in order to take into account the heat transfer. Manipulations are the following: Hydrodynamics in a packed column, Heat exchanger Fluid mechanics
Additional information:
Media: Teachers documents
Bibliographical references: Courses of chemical engineering P. Wuithier : Raffinage et Génie Chimique, ed. Technip Perry : Chemical Engineers Handbook, Mc Graw Hill Mc Cabe & Smith: Unit Operations of Chemical Engineering, Mc Graw Hill
Assessment: Written report
Remarks:
CI 1Y
MODULE : INORGANIC CHEMISTRY (Practical studies)
SUBJECT:
INORGANIC CHEMISTRY
Chim
Coordinator:
Catherine Renard
catherine.renard@ensc-lille.fr
+33 (0)320434434
Building C7A, office 226
Compulsory
Code: TP1603
Semester: 6
Practical studies: 48 Hours
Project:
Language: French
Coefficient: 7
ECTS : 4.5
Instructor(s):
Teachers :
Marie Colmont
Murielle Rivenet
Catherine Renard
Nathalie Tancret
Christophe Volkringer
Technical staff :
Catherine Candelier
Learning outcomes:
- Carry through a synthesis from a detailed protocol and master the methods of analysis,
- Know how to write the chemical equations and to exploit the results,
- Know the safety rules and how to manage waste.
Prerequisite:
Contents: Know the glassware and its use
Have acquired the basics of analytical chemistry and physical chemistry
Contents:
The purpose of this lab is to introduce engineering students to the multiplicity of preparation
techniques of inorganic chemistry - by ceramic method, in solution, by co-precipitation - and synthesis
of commodity chemicals (sodium carbonate by the Solvay process, soda and chlorine by electrolysis)....
The products obtained after each synthesis must be characterized, this brings the engineering students
to apply their knowledge in analytical and physical chemistry. It is also an opportunity to introduce
engineering students to physicochemical techniques of analysis such as X-ray diffraction, thermal
analyzes
Additional information:
Media:
Bibliographical references:
Assessment:
Reporting of practical work,
Practical assessment : preparation, understanding of the practical work, general behavior,
Final written examination (1h)
Remarks:
CI 1Y
MODULE : ORGANIC CHEMISTRY (Practical studies)
SUBJECT:
ORGANIC CHEMISTRY
Chim
Coordinator:
Vangelis.agouridas@ensc-
lille.fr
03.20.43.44.40
Building C3, office 210
Compulsory
Code: TP1604
Semester: 6
Practical studies: 36 Hours
Project:
Language: French
Coefficient: 7
ECTS: 4.5
Instructor(s):
Vangelis Agouridas
Learning outcomes:
Organic Synthesis, Purification and characterization of organic compounds by FTIR, NMR
Prerequisite:
Basic Organic Chemistry (Sem 4)
Contents:
9*4h session:
1. Distillation (evaluation of purity by Gas Chromatography)
2. Liquid-liquid extraction
3. Purification of a solid by recristallization
4. Friedel-Craft acylation of toluene (GC, FTIR)
5. Functional group protection (FTIR)
6. Grignard addition (FTIR, NMR)
7. Wittig Olefination under microwave + column chromatography (FTIR, NMR)
8. Green synthesis of heterocycles + introduction to green metrics (FTIR, NMR)
9. Camphor: oxidation et stereoselective reduction (GC, FTIR, NMR)
Additional information:
Media:
Handout
Bibliographical references:
Purification of laboratory chemicals fifth edition, 2003, W. L. F. Armarego and C. L. L. Chai, Butterworth
Heinemann (imprint of elsevier science), ISBN 0-7506-7571-3
Assessment:
Continual assessment + 1*2h written exam
Remarks:
CI 1Y
MODULE : SUSTAINABLE DEVELOPMENT
SUBJECT:
FUNDAMENTALS OF SUSTAINABLE DEVELOPMENT
Coordinator:
Jean Claude Van Duysen
Compulsory
Code: FE1501-1
Semester: 5
Lecture: 8 Hours
Directed studies:
Language: French
Coefficient: 5
ECTS: 1
Instructor(s):
Jean Claude Van Duysen
Learning outcomes:
The course has for objectives 1) to explain the concept of sustainable development, 2) to show how
this concept became influential and 3) to describe the way it is used in current society (companies,
cities, etc.).
The student will acquire all the cultural bases needed to apply sustainable development principles in his
professional career, and more globally in the society.
Prerequisite:
There is no prerequisite to follow the course.
Contents:
The course will explain:
the sustainable development principles,
the origins of the environmental consciousness and notion of sustainability,
the current issues of the planet (environment, energy, social, etc.),
the national and international regulatory context supporting a sustainable development,
the implementation of sustainable development principles in current society,
three examples of application of these principles in industry: reduction of CO2 emissions, green
growth and energy efficiency.
Each lecture will partially rely on a discussion between the Professor and the students, in particular on
themes regarding current society.
Additional information:
Support:
Regular reading of a daily newspaper or a societal magazine.
Bibliographical references :
J. C. van Duysen et Stéphanie Jumel, le Développement Durable, éditions l’Hamarttan, 2008.
Site Internet de Jean-Marc Jancovici : http://www.manicore.com/inc_menu/plan_fr.html
Stratégie Européenne en faveur du développement durable :
http://europa.eu/legislation_summaries/environment/sustainable_development/l28117_fr.ht
m
Site Internet du Ministère du Développement Durable :
http://www.developpement-durable.gouv.fr/
André Jean Guérin et Thierry Libaert, Le développement durable, Dunod. Topos. 2008.
Assessment :
no exam.
the knowledge acquired by the students during the course is assessed through the interest they
manifest during the lectures, the level of their involvement in a dialogue with the professor,
and their participation in the « Ingenieur 21 » cell which is in charge of managing sustainable
development activities within the School.
Remarks:
CI 1Y
MODULE : SUSTAINABLE DEVELOPMENT
SUBJECT:
INDICATORS OF SUSTAINABILITY
Coordinator:
Jean Claude van Duysen
Compulsory
Code: FE1501-2
Semester: 5
Lecture: 4 Hours
Directed studies:
Language: French
Coefficient: 5
ECTS : 1
Instructor(s):
Jean Claude van Duysen
Learning outcomes:
The course has for objectives to train the student 1) to use the main indicators of sustainability and 2)
to contribute to the writing of a “sustainable development report”.
At the end of the training, the student:
will have understand the principles on which rely the indicators taken into account,
will have identify the strengths and weaknesses of these indicators,
will be able to calculate them,
will be able to interpret the results and define an action plan to improve them,
will know the main rubrics required in a “sustainable development report”.
Prerequisite:
The only prerequisite is to have assimilated the notions presented in the course on “the foundation of
sustainable development”.
Contents:
The course focuses on three indicators of sustainability:
ecological footprint,
carbon accounting,
external costs.
For each of these indicators, the course will detail:
the principles on which relies the indicator,
the calculation method,
the strengths and weaknesses.
The course includes also a description of the main rubrics required in “sustainable development report”,
as well as an analysis of some “sustainable development reports” from large French companies.
Additional information:
Bibliographical references:
WWF Living Planet Report : http://awsassets.panda.org/downloads/lpr2010.pdf
Calcul de l’empreinte écologique du Grand Lyon :
http://www.grandlyon.com/fileadmin/user_upload/Pdf/developpement_durable/referentiel_envir
onnement/2004118_gl_referentiel_environnement_empreinteecolo.pdf
Qunatification des coûts externes liées à la pollution atmosphériques :
http://web.me.com/arirabl/Site/Publications_files/Re%CC%81sultatsExternE-PollAtmos.pdf
Bilan de Carbone – ADEME :
http://web.me.com/arirabl/Site/Publications_files/Re%CC%81sultatsExternE-PollAtmos.pdf
Assessment:
no exam.
the knowledge acquired by the students during the course is assessed through the interest they
manifest during the lectures, the level of their involvement in a dialogue with the professor,
and their participation in the « Ingenieur 21 » cell which is in charge of managing sustainable
development activities within the School.
Remarks:
CI 1Y
MODULE : SUSTAINABLE DEVELOPMENT
SUBJECT:
SECURITY AND RISKS
Coordinator :
Serge.bourbigot@ensc-lille.fr
+33 (0)3.20.43.48.8
Building C7 - office 8
Compulsory
Code: FE1501-3
Semester: 5
Lecture: 8 Hours
Directed studies:
Language: French
Coefficient: 5
ECTS: 1
Instructor(s) :
Serge BOURBIGOT
Learning outcomes:
To learn the basics of lab safety and of methods of risk analysis
Prerequisite:
Basics in chemistry Contents :
Lab safety: the basic rules for the chemist, labelling, what to do if…?, protect yourself, signboard, the experiments, risk estimation Risk analysis: general approach for risk analysis, preliminary analysis of risk, fault tree analysis, Hazop method, Mosar method
Additional information:
Media: Powerpoint
Bibliographical references: La sécurité en laboratoire de chimie et de biochimie par
André Picot - La Gestion Des Risques, Manuel De Mise en Œuvre par Pierre Périlhon
Assessment:
Remarks:
CI 1Y
MODULE : SUSTAINABLE DEVELOPMENT
SUBJECT:
LIFE CYCLE ANALYSIS
Coordinator :
Serge.bourbigot@ensc-lille.fr
+33 (0)3.20.43.48.8
Building C7 - office 8
Compulsory
Code: FE1501-4
Semester: 5
Lecture: 8 Hours
Directed studies:
Language: French
Coefficient: 5
ECTS: 1
Instructor(s) :
Serge Bourbigot
Learning outcomes:
To learn the basics of life cycle analysis
Prerequisite:
No specific knowledge is required Contents :
Climat and energy LCA definition How to make LCA? LCA in context LCA and reduction of environmental impacts Examples SimaPro software
Additional information:
Media:
Bibliographical references:
Assessment: ACV project with report and defense
Remarks:
CI 1Y
MODULE : ENGLISH
SUBJECT:
ENGLISH
Chim
Coordinator:
Anne GUEGAND
Abdelamar BENAÏSSA
Office 965
Tel:+33 (3)20336060
Compulsory
Code: LV1501
Semester(s): 5+6
Lecture:
Directed studies: 80 Hours
Language: English
Coefficient: 9
ECTS: 5
Instructor(s):
Anne GUEGAND
Abdelamar BENAÏSSA
Learning outcomes:
Language tuition at the ENSCL has a double objective:
-To help all students develop the communication skills they will need in professional situations through
interactive practice activities.
- To encourage prospective graduates to develop an international opening onto foreign companies and
universities to facilitate cross-cultural adaptability and adaptation.
Contents:
-TOEFL
-Ist year topics (for example: Travelling, Work, Education…)
Additional information:
Media: Various (newspaper articles, publications, video documents, case studies…)
Assessment: Continuous language assessment is carried out through two written tests, an interview
and a presentation in English.
Remarks:
No English course for beginners
CI 1Y
MODULE : GERMAN
SUBJECT:
GERMAN
Chim
Coordinator:
Beate WINKLER
beate.winkler@ensc-lille.fr
Tel. +33 (0)320336061
Office 951
Compulsory
Code: LV1502
Semester(s): 5+6
Lecture:
Directed studies: 80 Hours
Language: German
Coefficient: 9
ECTS: 5
Instructor(s):
Beate WINKLER
Monika BERTOUT
Nathalie CHAPTAL
Caroline SIPPL
Learning outcomes:
Prerequisites:
All levels.
Pupils who have never studied German can enroll in a course for "beginners".
Objectives and skills referred:
Progress in the four language skills, but especially in the two that cause the greatest problem (listening
comprehension and oral expression) to validate at least the level B1 or B2 (A2 for the beginners) of the
CEFR.
Ability to integrate in a professional environment (with regard to courses and internships at University
or in foreign companies) and to communicate in situations of everyday life; acquisition of basic
knowledge of scientific and technical German in the field of chemistry
Contents:
Non-exhaustive list - all aspects are not always treated and sometimes deferred or deepened in the
second year:
school career: learn how to describe personal curricula and talk about own motivation, differences
between the educational systems; the student life.
Work: basic business vocabulary, internships; writing a CV, letter of motivation, e-mails. Reflection on
the way how to submit and first simulations of telephone interviews with the intention to the search
for internships; active search for internships…
Housing: housing search (internship), administrative approaches, living in collocation, "casting" with
future roommates …
Means of communication: specific vocabulary of the telephone, the computer; discovery of the main
websites of German information…
Food, food security, health: vocabulary of everyday life, an aspect of the chemistry in the area of food.
Travel and work in German speaking countries: (focusing on the internship), administrative procedures,
geography, tourism, intercultural aspects …
working in chemical laboratories: basic vocabulary, describe basic experiments
Additional information:
Media:
Various authentic media (print media, audio, video, movies, business documents, the internet).
The method "Studio D" for beginners.
Bibliographical references:
Books, movies in original version and journals are available on loan in a small German library.
Assessment:
Continuous language assessment is carried out through at least two written tests (two hours each) and
an oral test divided into two parts (a presentation and an interactive part)
Remarks:
Students are strongly encouraged to confirm their level by a certification in cooperation with the
Goethe-Institute:
"Zertifikat Start 2" (level A2 of the CEFR) for beginners.
"Zertifikat Deutsch" (Level B1 /B2 /C1 of the CEFR) for the more advanced students.
CI 1Y
MODULE : SPANISH
SUBJECT:
SPANISH
Chim
Coordinator:
Compulsory
Code: LV1506
Semester(s): 5+6
Lecture:
Directed studies: 80 Hours
Language: Spanish
Coefficient: 9
ECTS: 5
Instructor(s):
Hakima Larabi
Learning outcomes:
Strengthening B1 level of the Frame Common reference European for Languages, preparation for B2
level. (At the end of the 1st year, the student must be able to talk about basic scientific subjects).
Helping all students develop the communication skills they will need in professional situations (through
interactive practice activities).
Contents:
Linguistic, scientific and cultural aspects: - Oral comprehension: multimedia language laboratory or video sequence. - Oral expression: simulations and role play activities. - Written understanding: scientific or cultural texts. - Written grammatical Competences - Written expression (writing a CV, a letter, an email…) Additional information:
Media: Various (newspaper articles, audio and video documents…)
Bibliographical references: Actividades para el Marco Común B2 (ELE).
Assessment: Continuous language assessment is carried out through two written tests, an interview
and a presentation in spanish
Remarks:
No Spanish course for beginners.
CI 1Y
MODULE : FRENCH AS A FOREIN LANGUAGE
SUBJECT :
FRENCH AS A FOREIN LANGUAGE
Chim
Coordinator :
Catherine FORTUNATO
Polytec 'Lille
Compulsory
Code : LV1505
Semester(s) : 5+6
Lecture:
Directed studies: 50 Hours
Language :
Coefficient : 9
ECTS : 5
Instructor(s) :
Catherine FORTUNATO
Polytec 'Lille
Learning outcomes :
Good knowledge of language in particular at a professional level: understanding the main part of a
text, take current notes, express one's opinion in a brief but clear way on a general or professional
subject.
Contents :
3 hours/week of Fench as a Foreign language
Additional information:
Media :
Bibliographical references:
Assessment:
Remarks:
CI 1Y
MODULE : JAPANESE (OPTIONAL)
SUBJECT:
JAPANESE (OPTIONAL)
Chim
Coordinator:
Jean-Luc RIGAL
Jean-luc.rigal@enscl-lille.fr
Office 951
Compulsory
Code: LV1504
Semester(s): 5+6
Lecture:
Directed studies: 60 Hours
Language: Japanese
Coefficient:
ECTS:
Instructor(s):
Geoffrey DUCATILLON 1 2
Hitomi KIMURA 3
Aki KIUCHI 1
Nozomu MIZUKAMI 2
Shoko MORITA 4 5
Jean-Luc RIGAL 1 2 3
Maki TAMAOKI 1
Sachie WATANABE 2
Learning outcomes:
The main object of this course is to give basic communication tools to the students who intend to do their first, second or/and third year industrial placements in Japan, but also to complete the curriculum of future managers of a branch of industry which has many relations with Japan.
Contents:
One third of the course is devoted to civilization and two thirds to language. Because of the very particular writing system of Japanese, in which two syllabaries and at least 2000 ideograms are combined, reading and writing are given the same importance as oral work. In addition to the learning and systematic use of the two syllabaries, strong emphasis is put on the logic of ideograms, the objective being, through the study of a few hundreds of them, to facilitate the subsequent assimilation of those - much more numerous - which are necessary to everyday life.
Level 1: In particular, Nihongo shoho 1-6, Hiragana nyûmon, Kanban no kanji, Survival Japanese,
JDSR 1-5 .
Additional information:
Media:
Minna no nihongo, Nihongo shoho (1, 2, 3), Nihongo chûkyû, Kana nyûmon (hiragana 1) (katakana 2),
Nelson Kan’ei jiten (2, 3), Kanji for everybody (2, 3)
Bibliographical references:
Nihon etoki jiten 1-16 (JTB), Nihongo notes 1-5 (The Japan Times), Situational Japanese 1-5 (The Japan
Times)
Assessment:
Oral and written exams, continuous assessment
Remarks:
The course is divided into 5 levels, and not according to the three years of the curriculum. As a matter of fact, if Level I is mainly attended by first year students, Level II by second year students and Level III by third year students, some students start the study of Japanese in their second/third year, whereas other students - especially those who come from the "CPI" - may have been studying Japanese for two years or more when they start their engineering studies.
Prerequisites:
None, other than the desire to learn Japanese (WRITTEN INCLUDED)
CI 1Y
Année 2012-2013
4th academic year (semesters 7 and 8)
MODULE : ORGANIC AND MOLECULAR CHEMISTRY
SUBJECT:
SYNTHESIS STRATEGY IN ORGANIC CHEMISTRY
Coordinator:
Professor Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (3) 20 43 48 58
Office 101 Building C1
Compulsory
Code: CI2703
Semester: 7
Lecture: 15 Hours
Directed studies: 14 Hours
Language: French
Coefficient: 3
ECTS: 1.5
Instructor(s):
Philippe Cotelle
Learning outcomes:
Being able of proposing a multi-step synthesis of a molecule of moderate complexity
Prerequisite:
Organic chemistry of monofunctional molecules, semester S5 module CH1503 and semester S6 module
CH1603
Contents :
Introduction: Analysis and synthesis approach Linear and convergent multi-step synthesis
Protection/deprotection: the protective groups
Selectivity
Chemio, regio, stereoselectivity
Enantiospecificity and asymmetric induction
Enantiomer resolution
Use of natural starting material
Use of chiral auxiliary
Enantioselective catalysis
Retrosynthesis: the disconnection approach
The course will be based itself on simple examples of total synthesis
Additional information:
Media:
Bibliographical references: F. A. Carey, R. J. Sundberg, Advanced organic chemistry, volume 2, 3rd Ed,
De Boeck, 1997, ISBN-10 2-8041-5233-2.
S. Warren, P Wyatt, Organic chemistry : the disconnection approach, 2nd Ed, Wiley, 2008, ISBN-978-0-
470-71237-5
Assessment: Written exam (2 hours) at the end of the semester (january)
Remarks:
CI 2Y
MODULE : ORGANIC AND MOLECULAR CHEMISTRY
SUBJECT:
ORGANOMETALLIC CHEMISTRY
Coordinator :
Pr Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (3) 20 43 48 58
Office 101 Building C1
Compulsory
Code: CI2705
Semester: 7
Lecture: 8 Hours
Directed studies:
Language: French
Coefficient :
ECTS: 1
Instructor(s) :
Pr PELINSKI Lydie
Lydie.pelinski@ensc-lille.fr
+33 (0) 3 20 43 65 01
ENSCL, Bureau 106
Learning outcomes:
The objective of this course is to get the student the importance of organometallic chemistry as a tool
in organic synthesis and bring her knowledge in this field.
Prerequisite:
Bases acquired in organic chemistry in 1st year.
Contents :
Introduction to organometallic chemistry, general properties of organometallic complexes and their
preparation.
Particular bound metal-ligand, backdonation
Organometallics: electronic effects, protecting and stabilising groups
Reaction of cyclisation: Pauson-Khand reaction, metallacyles with titanium, trimerisation of alkynes
Additional information:
Media :
Chimie organométallique, Didier Astruc, Ed EDP Sciences.
Chimie organique : Hétéroéléments, stratégies de synthèse et chimie organométallique, Nicolas
Rabasso, Ed. De Boeck.
Bibliographical references:
Assessment: no evaluation
Remarks:
CI 2Y
MODULE : ORGANIC AND MOLECULAR CHEMISTRY
SUBJECT:
APPLIED SPECTROSCOPY
Coordinator:
Pr Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (3) 20 43 48 58
Office 101 Building C1
Compulsory
Code: CI2702
Semester: 7
Lecture: 17 Hours
Directed studies: 6 Hours
Language: French
Coefficient: 3
ECTS: 1.5
Instructor(s):
Eric BUISINE
(NMR course)
Caroline TOKARSKI
(mass spectrometry and
chromatography: course and
directed studies)
caroline.tokarski@univ-
lille1.fr
Phone: +33 (0)3 20 33 64 33
MSAP - C4
Learning outcomes:
Mass spectrometry and chromatography (12-hour course and 6-hour directed studies): develop strong
theoretical knowledge; interpret mass spectra allowing chemical molecule identification (low molecular
weight organic molecules, macromolecules, polymers, etc.); identify the most suitable instruments for
specific applications (target molecule and specific question) and describe the extent and limitations of
the data obtained.
NMR (5-hour course): initiate to 2D-NMR spectroscopy; have a good understanding of homo-nuclear
1H-1H and hetero-nuclear 1H-13C 2D correlation experiments; after NMR practicals (TP2701, semester
7), being able to determine the structures of small organic molecules from their related sets of 1D- and
2D-NMR spectra; completing the course of first year (CH1602, semester 6) with respect to 13C NMR
spectroscopy.
Prerequisite:
Contents: course unit CH1602 (semester 6) Contents:
Mass spectrometry: main ionization techniques (electron impact, chemical ionization, desorption-
ionization, desolvatation-ionization) and analyzer geometries (quadripolar filters, ion trap, orbitrap,
time of flight, magnetic sectors, Fourier transform ion cyclotron resonance) including most recent
hybrid devices.
Chromatography: theoretical and instrumental basis for technique application including recent
developments ; main fundamental values characteristic of a separation ; liquid, gas and supercritical
chromatographies ; optimization of analytical conditions (resolution, analysis length and charge loss) ;
different recent chromatographic systems (nanoflow systems and coupling to mass spectrometry).
NMR: 1H decoupling technique; NOE effects ; 1D-13C APT experiment; 1D-13C DEPT135 experiment;
principle of the 2D-NMR experiment ; the signal in 2D-NMR and its Fourier Transform; principal 2D-
homonuclear (COSY, TOCSY, NOESY) and heteronuclear (HMQC/HSQC, HMBC) correlation experiments
Additional information:
Media: copy of PowerPoint NMR presentations are accessible from the intranet
Bibliographical references: Mass Spectrometry: Principles and Applications. Edmond de Hoffmann and
Vincent Stroobant. Publisher: Wiley-Interscience
Assessment: written 2 hour exam without documents
Remarks:
CI 2Y
MODULE : ORGANIC AND MOLECULAR CHEMISTRY
SUBJECT:
POLYMERS CHEMISTRY
Coordinator:
Pr Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (3) 20 43 48 58
Office 101 Building C1
Compulsory
Code: CI2704
Semester: 7
Lecture: 15 Hours
Directed studies: 8 Hours
Language: French
Coefficient: 3
ECTS: 1.5
Instructor(s):
Patrice WOISEL
Frédéric CAZAUX
Learning outcomes:
The course aims at giving an extensive knwoledge of the molecular design fo synthetic
macromolecules. Aftre the course, the student should be able to :
- draw up a synthetic pathway for the synthetis of different functionalized polymers
- predict the structure, the architecture and the composition of synthetic polymers
Prerequisite:
CH1604
Contents:
-Polyadditions: free radical, anionic and cationic polymerizations-mechanisms, kinetics,
thermodynamics, stereoregularity, average molecular weights and distribution. Living polymerization.
-Free radical copolymerization: kinetics, reactivity ratios, Q-e scheme.
-Step-growth polymerization: linear polycondensation, gels.
Additional information:
Media:
Duplicated lecture note + documents given during the courses
Bibliographical references:
- La polymérisation : Principes et applications
George ODIAN Polytechnica, 1994 ISBN 2840540282
- Chimie et physico-chimie des polymères
Michel FONTANILLE, Yves GNANOU Dunod, 2002 ISBN 2100039822
- Exercices et problèmes de chimie macromoléculaire
Thierry HAMAIDE, Michel BARTHOLIN Editions TEC & DOC, 1999 ISBN 2743003537
Assessment: 1 written exam (1H30)
Remarks:
CI 2Y
MODULE : ORGANIC AND MOLECULAR CHEMISTRY
SUBJECT:
PHYSICO CHEMISTRY OF POLYMERS
Coordinator:
Pr Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (3) 20 43 48 58
Office 101 Building C1
Compulsory
Code : CI2804
Semester : 8
Lecture: 14 Hours
Directed studies:
Language : French
Coefficient : 2
ECTS : 1
Instructor(s):
Patrice WOISEL
Patrice.woisel@ensc-lille.fr
+33 (0)320434954
Build. C6 - office 123
Learning outcomes:
After the course, the student should obtain a broad theoretical knowledge about structure and
properties of polymers and about the methods and techniques that are used to characterize polymers
Prerequisite:
CI2704
Contents:
- Introduction to the physico-chemistry of polymers
- Thermodynamics of polymer solutions and blends : Flory-Huggins theory, predicting polymer solubility
- Determination of molecular weights: osmometry, mass spectrometry, NMR
- Light scattering: principle, experimental method, Zimm plot, MW determination and radius of giration
Additional information:
Media:
Duplicated lecture note + documents given during the courses
Bibliographical references:
Polymers : Chemistry & Physics of Modern Materials, 2nd edition J. M. G. COWIE, Blackie Academic & Professional, Chapman & Hall, 1997, ISBN 075140134X
Initiation à la chimie et à la physico-chimie macromoléculaires Vol.12 : Chimie de l’élaboration du matériau polymère, Collectif, Groupe Français des Polymères, 2001
Introduction to Polymer Science, F. W. BILLMEYER, Wiley, 1984, ISBN 0471031968
Assessment: 1 written exam (1H30)
Remarks:
CI 2Y
MODULE : MATERIALS SCIENCE
SUBJECT :
MAIN CLASSES OF MATERIALS
Coordinator :
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
Compulsory
Code : CI2706
Semester : 7
Lecture: 20 Hours
Directed studies:
Language : French
Coefficient :
ECTS : 1
Instructor(s) :
Nathalie TANCRET
Jean-Bernard VOGT
Patrice WOISEL
Industrial lecturer
Learning outcomes :
Knowledge of main classes of materials – metals, polymers, ceramics, composites- , of their
microstructure, of their physico –chemical characteristics and range of applications
Prerequisite:
Physics and chemistry basis, thermodynamics, bachelor level
Contents :
I- INTRODUCTION
Main properties of materials: thermal, electrical, mechanical, corrosion resistance
Functional materials/ structural materials
II – POLYMERIC MATERIALS
General introduction of polymeric materials, basic polymers, advanced polymers
III – METALLIC ALLOYS
Solidification, crystallography, cast irons and steels, copper and copper alloys, aluminium and Al alloys:
IV – GLASSES AND CERAMICS
From the divided solid to the melted solid, cement, zeolite, ceramic, glass, methods of synthesis,
relation between techniques and energy savings
Additional information:
Media : copies of slides or copies of slide figures
Bibliographical references:
Materials Science and Engineering: an introduction, W.D. Callister, 2000, John Wiley & Sons
Assessment: no exam
Remarks:
CI 2Y
MODULE : MATERIALS SCIENCE
SUBJECT :
MECANICAL ANALYSIS OF MATERIALS
Coordinator :
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
Compulsory
Code : CI2707
Semester : 7
Lecture: 11 Hours
Directed studies:
Language :
French/English
Coefficient :
ECTS : 1
Instructor(s) :
Jean-Bernard VOGT
Learning outcomes :
- The course aims at extending the knowledge towards mechanical aspect of materials. Modern
analytical techniques and testing methods used when assessing materials behaviour such as plasticity
and failure are presented.
After completion of this course, the student should be able to:
I) describe the most important methods and techniques used in materials testing and characterization
II) choose the most appropriate one according to the material and the integrity to emphasize
III) describe the basic aspects of failure feature related to mechanical loading
Prerequisite:
General knowledge in physics, bachelor level
Contents :
I – INTRODUCTION
Stress, strain, types of solicitation
II- MECHANICAL TEST for PLASTICITY CHARACTERIZATION
Tensile test, compression, hardness, creep
III - MECHANICAL TEST for FRACTURE CHARACTERIZATION
Notch effect, impact test, toughness, fatigue
Additional information:
Media: photocopies of slide figures
Bibliographical references:
Des matériaux, J.-P. Baïlon et J.-M. Dorlot Presses Internationales Polytechnique -
Science et génie des matériaux, W.D. Callister Jr, Dunod
Assessment: no exam
Remarks:
Slides are in English
CI 2Y
MODULE : MATERIALS SCIENCE
SUBJECT :
ANALYSIS OF SOLIDS
Coordinator :
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
C7A -office 208
Compulsory
Code: CI2708
Semester: 7
Lecture: 15 Hours
Directed studies:
Language: French
Coefficient: 2
ECTS: 1
Instructor(s) :
Marie COLMONT
Rose-Noëlle VANNIER
rose-noelle.vannier@ensc-
lille.fr
+33(0)3 20 43 65 83
Learning outcomes:
A general knowledge of the main techniques of characterization of solids. In order to be able to face a
given problem.
Prerequisite:
Basics in crystallography abd X-ray diffraction (Lectures CH-1507, CI 1A ) Contents: space groups, Bragg law, diffraction
Contents:
This lecture is an overview of the main techniques used for the characterization of solids: X-ray fluorescence, X-ray diffraction (quantitative analysis, size of crystallite, micro-strain, residual strain, texture), SEM, TEM, XPS, SIMS (XPS and SIMS will be detailed in S9 in the frame of the materials specialty). Large facilities (synchrotron radiation, neutron reactors) will be introduced with a focus on absorption techniques (EXAFS and XANES)… Additional information:
Media: A copy of the necessary media to follow the lecture will be given to the student. The main part
of the lecture is available on the intranet network of the school.
Bibliographical references:
Techniques de l'Ingénieur,
Analyse structurale et chimique des matériaux, J.P. Eberhart, Dunod,
Analyses chimiques, Francis Rouessac et Annick Rouessac, Dunod,
Assessment:
Written exam, 2h
Remarks:
These lectures are completed by case studies, initiation into the treatment of X-ray patterns by the
Rietveld method, a demonstration in X-ray fluorescence X and the visit of the technical platforms in the
CIMAS module.
CI 2Y
MODULE : FORMULATION CHEMISTRY
SUBJECT:
FORMULATION PHYSICAL CHEMISTRY
Coordinator:
Jean-marie.aubry@univ-
lille1.fr
Tél. +33 (0)3 20 33 63 64
Compulsory
Code: CI2709
Semester: 7
Lecture: 15 Hours
Directed studies:
Language: French
Coefficient: 2
ECTS: 1
Instructor(s) :
Jean-Marie Aubry
Learning outcomes:
● Be aware of the nature, the diversity and the specificities of formulation industries
● Discover "performance chemicals" defined by their functional properties but neither by their
chemical structure nor their purity.
● Understand the logic of formulation design complying with predefined specifications.
● Acquire the fundamentals of physical chemistry of surfaces and interfaces.
Prerequisite:
● Basics of organic chemistry, macromolecular chemistry and physical chemistry acquired in first year
● Thermodynamics of ideal solutions
Contents:
INTRODUCTION TO FORMULATION CHEMISTRY: ● Description and specificities of formulation industries: detergent, cosmetics, paint, pharmaceutical… ● Performance chemicals and their functional properties: surfactants, pigments, fragrances, binders ... ● Specifications and usage properties of formulated products. ● Strategy to design formulated products illustrated on the example of a detergent PHYSICAL CHEMISTRY OF SURFACES AND INTERFACES: ● Surface and interfacial tensions: definition and measurement methods. ● Influence of interfacial curvature: capillary pressure and Young-Laplace equation. ● Solvents (risks, selection criteria, Hansen parameters), application du surface degreasing. ● Contact angle, wetting and dewetting of ideal and real surfaces, Zisman method. Additional information:
Media: Duplicated lecture notes with exercises
Bibliographical references:
AUBRY, SCHORSCH, La Formulation : Présentation Générale, Techn. Ingén. (1999) J 2110, 1-20
NARDELLO-RATAJ, HO TAN TAÏ, Les lessives en poudre, Actualité Chim. (mars 2003), 3-10
Assessment: One written exam 1h
Remarks:
CI 2Y
MODULE : FORMULATION CHEMISTRY
SUBJECT :
EXPERIMENTAL DESIGNS
Coordinator :
Jean-Marie Aubry
Jean-Marie.Aubry@univ-
lille1.fr
C6 Building, room 21 or 11
Build. C6 room 21 ou 11
Tél. +33 (0)3 20 33 63 64
Compulsory
Code: CI2813
Semester: 8
Lecture: 16 Hours
Directed studies: 8 Hours
Language: French
Coefficient: 2
ECTS: 1
Instructor(s) :
Christel Pierlot
Christel.pierlot@univ-lille1.fr
Jean-Marie Aubry
Learning outcomes :
After the teaching, the student should be able to
-select the strategy (Screening , Interaction, Optimization, ...) to solve a problem.
-determine the experimental area (factors, levels, number of levels)
-interpret the mathematical model obtained (importance of the coefficients or isoréponses curves)
Prerequisite:
Statistics (mean, standard deviation, normal distribution, Student's coefficients) Matrix algebra (transposed matrix, multiplication) Discussion on the coefficients of mathematical models of degree 1 Contents :
Course, application works, use of experiments design software (Nemrod) Plan of the course :
Study of the influence of many independent factors
Screening matrix
Study of the factors with interactions
Factorial matrix at 2 levels
Factorial fractional matrix
Optimization by the Simplex method
Isoresponses curves
Composite matrix
Doehlert design
Additional information:
Media : Issue paper for course and application exercises
Bibliographical references: Pharmaceutical experimental design, Gareth A. Lewis, Didier Mathieu, Roger
Tan Luu Phan. Marcel Dekker Inc, 1999, New York, Basel
Assessment: Written examination, 2 hours, without documents
Remarks:
CI 2Y
MODULE : FORMULATION CHEMISTRY
SUBJECT:
POLYMER FORMULATION
Coordinator:
Jean-marie.aubry@univ-
lille1.fr
C6 Building, room 21 or 11
Build. C6 room 21 ou 11
Tél. +33 (0)3 20 33 63 64
Compulsory
Code: CI2710
Semester: 7
Lecture: 9 Hours
Directed studies:
Language: French
Coefficient:
ECTS: 1
Instructor(s):
Serge.bourbigot@ensc-lille.fr
/ +33 (0)3.20.43.48.88/
Office N°8
Learning outcomes:
To discover the formulation for polymeric materials and to understand why it is necessary
Prerequisite:
Physics, chemistry and polymer chemistry at the undergraduate level
Contents:
Polymer structure Processing of polymeric materials: thermoplastics, thermosets Fillers and additives: nanocomposite, flame retardants, stabilizers Composites
Additional information:
Media: Powerpoint
Bibliographical references: -
Assessment: -
Remarks:
CI 2Y
MODULE : CHEMICAL ENGINEERING
SUBJECT:
SEPARATION PROCESS
Coordinator:
Nouria.fatah@ensc-lille.fr
+33 (0)320335436
ECLille Building C
Compulsory
Code: CI2715
Semester: 8
Lecture: 8 Hours
Directed studies: 6 Hours
Language: French
Coefficient: 2
ECTS: 1
Instructor(s):
Nouria/Fatah
Learning outcomes:
UNIT OPERATIONS: Separation technology an drying
-Separations "liquid-solid" : particle size, shape and size distribution-Filtration process equipment and
calculations- Filter media- membrane filtration- membrane technology- centrifugation- sedimentation.
-separation "gas-solid" : Cyclone technology, design and calculations
-Drying solids: spray drying and fluidization-design, calculations and industrial applications
-Special care is taken to point out industrial applications and economic impact.
Prerequisite:
Fluids mechanics, heat transfer and thermodynamics Contents:
-Introduction -Filtration Fondamentals - Particle size, shape and size distribution -Fluid Flow through porous media -Membrane filtration -Membrane technology
-Inverse osmosis
-Electrodyalisis
-Sedimentation
-Centrifugation
-Gas cleaning: separation "gas-solid" : Cyclone technology
- Drying solids : spray drying and fluidization
Additional information:
Media: copy of slides presentation
Bibliographical references:
-Procédés de séparation, Techniques, sélection, dimensionnement, J. L.Humphrey et G. E. Keller, Dunod
-Génie Industriel alimentaire tome II, Techniques Séparatives, P. Mafart et E. Béliard, Lavoisier
-Aide mémoire, Génie Chimique, E. Koller, Dunod
Assessment: Lectures: 6 sessions of course, 1h20 duration and 3 sessions of class work, 2h duration.
Written exam 2h, without documents,
Remarks:
CI 2Y
MODULE : CHEMICAL ENGINEERING
SUBJECT:
BINARY AND MULTICOMPONENT DISTILLATION
Coordinator:
Nouria.fatah@ensc-lille.fr
+33 (0)320335436
ECLille Building C
Compulsory
Code: CI2711
Semester: 7
Lecture: 7 Hours
Directed studies:
Language: French
Coefficient: 2
ECTS: 1
Instructor(s):
Marek Czernicki
Fabien Dhainaut
Learning outcomes:
Main objective of this course is to give basic concepts of the binary and multicomponent distillation.
This lecture covers the methods used to calculate the distillation column.
In the second part of this unit, liquid-liquid extraction focus on how to selectively remove a compound
from a liquid phase with a solvent
Prerequisite:
Mass transfer and its application to the unit operations, heat transfer and heat exchangers, applied
thermodynamics.
Mixture rule
Contents:
Topics to be covered include: Principles of distillation, McCabe-Thiele method for binary distillation,
tray efficiency. Vapour Liquid equilibrium relations for non-ideal multicomponent solutions. MESH
equations for rigorous distillation, short-cut methods, distillation column network, extractive and
reactive distillation
Introduction to ternary diagrams, agitated vessels. Combination of agitated vessels and extraction
columns. Multiple alimentation columns. Continuous countercurrent extraction with reflux
Additional information:
Media:
Bibliographical references:
● H.Z. Kister, « Distillation Design », McGraw-Hill, 1992
● H.Z. Kister, « Distillation Operation », McGraw-Hill, 1989
● J.G. Stichlmair, J.R. Fair, « Distillation Principles and Practices », WILEY-VCH, 1998
● Techniques de l’Ingénieur, Génie des Procédés, J1070, J1072, J2623
● Equilibrium-Stage Separation Operations in Chemical Engineering, E.J. HENLEY et J.D. SEADER
(WILEY), 1981
R.E. Treybal, "Mass Transfer Operations", McGraw-Hill, 1981
Assessment:
Written exam 2h, without documents
Remarks:
Student will be able to calculate distillate columns
CI 2Y
MODULE : CHEMICAL ENGINEERING
SUBJECT:
REACTORS
Coordinator:
Nouria.fatah@ensc-lille.fr
+33 (0)320335436
ECLille Building C
Compulsory
Code: CI2816
Semester: 8
Lecture: 7 Hours
Directed studies: 14 Hours
Language: French
Coefficient : 2
ECTS: 1
Instructor(s):
Rafeh BECHARA
Rafeh.bechara@ec-lille.fr
03.20.33.54.44
Learning outcomes :
At the end of this course, students are capable to choose the type of reactors and to identify their
operating conditions.
Prerequisite:
1st year chemical kinetics basic knowledge, and thermodynamics basic knowledge Contents :
Reactors are equipment in which the chemical transformations are performed. The way they work is
very important for all the equipment placed upstream and downstream in an industrial process. The
objectives of the present course are to give the students basic knowledge of different kinds of reactors.
In order to make the reactor design calculation clearer, only homogeneous reactive mixtures are
considered.
After a description of the fundamental aspects needed for reactor calculations, such as mass and heat
transfers, several kinds of reactors are examined in more detail. They are respectively the well-mixed
batch reactor, the continuous stirred tank reactor, the continuous tubular plug flow reactor and the
cascade of tank reactors.
A selection of problems with numerical calculations is proposed to illustrate the importance of the
choice of the reactor for given chemical transformation(s).
Additional information:
Bibliographical references:
J. Villermaux, Génie de la Réaction Chimique, 2nd Ed., Lavoisier Tec&Doc, 1993.
O. Levenspiel, Chemical Reaction Engineering, John Wiley & Sons, 1962.
D. Schweich, Génie de la Réaction Chimique, Lavoisier Tec&Doc, 2001.
J.M. Coulson, J.F. Richardson, Chemical Engineering, Pergamon Press, 1990.
P. Trambouze, Réacteurs chimiques, Techniques de l’Ingénieur, J 4020.
Assessment: Written Examen
Remarks:
CI 2Y
MODULE : CHEMICAL ENGINEERING
SUBJECT:
ASPEN
Coordinator:
Nouria.fatah@ensc-lille.fr
+33 (0)320335436
ECLille Building C
Compulsory
Code: CI2714
Semester: 7
Lecture:
Directed studies: 6 Hours
Language: French
Coefficient: 1
ECTS: 1
Instructor(s):
Marek Czernicki
Learning outcomes:
Student will be able to do typical basic numerical simulation of industrial Unit.
Prerequisite:
Mass transfer and its application to the unit operations, heat transfer and heat exchangers, applied thermodynamics
Contents:
Topics to be covered include basic knowledge of steady-state simulation of distillation column, heat exchangers; use the thermodynamics bank of data
Additional information:
Media:
Bibliographical references:
Documentation of Aspen Plus, www.aspentech.com
Assessment:
Students are evaluated during Laboratory classes of Chemical engineering.)
Remarks:
CI 2Y
MODULE 1 : MATERIALS SCIENCE
SUBJECT:
CORROSION
Coordinator:
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
Semi-optional
Code: OP2801-1
Semester: 8
Lecture: 16 Hours
Directed studies:
Language: French
Coefficient: 2
ECTS: 1
Instructor(s):
Ingrid PRORIOL-SERRE,
Ingrid.serre@univ-lille1.fr
+ Industrial lecturer
Learning outcomes:
The objective of the course is to present the origin and mechanism of corrosion degradation.
After completion of this course, the student should be able to: i) identify the type of corrosion
degradation - ii) propose an experimental procedure for corrosion resistance characterization
iii) select a material resistant against corrosion or a method for corrosion protection
Prerequisite:
Electochemistry, metallurgy, materials science knowledge : bachelor and first year master Contents:
Introduction: definition of corrosion – impacts of corrosion in industry
● Electrochemical aspects and types of corrosion : electrochemical reactions, Ellingham diagram, dry
corrosion, aqueous corrosion (Nernst law, Pourbaix diagram, electrochemical kinetic, Bulter-Volmer
equation, Tafel extrapolation method, corrosion potential, potential / current density curves), factors
influencing corrosion phenomena, types of corrosion
● General corrosion: atmospheric corrosion, uniform aqueous corrosion, passive materials
● Localized corrosion: galvanic corrosion, pitting corrosion, crevice corrosion, intergranular corrosion,
erosion corrosion and cavitation corrosion
● Corrosion at elevated temperature
● Corrosion prevention: materials selection, structures design, layer protection (coatings, paints,
surface treatments), use of corrosion inhibitors, electrochemical protection (sacrificial anode,
impressed current protection), service corrosion tests
Additional information:
Media: photocopies of slide figures
Bibliographical references: Corrosion et chimie de surface des métaux, D. Landolt, Traité des Matériaux,
Volume 12, Presses polytechniques et universitaires Romandes
Corrosion des matériaux à haute température, G. Béranger, JC. Colson, F. Dabosi, Editions de Physique
Corrosion et anticorrosion, G. Béranger, H. Mazille, Mécanique et Ingénerie des matériaux, Hermes,
Précis de corrosion, J-J. Lanoureux, Sciences des matériaux, MASSON
Corrosion Engineering Handbook, Edited by Philip A. Schweitzer, P. E., Marcel Dekker, Inc.
Principles and prevention of corrosion, Denny A. Jones, printed by Quinn-Woodbine, 1991
Assessment: single written test
Remarks:
CI 2Y
MODULE 1 : MATERIALS SCIENCE
SUBJECT:
CATALYTIC MATERIALS
Coordinator:
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
Semi-optional
Code: OP2801-2
Semester: 8
Lecture: 15 Hours
Directed studies:
Language: French
Coefficient: 2
ECTS: 1
Instructor(s):
Anne-Sophie MAMEDE
anne-sophie.mamede@ensc-
lille.fr
+33 (0)3 20 33 70 90
Bureau 106
Bâtiment C3
Learning outcomes:
The course is designed so that engineering students can acquire and use the concepts of
heterogeneous catalysis. This course aims to define the phenomena that occur at the surface of a solid
and that regulate the catalytic act. It also presents the main characterization tools to determine the
textural and physico-chemical properties of catalytic materials. Finally, industrial applications of the
three classes of catalysts (metal, oxide, and acid-base) are presented.
Prerequisite:
Knowledge acquired in the kinetics module in CI 1Y - CH1609
Basic knowledge gained in CI 1Y and in preparatory classes (CPGE, CPI, L2, DUT, BTS, ATS…)
Contents:
The course is divided into six chapters:
- Introduction and Overview: Definitions, Chemical equilibrium, Action mode of a catalyst
- Adsorption - Application to the measurement of the solid surface: Physisorption, Adsorption
isotherms (Langmuir, BET method), Chemisorption, Chemisorption isotherms (Langmuir, Temkin,
Freundlich), Application to surface characterization of metal catalysts
- Textural characterization of catalysts: Surface Area, Distribution of pore size, Porosimetry,
Characterization of the active phase by temperature programmed measurements
- Physical Kinetics - Transfers of heat and mass: Overview, Diffusion of reactants and products, Extra-
and intra granular diffusions
- Metal Catalysts: Preparation and design, Industrial applications (Fischer-Tropsch reaction, automotive
depollution, desulfurization ...)
- Acid-Base Catalysts: Acid solids, Zeolites
Additional information:
Media: Class manual including exercises
Bibliographical references:
Cinétique et catalyse, G. Scacchi, M. Bouchy, J.-F. Foucaut, O. Zahraa, R. Fournet, Editions Tec&Doc,
Lavoisiser, 2011
Cinétique et catalyse hétérogène, B. Gilot, R. Guiraud, Technosup, Ellipses, 2004
Chimie des surfaces et catalyse, G.A. Somorjai, M.-P. Delplancke, Ediscience International, 1995
Assessment: Written evaluation of 1h30
Remarks:
CI 2Y
MODULE 1 : MATERIALS SCIENCE
SUBJECT:
METALLURGY
Coordinator:
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
Semi-optional
Code: OP2801-3
Semester: 8
Lecture: 15 Hours
Directed studies:
Language: French /English
Coefficient: 2
ECTS: 1
Instructor(s):
Charlotte Becquart
Charlotte.becquart@ensc-
lille.fr, Bât C6. Bureau 217
Tel 03 20 43 49 44
Learning outcomes:
A good understanding of phase diagrams, specially the steel and cast iron phase diagrams. Good
knowledge of the different kinds of defects in metallic materials. Good knowledge of solidifications and
solid state phase transitions.
Prerequisite:
Applied Thermodynamics S5
Cristal structure S5
Contents:
Solidification;I Experimental study of solidification : determination et interpretation of the phase
diagrams
Defects; I Point defects: vacancies, self-interstitials, substitutional atoms, hetero-interstitials. ; II 1D :
dislocations ; III 2D : twins, grain boundaries ; IV 3D : precipitates
The FeC diagram;I Steels; II Norms; III Steels heat treatments; IV Cast Irons
Phase transformations;I Thermodynamics behind solidification diagrams; II Kinetics of phase
transformation in metals and metallic alloys in the solid state. ; III Precipitation in metal solid solutions;
IV The martensitic transformation V The bainitic transformation
Solidification in real conditions
Additional information:
Media: copy of the slides.
Bibliographical references: 1/ « Précis de métallurgie », Jean Barralis et Gérard Maeder, Edition Nathan,
2005. 2/ « Des matériaux », Jean-Paul Baïlon et Jean-Marie Dorlot, Presses internationales
polytechnique, Ecole polytechnique de Montréal, 2000. 3/« Métallurgie : du minerai au matériau »,
Jean Philibert, Alain Vignes, Yves Bréchet et Pierre Combrade, Edition Dunod, 2002 4/ « Aide mémoire
de l’ingénieur, métallurgie. Alliages. Propriétés», Guy Murry, Dunod, Paris 2004 5/« Phase
transformations in metals and alloys », David A. Porter and K.E. Easterling, Van No strand Reinhold (UK)
Co. Ltd 1981 6/« Binary alloy phase diagrams » T.B. Massalski, ASTM publishers, 1990
Assessment: 2 h written exam
Remarks:
CI 2Y
MODULE 1 : MATERIALS SCIENCE
SUBJECT:
PHYSICS OF POLYMERIC MATERIALS
Coordinator:
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
Semi-optional
Code: OP2801-5
Semester: 8
Lecture: 12 Hours
Directed studies:
Language: French/ English
Coefficient: 2
ECTS: 1
Instructor(s) :
Serge Bourbigot
Serge.bourbigot@ensc-lille.fr
03.20.43.48.88
Bureau N°8
Learning outcomes:
To learn the basics of the physics of polymeric materials
Prerequisite:
Physics, chemistry and polymer chemistry at the undergraduate level
Contents:
Part 1: structure and dynamics Polymer structure Molecular dynamic Semi-crystalline polymer Part 2: Mechanics of polymeric materials Thermomechanical analysis Creep, recovery and relaxation Time/temperature scanning: transitions in polymer Time/temperature scanning: thermosets Frequency scanning
Additional information:
Media: Powerpoint
Bibliographical references: De la macromolécule au matériau polymère by JL Halary et F Lauprêtre
Assessment: written exam
Remarks:
CI 2Y
MODULE 1 : MATERIALS SCIENCE
SUBJECT:
PLASTICITY RUPTURE
Coordinator:
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
Semi-optional
Code: OP2801-6
Semester: 8
Lecture: 16 Hours
Directed studies:
Language: French/English
Coefficient: 2
ECTS: 1
Instructor(s):
Jean-Bernard VOGT
Learning outcomes:
The course deals with the mechanisms of plastic deformation of metals and metallic alloys and are
explained with the dislocation theory. The applications of plasticity are described through numerous
examples related to forming technology and to fracture mechanisms
Prerequisite:
Mechanical properties of materials - crystallography, bachelor level
Contents:
I ELASTICITY
Stress-strain relations, physical origin
II PLASTICITY (cf.dislocations)
Physical origin - concept of dislocations - Schmid Boas law - plastic behaviour - twinning
III HARDENING
Solid solution, cold working, grain refinement, precipitation
IV RUPTURE
Brittle fracture, ductile fracture, fatigue failure
V. FORMING
Processes, drawing, lubrication
Additional information:
Media: photocopies of slide figures
Bibliographical references:
Engineering materials, an introduction to their properties and applications, M.A. Ashby and D.R.H.
Jones, materials Science and technology, Vol.34, Pergamon press (1982) -
Mechanical behaviour of materials, T.H. Courtney, Mc Graw Hill Publishing Company (1990)
Assessment: single written exam, 1h
Remarks:
Slides are in English and the teacher is ready to switch to English language if necessary
CI 2Y
MODULE 1 : MATERIALS SCIENCE
SUBJECT:
GLASSES CERAMICS
Coordinator:
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
Semi-optional
Code: OP2801-7
Semester: 8
Lecture: 19 Hours
Directed studies:
Language: French
Coefficient: 2
ECTS: 2
Instructor(s):
Nathalie TANCRET
Learning outcomes:
Know the different families of ceramics (traditional, technical, cement) and glasses chemically and
structurally (crystallized, amorphous) and the related physical properties (magnetism,
superconductivity, ...)
Know the methods of manufacture in the laboratory and in industry, and know how to choose the best
method of manufacture according to specifications: energy saving, desired purity of the material, form
and use of the final material ...
Prerequisite:
Basics of inorganic chemistry
S7 course "introduction to materials," glasses and ceramics part
Notions of crystallography
Contents:
The aim of this course is to deepen the concepts covered in the course "Introduction to Materials" (S7)
of the great families of ceramics and glass. In particular, we will consider the following materials:
traditional and technical ceramics, cements, glasses and zeolites. Part will be devoted to various
methods of manufacturing that directly affect the nature of the material and, therefore, on its
properties. We will see manufacturing methods most commonly used in industry and we will discuss
the importance of techniques for energy savings.
Finally, special attention will be given to applications of these materials on an industrial scale and in the
daily lives of us all.
Although not all aspects can be considered in this course, the most important points will be developed
to give students good basics in solid state matter. This knowledge can be further explored in the third
year in the option "optimization and reliability of materials" or further studies (Master).
Additional information:
Media: lecture notes given by instructor
Bibliographical references: Solid State Chemistry : An Introduction, second edition, Lesley SMART and
Eliane MOORE, published by Chapman et Hall (UK - 1995).
Chimie Industrielle, Robert PERRIN et Jean-Pierre SCHARFF, 2ème édition, Masson (Paris - 1997).
Matériaux 2 : Microstructure et Mise en Œuvre, Michael ASHBY et David Rayner Hunkin JONES,
translated from English by Yves BRECHET, Joël COURBON et Michel DUPREUX, Editions Dunod (Paris -
1991).
Assessment: one written test, 1.5 h, at the end of the semester, with documents.
The aim is to transpose this knowledge seen during the course to real cases studies.
Remarks:
CI 2Y
MODULE 2 : MOLECULES
SUBJECT:
NATURAL MOLECULES
Coordinator :
Professeur Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (0)3 20 43 48 58
Office 101 Building C1
Semi-optional
Code: OP2802-6
Semester: 8
Lecture: 12 Hours
Directed studies:
Language: French/English
Coefficient: 2
ECTS: 1
Instructor(s):
Philippe Cotelle
Learning outcomes:
Have a vision of set on the chemistry of natural substances, their biosynthesis (steroids and terpenes),
of their total synthesis (some examples) and their biological, physiological properties
Prerequisite:
Basis in organic chemistry, semesters S5 & S6, CH1503 and CH1603 and semester S7, CH2703
Contents:
General introduction on secondary metabolites
Steroids (Cholesterol, vitamin D3, Sexual and adrenocortical hormones, Diosgenin (an important raw
material from plants)
Terpenoids (Sesquiterpenes, Monoterpenes, Sesquerterpenes, Diterpenes, Carotenes and A, E and K
vitamins)
Lipids and eicosanoids (true lipids (esters of fatty acids and alcohols (glycerol, fatty alcohols, sterols),
glycerolipids, waxes), complex lipids (Glycerophospholipids), eicosanoids (Prostaglandins, Leucotrienes)
Alkaloids (papaverine, morphine, quinine, lysergic acid, colchicine)
Polyphenols (Phenylpropanoids, catecholamines and derivatives, lignans, flavanoids, tannins)
Natural dyes and pigments
Additional information:
Media: powerpoint
Bibliographical references: S .V. Bhat, B.A. Nagasampagi, M. Sivakumar, Chemistry of natural products,
Springer, 2005, ISBN 3-540-40669-7
K. C. Nicolaou, T. Montagnon, Molecules that changed the world, Wiley-VCH, 2008, ISBN 978-3-527-
30983-2
Assessment: Written exam (1 hour)
Remarks:
CI 2Y
MODULE 2 : MOLECULES
SUBJECT:
FORMULATION OF SURFRACTANTS AND DISPERSED SYSTEMS
Coordinator:
Professeur Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (0)3 20 43 48 58
Office 101 Building C1
Semi-optional
Code: OP2802-4
Semester: 8
Lecture: 15 Hours
Directed studies:
Language: French
Coefficient: 2
ECTS: 1
Instructor(s):
Prof. Jean-Marie Aubry
Jean-marie.aubry@univ-
lille1.fr
Tél. +33 (0)3 20 33 63 64
Learning outcomes:
Know the major classes of surfactants and their main physicochemical and functional properties
Know the traditional and modern scales for the classification of surfactants based on their
amphiphilicity.
Discover the principles of formulation of emulsions and microemulsions
Prerequisite:
Basics of organic chemistry, macromolecular chemistry and physical chemistry acquired in first year
Concepts acquired in the introductory course in the formulation chemistry course of the second year
Contents:
Surfactants: Définition, main classes and synthesis Physical chemistry of aqueous solutions of surfactant (CMC, Gibbs' equation, liquid crystals, packing parameter, cloud point, Krafft temperature) Functional properties (wetting, dispersing, emulsifying, foaming, detergency, antistatic, antifoaming). Introduction to the formulation of emulsions and microemulsions. Additional information:
Media: Duplicated lecture notes with exercises
Bibliographical references:
Assessment: One written exam 1:30h
Remarks:
CI 2Y
MODULE 2 : MOLECULES
SUBJECT:
FUNCTIONAL POLYMERS
Coordinator:
Professeur Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (0)3 20 43 48 58
Office 101 Building C1
Semi-optional
Code: OP2802-1
Semester: 8
Lecture: 20 Hours
Directed studies:
Language: French/English
Coefficient: 2
ECTS: 1
Instructor(s):
Patrice WOISEL
Patrice.woisel@ensc-lille.fr
0320434954
Bât. C6 p. 123
Learning outcomes:
This course will overview various synthetic methods for making well-defined polymers. This course also
discusses about the applications of well-defined polymer systems as smart drug delivery materials.
After attending this course, students should be able to:
- distinguish between principle radical polymerization techniques allowing the elaboration of well-
defined polymer molecules and describe the characteristic features of each..
- unterstand the role of polymer structure and intermolecular interactions in determining the
properties of assemblies.
- distinguish the different stimuli capable of altering polymer properties
Prerequisite:
Modules CH1604/CI2704/CH1503
Other:
Contents:
- The general concepts about the preparation of well-defined polymers - Different Controlled Radical Polymerization( CRP) techniques - Elaboration and self-assembly of amphiphilic diblock copolymers - Main types of stimuli for stimulus-responsive polymers/ Applications of stimuli responsive polymers
Additional information:
Media: Duplicated lecture note of practical class + Publications given during the courses
Bibliographical references:
- Controlled/Living Radical Polymerization : Progress in ATRP
Krysztof MAtyjaszewski ACS Division of Polymer Chemsitry ISBN 9780841269958
Assessment:
One written exam (2H)
Remarks:
CI 2Y
MODULE 2 : MOLECULES
SUBJECT:
HOMOGENEOUS CATALYSIS
Coordinator:
Professeur Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (0)3 20 43 48 58
Office 101 Building C1
Semi-optional
Code: OP2802-3
Semester: 8
Lecture: 15 Hours
Directed studies:
Language: French/English
Coefficient: 2
ECTS: 1
Instructor(s):
Francine Agbossou-
Niedercorn
francine.agbossou@ensc-
lille.fr
03 20 43 49 27
Bureau 108
Learning outcomes:
Catalysis is the central issue of many chemical processes which can be examined on an academic level,
but which also take place in living systems or in large scale industrial rectors. This teaching aims (1) at
providing students the understanding of the science lying behind the important industrial applications
of homogeneous catalysis, especially for the manufacture of both commodity and fine chemicals (2)
give the future chemists a global vision of the elementary steps of organometallic chemistry and of the
catalytic cycles (3) provide kinetic and selectivity data as well as plant schemes. The most important
industrial applications of homogeneous catalysis will be covered i.e. carbonylations, hydroformylations,
polymerizations, oligomerizations, metathesis, hydrocyanation, oxidations, fine chemistry (C-C
coupling, hydrogenation, isomerization).
Prerequisite:
A good knowledge of organic chemistry, some training in organometallic chemistry will be welcome.
Contents:
Chap. 1: Sustainable chemistry, introduction to catalysis - Chap. 2: Introduction to homogeneous
catalysis, rôle of the catalyst and of the catalytic cycle - Chap. 3: Introduction to the transition metal
chemistry, reactivity of the complexes and to the elementary steps of organometallic chemistry - Chap.
4: Carbonylation: acetic acid and acetic anhydride synthesis, alkynes carbonylation, other
carbonylations - Chap. 5: Hydroformylation: OXO synthesis, biphasic hydroformylation, other
hydroformylation processes - Chap. 6: Oxidation: Wacker process, other industrial oxidation processes
- Chap. 7: Oligomerization: SHOP process, Dimersol, Difasol, other oligomérization processes - Chap. 8 :
Metathesis - Chap. 9: Polymerization: Ziegler Natta catalysis, homogeneous polymerization processes-
Chap. 10: Fine chemistry: isomerization, C-C coupling - Chap. 11: butadiene Hydrocyanation,
adiponitrile synthesis - Chap. 12: Hydrosilylation - Chap. 13: Hydrogenation and asymmetric
hydrogenation.
Additional information:
Media: handouts containing the slides of the course
Bibliographical references: a) Applied Homogeneous Catalysis with Organometallic Compounds B.
Cornils, W. A. Herrmann, Second Ed. Wiley-VCH, 2002 - b) Catalysis : concepts and green applications,
G. Rothenberg, Wiley-VCH, 2008 - c) Homogeneous catalysis, understanding the art, P.W.N.M. van
Leeuwen, Kluwer Academic Publishers, 2004
Assessment: 1h30, end of the course, annual
The final assessment relies on the content of the course without document neither calculator. The
students should have a very good knowledge of the basics of organometallic chemistry, the catalytic
cycles, and the important industrial applications of homogeneous catalytic processes. Specific trends of
the industrial processes have to be known. The general level of understanding of the kinetic and
selectivity of the processes will be evaluated through comparison of the processes, the catalytic
cycles…
Remarks:
CI 2Y
MODULE 2 : MOLECULES
SUBJECT:
MOLECULAR CHEMISTRY AND FORMULATION
Coordinator:
Professeur Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (0)3 20 43 48 58
Office 101 Building C1
Semi-optional
Code: OP2802-7
Semester: 8
Practical studies: 20 Hours
Project:
Language: French
Coefficient: 3
ECTS: 2
Instructor(s):
Christel PIERLOT
Christel.Pierlot@ensc-lille.fr
Valérie MOLINIER
Valerie.Molinier@ensc-lille.fr
Patrick DAUBIAS, Ingénieur
Maxence VANDEWALLE,
Technicien
Doctorants moniteurs
Learning outcomes:
Illustration of the notions of colloidal chemistry presented during the lessons (superficial tension,
surface agents, rheological agents)
Implementation of conductimetric measurements to determine the critical micellar concentration of
surfactants and the phase inversion temperature of an emulsion
Synthesis of functional compounds (dyeing agents, cosmetic oil). Implementation of an enzymatic
catalysis illustrating the principles of green chemistry
Setting up of an experimental design to optimize the dyeing of fibers
Prerequisite:
Physico-chemistry of formulation (S7), experimental design (S8), formulation of surfactants and
dispersed systems (S8)
Organic and macromolecular chemistry (S5, S6, S7)
Contents:
TP1: Synthesis of dyeing agents for textile
TP2: Enzymatic synthesis of a cosmetic oil: Isopropylmyristate
TP3: Determination of surfactants' CMC by conductivity and UV spectrophotometry
TP4: Superficial tension and rheological agents
Additional information:
Media: practical booklet
Bibliographical references: -
Assessment: notation of the reports written for each practical
Remarks:
CI 2Y
MODULE 2 : MOLECULES
SUBJECT:
ORGANOMETALLIC CHEMISTRY
Coordinator:
Professeur Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (0)3 20 43 48 58
Office 101 Building C1
Semi-optional
Code: OP2802-5
Semester: 8
Lecture: 12 Hours
Directed studies:
Language: French
Coefficient: 2
ECTS: 1
Instructor(s):
Pr PELINSKI Lydie
Lydie.pelinski@ensc-lille.fr
+33 (0) 3 20 43 65 01
ENSCL, Bureau 106
Learning outcomes:
The objective of this course is to get the student the development of organometallic chemistry as a tool
in organic synthesis, especially in drug synthesis. Examples of industrial development should make it
possible to the students to better understand the importance of metals during synthesis steps
Prerequisite:
Bases acquired in organic chemistry in 1st year.
Contents:
Organometallic synthesis and applications in fine chemistry: organometallics as electrophiles and as
nucleophiles.
Synthetic applications of transition metal carbene complexes: introduction, Fischer and Schrock
carbène complexes, Dötz reaction.
Palladium catalysed reactions in organic synthesis: introduction, Heck, Sonogashira, Stille, Suzuki
réactions, …
Chemistry of lanthanides, gold and Zirconium in organic synthesis
Bioorganometallic chemistry: metalloenzymes, bioanalysis, organometallics and therapy.
Additional information:
Media:
Chimie organométallique, Didier Astruc, Ed EDP Sciences.
Chimie organique : Hétéroéléments, stratégies de synthèse et chimie organométallique, Nicolas
Rabasso, Ed. De Boeck.
Les complexes de palladium en synthèse organique, Jean-Marc Campagne et Damien Prim, CNRS
Editions.
Bibliographical references:
Assessment: written tests, 1h30.
Remarks:
CI 2Y
MODULE 2 : MOLECULES
SUBJECT:
STRUCTURE AND FUNCTIONALITY OF BIOMOLECULES
Coordinator:
Professeur Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
+33 (0)3 20 43 48 58
Office 101 Building C1
Semi-optional
Code: OP2802-2
Semester: 8
Lecture: 20 Hours
Directed studies:
Language: French/English
Coefficient: 2
ECTS: 1
Instructor(s):
Vangelis Agouridas
Learning outcomes:
Aminoacids, Protein Structure, Knowledge of tools related to enzymatic catalysis as well as industrial
applications
Prerequisite:
Advanced Organic Chemistry (Sem. 7), Kinetics and Thermodynamics (notions)
Contents:
0. General introduction 1. From aminoacids to functional proteins: enzymes (aminoacids, protein structure, enzymes and coenzymes) 2. Theory of enzymatic activity (Enzymatic catalysis through history, a molecular approach to enzymatic catalysis) 3. Kinetics, Influence of physicochemical effectors (Henri-Michaelis-Menten, influence of pH, T°, ionic strenght) 4. Enzymatic catalysis: different types of transformations (study of hydrolytic reactions, oxidoreductases and application for fine chemicals and industrial processes) Additional information:
Media:
Lecture notes
Bibliographical references:
The organic chemistry of drug design and drug action, R. B. Silverman, 1992, Academic Press, Inc, ISBN
0-12-643730-0
Biocatalysis, A.S. Bommarius & B. R. Riebel, 2004, Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim ISBN
3-527-30344-8
Biotransformations in Organic Chemistry 6th edition, K. Faber, 2011, Springer-Verlag Berlin Heidelberg,
ISBN 978-3-642-17392-9
Assessment:
1h written exam
Remarks:
CI 2Y
MODULE : DESIGN AND SYNTHESIS OF MATERIALS AND COMPOUNDS WITH DEFINED PROPERTIES
SUBJECT:
DESIGN AND SYNTHESIS OF MATERIALS AND COMPOUNDS WITH DEFINED PROPERTIES
Coordinator :
Catherine Renard
Catherine.renard@ensc-lille.fr
+33 (0)3 20 43 44 34
BLDG C7A, office 226
Compulsory
Code: TP2703
Semester: 7
Practical studies: 56 Hours
Project: 20 Hours
Language: French
Coefficient: 10
ECTS: 8
Instructor(s) :
Vangelis Agouridas
Marie Colmont
Gaëlle Fontaine
Valérie Molinier
Catherine Renard
Murielle Rivenet
Nathalie Tancret
Personnel technique :
Catherine Candelier
Patrick Daubias
Maxence Vandewalle
Learning outcomes:
Manage a project from planning to implementation :
- Conduct a bibliographic survey on a given subject,
- Select, prepare, organize and conduct experiments,
- Prepare a written report including a bibliographic review and a report of the experiments conducted,
- Present their work as an oral presentation.
Prerequisite:
Contents: Introduction to bibliographic research and writing a report - theoretical and practical
knowledge of conventional chemical characterization techniques.
Contents:
The projects are designed as mini-research projects. The goal is to lead students to gain more
autonomy in the preparation, selection, organization and carrying out manipulations. If the subject
lends itself to it, students are encouraged to contact industrial or academic experts in the field.
Projects start with a bibliographic review, after which students must develop their own project. This
first step allows a thorough introduction to bibliographic research methods. Students then determine
the most appropriate synthesis routes and analysis for the subject. They are encouraged to use the
division of instrumentation available at ENSCL and expand their investigation to characterization
techniques available in the research laboratories of the USTL. After this period, the students have 56
hours, blocked for a week and a half, to implement their project.
Topics are updated every year and have an industrial and / or fundamental interest.
Additional information:
Assessment:
Report (bibliographic and practical) - oral presentation - investment in the project.
Remarks:
CI 2Y
MODULE : INDUSTRIAL CHEMISTRY/ANALYSIS METHODS AND SECURITY
SUBJECT:
INDUSTRIAL CHEMISTRY:ANALYSIS METHODS AND SECURITY (CIMAS)
Coordinator:
Eric BUISINE
eric.buisine@ensc-lille.fr
/ +33 (0)3 20 33 77 48 / ENSCL
- C7B
Compulsory
Code : TP2701
Semester : 7
Practical studies: 32 Hours
Project:
Language : French
Coefficient : 6
ECTS : 3
Instructor(s):
Serge BOURBIGOT
Rose-Noëlle VANNIER
Patrice WOISEL
Jérémie BOUQUEREL
Ludovic THUINET
Eric BUISINE
Assistant-engineer:
Patrick DAUBIAS
Learning outcomes:
Acquiring practical knowledge of analytical techniques frequently used in industry: NMR , X-ray
diffraction, X-ray fluorescence, chromatography gas and liquid (HPLC) , gas chromatography–mass
spectrometry (GC-MS), scanning electron spectroscopy (SED). Quantitative, qualitative aspects and
limits of each technique are underlined. With these practicals, students have also the opportunity to be
sensitized to safety problems and the means deployed in industry (thermal control of chemical
reactions, resistance to fire and to heat of materials).
Prerequisite:
Program: course units CH1502 (semester 5), CH1602 (semester 6), CI2702 and CI2708 (semester 7)
Contents:
Analysis techniques:
- 1D and 2D dimensional Nuclear Magnetic Resonance (NMR) spectroscopy ; X-ray fluorescence ; X-ray
diffraction ; chromatography gas and liquid (HPLC) ; gas chromatography–mass spectrometry (GC-MS) ;
mechanical characterization of materials: hardness test, monotonic tensile test ; scanning electron
spectroscopy (SED)
Safety:
Evaluation of the fire-resistance for an intumescent coating ; calorimetry for safety evaluation of
chemical reactions
Additional information:
Media: paper documentation
Bibliographical references: given in the documentation
Assessment: participation during the practicals ; level of knowledge ; no result report
Remarks:
Working by group of four students
CI 2Y
MODULE : POLYMER CHEMISTRY
SUBJECT:
POLYMER CHEMISTRY
Coordinator:
Frederic.cazaux@ensc-lille.fr
+33 (0)3 20 43 43 40
Build. C6 -office 120
Compulsory
Code: TP2806
Semester: 8
Practical studies: 25 Hours
Project:
Language: French
Coefficient: 6
ECTS: 3
Instructor(s):
Frédéric CAZAUX
Fabienne Samyn
Learning outcomes:
To put into practice knowledge acquired in courses and directed studies upon various synthesis
methods, as molecular weights determination and kinetics parameters during a polymerization
reaction.
Prerequisite:
Modules CH1604 et CI2704 Contents:
5 practicals by student:
- Synthesis of a styrene / methyl methacrylate copolymer
- Production of a plate of poly(methyl methacrylate) by a thermal or a photochemical process
- Synthesis of a polyamide-6,6, a polyurethane, and a phenolic thermoset
- Curing of a stratified composite material
- Suspension and emulsion polymerization of styrene - Mass distribution characterization by Gel
Permeation Chromatography analysis (GPC)
- Kinetics of free radical bulk polymerization of styrene by dilatometry
- Kinetics of polycondensation of amino-11 undecanoic acid
Additional information:
Media: Duplicated lecture note of practical class + documents given during the sessions
Bibliographical references:
- La polymérisation : Principes et applications
George ODIAN Polytechnica, 1994 ISBN 2840540282
- Chimie et physico-chimie des polymères
Michel FONTANILLE, Yves GNANOU Dunod, 2002 ISBN 2100039822
- Exercices et problèmes de chimie macromoléculaire
Thierry HAMAIDE, Michel BARTHOLIN Editions TEC & DOC, 1999 ISBN 2743003537
Assessment:
A report by practical, among which 3 with an oral evaluation on a part.
Remarks:
CI 2Y
MODULE : CHEMICAL ENGINEERING (Practical studies)
SUBJECT:
CHEMICAL ENGINEERING
Coordinator:
Nouria.fatah@ec-lille.fr
+33(0)320335436
Build.
Obligatoire
Code: TP2805
Semester: 8
Practical studies: 15 Hours
Project:
Language: French
Coefficient: 3
ECTS: 2
Instructor(s):
R. BECHARA, M. CZERNICKI, F.
DHAINAUT and N. FATAH
Learning outcomes:
Practical work of Chemical engineering gathers theory, practical program and simulation. They try to carry out a harmonization accentuated between the basic disciplines of chemistry and those of Chemical engineering and target three objectives: - to supplement the course of the teaching of Chemical engineering. - to confront the students with pilots of semi-industrial scale during a sufficient working time in order to obtain results of good quality and into practice to put the theoretical teaching exempted at the time of the courses and directed work. The unit operations of Chemical engineering implemented are: - Distillation and simulation by software ASPEN, - Absorption on columns, - Evaporator - Reactors
Prerequisite:
Notions of heat transfer, Thermodynamics of equilibrium between phases, Notions of elements of chemical reaction engineering.
Contents:
Manipulations are the following :
Absorption in a packed column
Distillation in a packed column and simulation (Aspen)
Evaporator “type Kestner,
Reactors: comparison between batch reactor, mixed flow reactor and plug flow reactor
Additional information:
Media:
Teachers documents
Bibliographical references: Courses of chemical engineering P. Wuithier : Raffinage et Génie Chimique, ed. Technip Perry : Chemical Engineers Handbook, Mc Graw Hill Mc Cabe & Smith : Unit Operations of Chemical Engineering, Mc Graw Hill
Assessment:
Written report
Remarks:
CI 2Y
MODULE : THE COMPANY
SUBJECT:
MANAGEMENT
Coordinator:
Robert VAZILLE
Compulsory
Code: FE2808
Semester: 8
Lecture: 16 Hours
Directed studies:
Language: French
Coefficient: 2
ECTS: 1
Instructor(s):
Robert VAZILLE
vazille.robert@wanadoo.fr
06 8498 3505)
Learning outcomes:
The objective is to facilitate the integration of the students and to enhance their success within the
organisation at the beginning of their professional carreer.
Prerequisite:
No prerequisite.
Contents:
SESSION 1:
Overall survey of the different styles of management through different case studies.
SESSION 2:
Quality – ISO 9001 – Processus – EFQM
SESSION 3:
Knowledge Management – Transformer of information – Key concepts – Explicit and tacit knowledge –
KM for individual application – KM within a team
SESSION 4:
Crisis Management, - conflicts - acquisition
Additional information:
Bibliographical references:
Peter Senge - la Vème discipline /Michael Porter - Competitive Advantage - Competitive Edge of
Nations/Patrick Lagadec - Le Management des Crises/Elihayu Goldratt - La théorie des contraintes - Le
but/Daniel Goleman - L'intelligence émotionnelle/Covey Stephen - The 7 habits of highly effective
people/ Gordon - Cadres efficaces/ Jack Welch - Jack/Carlos Ghosn - Turn round/Byham William -
Zapp/Michel Hammer - le re-engineering/Tom Peter - Liberation Management/Michael Tracy -
L'exigence du choix/Ouakin Mark Alain - Lire aux éclats/Walter Isaacson - Steve Jobs.
Assessment:
This is done through a short report made by the students at the end of each session, They have the task
to show their understanding of the key concepts.
Remarks:
CI 2Y
MODULE : THE COMPANY
SUBJECT :
LAW
Coordinator :
Philippe BRELIVET Avocat
Compulsory
Code : FE2809
Semester : 8
Lecture: 12 Hours
Directed studies:
Language : French
Coefficient : 2
ECTS : 1
Instructor(s) :
Philippe BRELIVET Avocat
Learning outcomes :
This law lecture aims to help students to know and to understand the international and national legal
system. As a result of this lecture, students will be able to understand fundamental legal system in a
great number of fields as for instance : International Law, European Union Law, Civil Law, Business Law,
Intellectual and Industrial Property Law, Criminal Law.
Prerequisite:
No prerequisite is asked to attend this law lecture.
Contents :
I – Public Law
1° International Law
United Nations Organisation: General Assembly, Security Council, setting up and function.
World Trade Organisation: General Assembly, Settlement Dispute Organisation, international
regulation of trade.
2° European Union (EU) Law
EU Treaty, EU commission, EU council, EU parliament, EU court of justice. EU Law (directives,
regulations, decisions).
3° The 4th october 1958 French fifth Republic Constitution
The President of the Republic, the Government, the Parliament, election, setting up, function,
executive branch power, government branch power, legislative branch power.
II – Private Law
1° Property law
Different goods and rights classification
2° Estate interest rights
Property system, intellectual and industrial property law, patents, brands, drawings and patterns
copyrightable designs, action for infrigement.
3° Contract law
Typology of various contracts, commercial sale contract, regulation of the e-business.
4° Competition and consumption law
Illicit and unfair competition law, consumption law, sale regulation for consumers and professionals.
5° Criminal law and business criminal law
9Penal offenses, different steps of a criminal trial, corporate asset abuse.
Additional information:
Media :
Bibliographical references:
Assessment:
Remarks:
CI 2Y
MODULE : ENTREPRISE
Unité de cours :
PROPRIETE INDUSTRIELLE
Chim
Coordonnateur :
INPI
Obligatoire
Code : FE2706
Semestre : 7
Cours : 10 Heures
TD :
Langue : Français
Coefficient :
Crédits ECTS : 1
Intervenants :
Objectifs et compétences visées :
- Appréhender les concepts de base et les finalités des différents outils de la propriété industrielle ;
- Savoir mobiliser la propriété industrielle comme source d’information dans le cadre d’un processus
d’innovation ou d’une recherche documentaire ;
- Maîtriser les méthodes et outils de recherches dans les bases de données de propriété industrielle.
Pré-requis :
Aucun
Programme :
Séance 1 – Enjeux et outils de la propriété intellectuelle / industrielle
- La propriété intellectuelle et industrielle : Définitions des concepts, Les enjeux de la propriété
industrielle, instrument de stratégie économique, Intérêt comme support de l’innovation dans
l’entreprise.
- Les précautions et bons réflexes avant tout lancement de projet : La conception (le brevet d’invention,
le brevet de perfectionnement), Comment protéger la valeur ajoutée par l’esthétique (le droit d’auteur
et les dessins et modèles), L’aspect commercial (les signes distinctifs, la marque, pour différencier ses
produits et services de ceux de la concurrence), Le développement à l’international.
- Les acteurs de la propriété industrielle : En France, A l’étranger.
Séance 2 – La propriété industrielle, source d’information pour la veille
- Le brevet, les marques, dessins et modèles : outils d’information incontournables de la créativité
industrielle.
- Veille et propriété industrielle : Le rôle de la veille dans la stratégie d’entreprise, Les différents types
de veille (technologique, économique, stratégique, concurrentielle…), brevets, marques, dessins et
modèles, outils d’informations stratégiques et concurrentielles.
- La place de la propriété industrielle dans le système d’information de l’entreprise : Organiser la
diffusion de l’information vers les utilisateurs clés, pour en faire un outil de connaissance et de
décision.
Séance 3 – Utiliser les bases de données de propriété industrielle
- Présentation des bases de données de propriété industrielle (payantes et gratuites)
- Les recherches dans les bases de données : Les différentes méthodologies de recherches dans les
bases de données de propriété industrielle ; remise d’un mémo.
Séance 4 – Cas pratiques de recherches dans les bases de données
- Mise en pratique : exercices de recherches dans les bases de données de brevets.
- Recherches bibliographiques dans les brevets du domaine de la chimie (en lien avec les projets
étudiants).
Informations supplémentaires :
Références bibliographiques :
Aucune
Modes d’évaluation et objectifs :
Aucune
Remarques Particulières :
CI 2A
MODULE : PRODUCTION TOOLS
SUBJECT :
INDUSTRIAL CATALYSIS AND PRODUCTION
Coordinator:
Edmond PAYEN
Edmond.payen@univ-lille1.fr
Office: +33(0)320337737
Mobile: 0680539988
Compulsory
Code : FE2703
Semester : 7
Lecture: 11 Hours
Directed studies:
Language : French
Coefficient : 3
ECTS : 1
Instructor(s):
Edmond PAYEN
Learning outcomes :
The objective is to show students the passage of fundamental knowledge in heterogeneous catalysis to
existing real systems, ie the production units The course is divided into two parts, i) the first one
covering the fundamental aspects of the catalysis for different processes will be taught by academics
and ii) the second one which aims students to understand the industrial aspects. It will be presented
by industrials will consist on the detailed presentation of industrial complexes.
This course focuses on the large chemical processes based on the fossil energy ressources, those
dealing with the biomasse ones are described in the S9
Prerequisite:
Fundamental knowledges required for this course are the theoretical basis of heterogeneous catalysis
namely, physical adsorption, ii) the mechanisms of catalysis of contact, the adsorption isotherms, the
chemical kinetics of simple and complex heterogeneous reactions.
Contents :
Part 1: Fundamental aspects of heterogeneous catalysis (12 h)
Chap. I: Introduction: Importance of heterogeneous catalysis: Economic data, Catalysis and Sustainable
Development, Petrorefining versus Petrochemistry
Chapter II: Hydrotreating/hydroconversion of petroleum fractions (HDS- kinetic and thermodynamic
aspect-reactors and micropilot), Hydrotreating (HDT), Aromatic hydrogenation (kinetic and
thermodynamic Aspect)
Chapter III: Cracking/Reforming/isomerization of petroleum fractions (catalyst/reactor) Chapter
IV: Diagram of a refinery and Valorisation of refinery gas (Syngas, FT synthesis)
Chapter V: Development of naphtha: production of large chemical intermediates
Oxidation of alkanes and olefins (ODH, mild oxidation): kinetic (Mars van Krevelen) and thermodynamic
aspects, reactor (type of reactor, explosive range), BTX.
Chapter VI: The DeNOx Catalysis: Fundamental aspects
Part 2: Industrial Units (12h): (Given by industrials)
Chapter I: Catalytic materials for automotive pollution control and industrial units (Dr V Harlé, Solvay-
Rhodia) – 2h40
Chapter II: Refining and Petrochemicals: on site course (3h) followed by a visit of the site)
Chapter III: Main chemical intermediates (Arkema) (2h40)
-Acrylic acid, maleic anhydride, formaldehyde, ... : Appearance and Reactor thermodynamic
- Basic rules for innovation in Catalysis and Processes and economics to value better catalyst
Chapter IV: Future of petroleum industry (IFPEN) (1h40)
Chap. V: dimerizations/co-dimerizations of olefins: Processes and New Technologies (IFPEN 2h)
Special Note: the bibliography will be given for each course
Additional information:
Media : Xerox copy of the Power Point Draw will be distributed
Bibliographical references: Techniques of the Engineer, D. horn - Kinetics and Catalysis, G. Scacchi, M.
Bouchy, J.F. Fouvaut, O. Zahraa Ed Lavoisier Technique and Documentation, 1996 ISBN: 2-7430-0144-5
- Chemical Kinetics and Catalysis, Richard I. Masel, A Wiley Interscience Wiley and Sons, INC.
PUBLICATION, 2001 ISBN 0-471-24197-0 - Principles and practice of heterogeneous catalysis, JM
Thomas, WJ Thomas, ISBN 3-527-29288-8 WCH 1996
Assessment: The writing examination will focus on real situation in which the students will have to
propose or justify the process selected or chosen for the implementation of a reaction in an industrial
environment taking into account the problems related to hygiene and safety.
Remarks:
CI 2Y
MODULE : PRODUCTION TOOLS
SUBJECT :
NUMERICAL MODELLISATION
Coordinator :
Ludovic.Thuinet@univ-lille1.fr
+33 (0)3 20 33 62 25
Office 232
Building C6
Compulsory
Code: FE2807
Semester: 8
Lecture:
Directed studies: 14 Hours
Language: French
Coefficient: 2
ECTS : 1
Instructor(s) :
Ludovic Thuinet
Andrée De Backer
Learning outcomes:
At the end of the course, the student must be able to use a rigorous method to model a specific
phenomenon in chemistry, which means :
To understand the underlying theory of the problem, to formulate the equations by specifying all the
assumptions made;
To solve the equations: generally, complex equations cannot be solved directly and require the use of a
specific numerical algorithm;
To write the programme in a specific language;
To analyze the numerical results and to compare them to experimental data.
At the end of this work, the student must understand how a scientific software is built.
Prerequisite:
Basic knowledge of a programming language, especially Scilab. Contents:
Subject CH1511: data systems
Subject TP1502: physical chemistry (practical studies)
Contents :
3 subjects will be chosen among the other courses taught at the ENSCL. The student will have to use
the following methodology:
To study a problem and to translate it mathematically
To choose an algorithm to solve the equations
To write the programme in Scilab
To plot and analyse the results with Scilab
Additional information:
Media: 1 short document summarizing the main features of Scilab.
Bibliographical references: a complete documentation on Scilab is at the disposal of the students on
the ENSCL Intranet. Various examples of scientific problems solved with Scilab can be found on the
ENPC website: http://cermics.enpc.fr/scilab_new/site/
Assessment: final exam of 2h on computers
Remarks:
CI 2Y
MODULE : ENGLISH
SUBJECT:
ENGLISH
Chim
Coordinator:
Anne GUEGAND
Abdelamar BENAÏSSA
Office 965
Tel:+33 (0)320336060
Compulsory
Code: LV2702
Semester(s): 7+8
Lecture:
Directed studies: 80 Hours
Language: English
Coefficient : 9
ECTS: 5
Instructor(s):
Anne GUEGAND
Abdelamar BENAÏSSA
Learning outcomes:
Language tuition at the ENSCL has a double objective :
-To help all students develop the communication skills they will need in professional situations through
interactive practice activities.
- To encourage prospective graduates to develop an international opening onto foreign companies and
universities to facilitate cross-cultural adaptability and adaptation.
Contents:
-TOEIC -2nd year topics (for example: Money and Commerce, Health and Safety, Recruitment…)
Additional information:
Media: Various (newspaper articles, publications, video documents, case studies…)
Assessment: Continuous language assessment is carried out through two written tests, an interview
and a presentation in English.
Remarks:
No English course for beginners
CI 2Y
MODULE : GERMAN
SUBJECT:
GERMAN
Chim
Coordinator:
Beate WINKLER
beate.winkler@ensc-lille.fr
Tel. +33 (0)320336061
Office 951
Compulsory
Code : LV2701
Semester (s): 7+8
Lecture:
Directed studies: 80 Hours
Language: German
Coefficient: 9
ECTS : 5
Instructor(s):
Beate WINKLER
Monika BERTOUT
Nathalie CHAPTAL
Caroline SIPPL
Learning outcomes:
Prerequisites:
All levels.
Pupils who have never studied German can enroll in a course for "beginners".
Objectives and skills referred:
Progress in the four language skills, but especially in the two that cause the greatest problem (listening
comprehension and oral expression) to validate at least the level B1 or B2 (A2 for the beginners) of the
CEFR.
Ability to integrate in a professional environment (with regard to courses and internships at University
or in foreign companies) and to communicate in situations of everyday life; acquisition of basic
knowledge of scientific and technical German in the field of chemistry.
Contents:
Internship report: learning how to describe and present the content of the students' internships. Describing a chemical process. The company: basic business German; overview of companies in the various areas of chemistry. Body, health, hygiene: visit to a doctor, security at work; cosmetic and pharmaceutical industry …
Environment and sustainable development: "green" chemistry, examples of businesses and their
activities in the German-speaking countries, current news on chemical incidents.
Dialects and characteristics of different regions in Germany and Austria - an introduction.
Additional information:
Media:
Various authentic media (print media, audio, video, movies, business documents, the internet).
The method "Studio D" for beginners.
Bibliographical references:
Books, movies in original version and journals are available on loan in a small German library.
Assessment:
Continuous language assessment is carried out through at least two written tests (two hours each) and
an oral test divided into two parts (a presentation and an interactive part).
Remarks:
Students are strongly encouraged to confirm their level by a certification in cooperation with the
Goethe-Institute:
"Zertifikat Start 2" (level A2 of the CEFR) for beginners.
"Zertifikat Deutsch" (Level B1 /B2 /C1 of the CEFR) for the more advanced students.
CI 2Y
MODULE : SPANISH
SUBJECT:
SPANISH
Chim
Coordinator:
Compulsory
Code: LV2706
Semester(s): 7+8
Lecture:
Directed studies: 80 Hours
Language: Spanish
Coefficient: 9
ECTS: 5
Instructor(s):
Hakima Larabii
Learning outcomes:
Strengthening B2 level of the Frame Common reference European for Languages, preparation at C1
level. At the end of the second year, the student must have attained the level of the autonomous
speaker.
Helping all students develop the condition skills they will need in professional situations (through
interactive practice activities).
Contents:
Linguistic, scientific and cultural aspects:
- Oral comprehension: multimedia language laboratory or video sequence.
- Oral expression: simulations and role play activities.
- Written comprehension: scientific or cultural texts.
- Written grammatical competences.
- Written expression (writing an informal or definite letter, a dialogue…)
- Preparation for the B2 DELE (Diploma de Español como Lengua Extranjera = B2 Spanish Certificate).
Additional information:
Media: Various (Newspaper articles, audio and video documents…).
Bibliographical references: Marco Común Europeo C1.
Assessment: Continuous language assesment is carried out through two written tests, an interview and
a presentation in Spanish.
Remarks:
No Spanish course for beginners.
CI 2Y
MODULE : FRANÇAIS LANGUE ETRANGERE
Unité de cours :
FRANÇAIS LANGUE ETRANGERE
Chim
Coordonnateur :
CUEEP
Obligatoire
Code : LV2705
Semestre(s) : 7+8
Cours :
TD : 50 Heures
Langue :
Coefficient : 9
Crédits ECTS : 5
Intervenants :
Objectifs et compétences visées :
Maîtrise efficace de la langue en particulier sur un plan professionnel : comprendre l’essentiel d’un
texte, prendre des notes en cours, donner son avis de façon brève mais claire sur un sujet général ou
professionnel.
Programme :
50H de FLE sur l'année en présentiel complétées, en fonction des acquis antérieurs et des besoins, par
un suivi individualisé avec auto-formation dirigée
Informations supplémentaires :
Supports :
Références bibliographiques :
Modes d’évaluation et objectifs :
Examen écrit et oral
Remarques Particulières :
CI 2A
MODULE : JAPANESE (OPTIONAL)
SUBJECT:
JAPANESE (OPTIONAL)
Chim
Coordinator:
Jean-Luc RIGAL
Jean-luc.rigal@enscl-lille.fr
Office 951
Compulsory
Code: LV2704
Semester(s): 7+8
Lecture:
Directed studies: 60 Hours
Language: Japanese
Coefficient:
ECTS:
Instructor(s):
Geoffrey DUCATILLON 1 2
Hitomi KIMURA 3
Aki KIUCHI 1
Nozomu MIZUKAMI 2
Shoko MORITA 4 5
Jean-Luc RIGAL 1 2 3
Maki TAMAOKI 1
Sachie WATANABE 2
Learning outcomes:
The main object of this course is to give basic communication tools to the students who intend to do their first, second or/and third year industrial placements in Japan, but also to complete the curriculum of future managers of a branch of industry which has many relations with Japan.
Contents:
One third of the course is devoted to civilization and two thirds to language. Because of the very particular writing system of Japanese, in which two syllabaries and at least 2000 ideograms are combined, reading and writing are given the same importance as oral work. In addition to the learning and systematic use of the two syllabaries, strong emphasis is put on the logic of ideograms, the objective being, through the study of a few hundreds of them, to facilitate the subsequent assimilation of those - much more numerous - which are necessary to everyday life. Level 2: In particular, Nihongo shoho 7-13, JDSR 6-14, Katana nyûmon, Bushu 1-100 (101-214 in level 3).
Additional information:
Media:
Minna no nihongo, Nihongo shoho (1, 2, 3), Nihongo chûkyû, Kana nyûmon (hiragana 1) (katakana 2),
Nelson Kan’ei jiten (2, 3)
Bibliographical references:
Nihon etoki jiten 1-16 (JTB), Nihongo notes 1-5 (The Japan Times), Situational Japanese 1-5 (The Japan
Times)
Assessment:
Oral and written exams, continuous assessment
Remarks:
The course is divided into 5 levels, and not according to the three years of the curriculum. As a matter of fact, if Level I is mainly attended by first year students, Level II by second year students and Level III by third year students, some students start the study of Japanese in their second/third year, whereas other students - especially those who come from the "CPI" - may have been studying Japanese for two years or more when they start their engineering studies.
Prerequisites:
None, other than the desire to learn Japanese (WRITTEN INCLUDED)
CI 2Y
MODULE 2 : MOLECULES
SUBJECT :
THE CHEMISTRY OF CARBOHYDRATES
Coordinator:
Professor Philippe Cotelle
Philippe.cotelle@ensc-lille.fr
03 20 43 48 58
Door 101 Building C1
Obligatoire
Code : OP2802-8
Semester : 8
Lecture : 10 Hours
Directed Studies :
Language : French
Coefficient : 1.5
ECTS :
Instructor(s):
Professor Philippe Cotelle
Learning Outcomes:
Have a vision of set on the carbohydrate structure (mono, di et polysaccharides) and their use as agro
sourced building blocks in the synthesis of biological active molecules
Be able to apply the protection/deprotection strategy to the carbohydrate chemistry and design
synthesis of mono and disaccharides of biological interest (ex : 18-fluoroglucose for positron emission
tomography, Tamiflu, AZT)
Prerequisite:
Basis in organic chemistry, semesters S5 & S6, CH1503 and CH1603 and semester S7, CH2703
Contents:
• Introduction: cycle of carbon, fonctions, métabolism
• Structure: Classification, fonctions (aldose, cétose, reductor, non-réducteur), isomerism,
anomerism, equilibrium (furanose, pyranose, acyclic form)
Monosaccharides, Disaccharides, Polysaccharides, Cyclic saccharides
• protection, reactivity, synthesis
• Introduction
• Reduction
• Oxidation
• Reactions at the carbonyl fonction
• Protection of the hydroxyl groups
• Synthesis of some compounds of biological interest
• Additional information:
Media : powerpoint
Bibliographical references : S .V. Bhat, B.A. Nagasampagi, M. Sivakumar, Chemistry of natural products,
Springer, 2005, ISBN 3-540-40669-7
Assessment : Written exam (1 hour)
Remarks:
CI 2Y
Année 2012-2013
5th academic year (semesters 9 and 10)Final year of study Master level
MODULE : BIOMASS
SUBJECT:
MOLECULAR AND ENZYMATIC CONVERSION OF BIOMASS INTO CHEMICALS
Coordinator:
Edmond.payen@ensc-lille.fr
Office :+33 (0)320434949
Mobile : 0680539988
Semi-optional
Code: OP3901-11
Semester: 9
Lecture: 20 Hours
Directed studies:
Language: French
Coefficient: 4
ECTS: 2
Instructor(s):
Valérie MOLINIER
Valerie.Molinier@ensc-lille.fr
+33 (0)320 33 63 66
Office 19, building C6
Learning outcomes:
Knowing the main biomass feedstock and their conversion into chemicals in a context of sustainable
development
Have an overview of the nature and use of the platform molecules easily accessible at an industrial
scale from chemical and enzymatic conversion of biomass, with an emphasis on the starch derivatives
Get familiar with the “Green Chemistry” principles
Knowing the solvents and surfactants obtained from biomass: their preparation, their properties, their
use and how they can substitute the petrochemical homologues
Prerequisite:
Contents:
Organic chemistry lessons of semesters S5, S6 and S7 ; Formulation physico-chemistry S7
Contents:
Context
Why using biomass as raw material for chemicals
Definitions: biomass / valorisation / green chemistry / synthon
Resources / biomass feedstock
Chemicals from starch
The starch-rich cultures
Starch extraction
From starch to glucose / main applications
From glucose to sorbitol / main applications
Some other synthons accessibles from starch via Oxydation / Fermentation / Dehydratation /
Hydrogenation
Solvents from biomass (see separate description)
Surfactants from biomass (see separate description)
Additional information:
Media: lesson documents
Bibliographical references:
Selected scientific articles corresponding to the keywords: biomass, biorefineries, agro-synthons,
chemicals from biomass, biosolvents, biosurfactants
« La chimie verte » Paul Colonna
Assessment:
Written exam (2h) at the end
Remarks:
CI 3Y
MODULE : CHEMISTRY OF BIOMASS
SUBJECT:
CATALYSIS FOR PRODUCING KEY CHEMICAL INTERMEDIATES
Coordinator:
Edmond.payen@ensc-lille.fr
+33 (0)320434949
0680539988
Building C3
Obligatoire
Code: OP3901-12
Semester: 9
Lecture: 20 Hours
Directed studies: -
Language: French
Coefficient: 4
ECTS: 2
Instructor(s):
Franck Dumeignil
franck.dumeignil@univ-
lille1.fr
+33(0)3.20.43.49.38
Bureau 101/Bât C3
Learning outcomes:
The student who will have validated this module will have acquired a broad, complete and up-to-date
view of the main types of catalytic transformations to be implemented in the latest concepts of
biorefineries. His(her) knowledge will place him(her) at the forefront of the state of art in a booming
emerging sector with a strong societal demand, where many - both academic and industrial - career
opportunities already open.
Prerequisite:
Students wishing to take this training must have a good background in catalysis and must be aware of
the most usual reactions (and of the main moieties of interest) in organic chemistry, together with
having a broad basic knowledge of the main current techniques used in spectrochemistry. The
multidisciplinary nature of the topic addressed in the lectures also requires a good general culture and
a spirit of curiosity that is not limited to chemistry but also touches on all scientific disciplines.
Contents:
The development and implementation of biorefinery processes is of the upmost importance to meet
the vision towards a sustainable economy based on bio-resources. In this context, catalysis, either
enzymatic, heterogeneous or homogeneous is playing a major role like this is already the case in a
‘conventional’ refinery based on the treatment and the conversion of petro-resources. Nevertheless,
contrary to petro-resources of which the nature and composition variations are ‘relatively’ limited,
under the term ‘bio-resource’ or ‘biomass’ are gathered compounds of very different natures, namely
cellulose, hemicellulose, oils, lignin and so on… Thus, a complete set of specific catalytic processes must
be developed, which will constitute core technologies that will be implemented in the so-called
‘biorefineries’.
The major catalytic technologies developed for – especially – elaborating the new generation of
biorefineries expected for 2015-2020 will be thus reviewed within the frame of these lectures (e.g.,
project 'EuroBioRef' leaded by the coordinator of this teaching unit:
http://www.dr18.cnrs.fr/assets/files/weblettre210/EuroBioRef_H_Res.pdf).
Additional information:
Media: Lecture presented under the form of Powerpoint presentations, with movies, and written
documents.
Bibliographical references: http://eurobioref.org/Summer_School/
‘Biorefinery: From Biomass to Chemicals and Fuels’ (Eds Michele Aresta, Angela Dibenedetto, Franck
Dumeignil) Degruyter editions. ISBN: 978-3-11-026028-1.
Assessment: Final control under the form of a multiple-choice questionnaire.
Remarks:
CI 3Y
MODULE : CHEMISTRY OF THE BIOMASS
SUBJECT:
CHEMISTRY OF NATURAL AND BIOSOURCED MACROMOLECULES
Coordinator:
Edmond.payen@univ-lille1.fr
0320434949
0680539988Tel / Bureau
Obligatoire
Code: OP3901-13
Semester: 9
Lecture: 20 Hours
Directed studies: -
Language: French
Coefficient: 4
ECTS: 2
Instructor(s):
Patrice Woisel
Patrice.woisel@ensc-
lille.fr/0320434954/Bât. C6 p.
123
Learning outcomes:
The main objective of this course is to present an overview of the different chemical transformations
that can be used to elaborate interesting polymeric materials from biosourced (macro)molecules.
Prerequisite:
CH1604/CI2704/CH1503
Contents:
Chapter 1: Introduction
1) Different classes of biosourced polymeric materials
2) Agricultural sectors involved
3) Industrial sectors involved
4) Assets and constraints
Chapter 2: Agro-materials
1) Main classes of vegetal based biopolymers
2) Biosynthesis and properties
3) Chemical transformations and applications
Chapter 3 : Bio-polymers
1) Main synthons
2) Polymerisation of synthons
Additional information:
Media: Duplicated lecture note + documents given during the courses
Bibliographical references:
1) Renewable Polymers: Synthesis, Processing, and Technology Vikas Mittal (Editor), Wiley, ISBN: 0470938773, 978-0470938775
2) Monomers, Polymers And Composites From Renewable Resources Elsevier, 2008 ISBN: 0080453163, 9780080453163
Assessment: 1 written exam
Remarks:
CI 3Y
MODULE : CHEMISTRY OF THE BIOMASS
SUBJECT:
BIOENERGIES
Coordinator:
Edmond.payen@ensc-lille.fr
+33 320434949
Building C3 – ground floor
Phone +33 (0)680539988
Semi-optional
Code: OP3901-14
Semester: 9
Lecture: 20 Hours
Directed studies:
Language: French
Coefficient:
ECTS: 2
Instructor(s):
Edmond PAYEN
Learning outcomes:
After the S6 and S7 during which the students had learned industrial heterogeneous catalysis and seen the major industrial processes especially for energy production, the student who has validated this module will have acquired a broad vision, integrity and timeliness, of the major types of transformations, catalytic or not, implemented or considered for the production of energy from biomass. Knowledge of the chemistry of these processes and reactors to implement will place them at the top of the state of the art in an emerging sector booming industrial level (bioTfuel project site on Total Dunkerque site, Sasol-Katar).
Prerequisite: Students wishing to follow this training would have a good grounding in i) heterogeneous catalysis, ca. physical and chemical adsorption, formal kinetics, catalyst preparation (ca. should have followed the course XXXX -A.S Mamede S6- and the XXXX-A S Mamede S8 ) and ii) Industrial Catalysis and production (course XXXX-E. Payen S7) Contents Chap. 1: (1 h): Introduction: The energy sources of the XIX to XXI century ; Chap. 2 (3 h): biogas (CH4, CO2, ...): Production process, purification; Downstream applications (oxidation of methane, etc ...). Chap. 3 (1 h): 1st generation of biobased fuels: @ Diester, process AXENS Chap. 4 (4 h): Bioconversion of cellulose and hemicellulose: Processes of hydrolysis and fermentation primarily for alcohols;
Valuation of alcohols (Bio fuel and fuel additives; steam reforming (hydrogen production and co-products
Chap. 5 (5 h): Biosyngas (CO/H2) of lignin and biomass waste Production process: gasification of waste biomass Processing / Applications: (FT synthesis for obtaining alkanes, diesel additives);
Synthesis Syngas for the production of alcohols and other compounds (MeSH, ethylene, hydrogen).
Chap. 6 (5 h): bio-oils and their transformations Methods for obtaining (Flash Pyrolysis, .... of lignin and biomass residues; Purification and processing of bio-oils (HDO, decarboxylation, FCC ...) Applications of bio-oils (diesel fuels by gasification and FT) Conclusion: Schematic global energy production from biomass 1 conference given by an industrial in the energy sector (1h) Additional informations Media: Power Point available on the intranet, Printout distributed (with inset for free student comments)) Bibliographical references: Les biocarburants, D Ballerini, Editions Technip, 2006, France
Bibliographic references given during the course Assessment: Final writing examination (2h) will be performed that will be divided into 2 parts, the 1
st one dealing
with fondamental aspects of a process and the second one which will consist in an analysis of a scientific publication on a process Remarks:
CI 3Y
MODULE : CLEAN PROCESSES
SUBJECT:
BIOPROCESSES
Coordinator:
Edmond.payen@ensc-lille.fr
+33 320434949
Building C3 – ground floor
Phone +33 (0)680539988
Philippe Jacques
Tel+33 (0)328767440
Philippe.Jacques@polytech-
lille.fr
Semi-optional
Code: OP3901-21
Semester: 9
Lecture: 20 Hours
Directed studies:
Language: French
Coefficient: 4
ECTS: 2
Instructor(s):
Marlène Chollet
François Krier
Alice Rochex
François Coutte
Learning outcomes:
To understand basic microbiology at qualitative and quantitative point of view (the different types of
micro-organisms, their conditions and kinetic of growth, their metabolism)
To be able to set up and develop a microbial product (strain screening, growth optimization, production
in bioreactors, formulation)
Prerequisite:
General biochemistry, mass transfer, heat transfer, mixing
Contents:
The course is organized with combined lectures and exercises.
Chapters : History, Microbial culture and mass balance, Growth kinetics, Growth control and
sterilization, cellular structure and microscopy, taxonomy, metabolism, genetic engineering, production
in bioreactors, downstream processing, Bioprocess optimization, Examples of production : yeast,
antibiotics, enzymes, biopesticides, biosurfactants, soil bioremediation.
Additional information:
Media: syllabus
Bibliographical references: Microbiology, Prescott ; Microbiologie Industrielle, Leveaux ; Techniques de
l’ingénieur
Assessment: written examination with general questions and exercises
Remarks:
CI 3Y
MODULE : PROCEDES PROPRES
Unité de cours :
GENIE DES REACTEURS – REACTEURS DU FUTUR/TECHNOLOGIES PROPRES
Chim
Coordonnateur :
Edmond.Payen@univ-lille1.fr
Semi-optionnel
Code : OP3901-23
Semestre : 9
Cours : 15 Heures
TD :
Langue : Français
Coefficient :
Crédits ECTS :
Intervenants :
Pascal Fongarland
Objectifs et compétences visées :
The objective of this learning unit is to give some skills for the experimental design and scale-up of
industrial or laboratory reactors for clean processes. The coupling between chemical reaction (catalytic
or not) and the mass/heat transfer will be studied using the chemical engineering tools. The first part
will allow to identify the limitations of the traditional reactor technologies in order to introduce the
different ways of improvements for the new reactors as process intensification (microreactors,
structured reactors ...) or the integration of other unit operations (reactive extraction ...).
Pré-requis :
The knowledge required for this course are the bases in mass/heat transfer and in dimensional analysis.
Bases in ideal reactors (perfectly mixed reactor, plug flow reactor) are also required. The knowledge in
heterogeneous catalysis will be brought with the course provided in the second year and will allow to
give a background in the problematic of the heterogeneous reactors .
Programme :
Part 1: Heterogeneous reactors (course/TD 15 h) Chap. I. Introduction Industrial reactors, the reactor in the process. Chap. II. Chemical production rate Measurement of a kinetic rate, apparent and intrinsic rate, chemical and physical phenomena coupling. Chap. III. Reaction/diffusion competition. External and internal mass transfer, the case of gas-liquid system. Chap. IV. Heterogeneous reactors Fixed and fluidized bed, agitated reactors, scaling and simulation of heterogeneous reactors. Part 2: New reactors and clean technologies (course/TD 10 h) Chap. I. What are the needs to design new reactors ? Limitations of actual technologies, process intensification: a "new-old" concept, the different approaches. Chap. II. Mass/heat Transfer intensification Micro and structured reactors, characteristic parameters, process security, drawbacks of the micro technology, "numbering-up" vs "scaling-up", energy saving, examples. Chap. III: From batch to continuous reactor. Chap. IV: Shift of the equilibrated reactions Shift equilibrium, reactive distillation, membrane technology. Chap. V: Conclusion et perspectives Intensification et clean process, integrated process
Informations supplémentaires :
Supports : Power Point with paper copy
Bilibiography: Génie de la réaction catalytique, D. Schweich, Ed. Tech&Doc; Techniques de l'ingénieur;
Elements of Chemical Reaction Engineering, H. Scott Foggler, Pearson Int. ed.
Course evaluation : Writing exam (2h).
Remarques Particulières :
CI 3A
MODULE : CLEAN PROCESSES
SUBJECT:
RECYLING AND GREEN PLASTIC MANUFACTURING PROCESS
Coordinator:
Edmond.payen@ensc-lille.fr
+33 320434949
Building C3 – ground floor
Phone +33 (0)680539988
Semi-optional
Code: OP3901-24
Semester: 9
Lecture: 15 Hours
Directed studies:
Language: French
Coefficient: 2.5
ECTS: 1
Instructor(s):
Sophie DUQUESNE,
+33(0)320337236, Office 112
Learning outcomes:
The aim of this lecture is to present the engineering processes of polymers and composite materials
that meet the criteria of sustainable development as well as the recycling processes.
Prerequisite:
Contents: Polymer Material sciences (S7-S8) ; Life Cycle Assessment (S5) ; Polymer characterisation and
formulation (S7-S8) ; Polymer from Renewable Resources (S9)
Contents:
Green Engineering Process of Polymer and Composites
- The use of natural substances (starch…)
- Bacterial polymers production
- Innovative Processes (reactive extrusion, use of supercritical fluid…)
- Clean Production of Composites
Polymer Recycling
- Sorting of polymers
- Chemical recylcing
- Mechanical recycling
- Recycling of polymer composites
Additional information:
Media:
Bibliographical references:
Caroline Baillie; Green Composites: Polymer Composites and the Environment, CRC Press
Assessment: written exam, 60min
Remarks:
CI 3Y
MODULE : ENVIRONMENT
SUBJECT:
GASEOUS EFFLUENT TREATMENT
Coordinator:
Edmond.payen@univ-lille1.fr
+33 320434949
Building C3 – ground floor
Phone +33 (0)680539988
Semi-optional
Code: OP3901-31
Semester: 9
Lecture: 20 Hours
Directed studies:
Language: French
Coefficient: 4
ECTS: 2
Instructor(s):
Jean-François / Lamonier
Anne / Ponchel
Learning outcomes:
Control the industrial emissions into the atmosphere to improve the air quality is a major
environmental and economic challenge for the industrial world. Since the reduction targets of
industrial pollutants in the air are increasingly difficult to reach, it has become essential to treat the
gaseous emissions before their release into the atmosphere. This course unit aims to present the most
suitable remediation methods but also recent developments which can be implemented for the
treatment of air containing pollutants. A student who has validated this course unit will have acquired
skills in current concepts and practices of treatment processes of the air (like regenerative or
destructive) but also will possess a thorough knowledge of the latest technological developments for
the treatment of industrial gaseous effluents
Prerequisite:
Basic notions of thermodynamics and kinetics (solubility, reactivity, catalysis ...)
Contents:
* Sources and impacts of major pollutants at local, regional and global scale
* Means implemented in the fight against air pollution
* Presentation of the different processes leading to the destruction or the recovery of the pollutants
* Application to the treatment of NOx, N2O, SOx, VOC and dust (current technology, emerging or
innovative / research)
* Capture, Storage and Recovery of CO2
Additional information:
Media:
Courses in the form of "powerpoint" presentation + handouts
Bibliographical references:
1. Traitement des pollutions industrielles – Emilian Koller - Dunod/L'Usine Nouvelle (2009)
2. Les COV dans l’environnement – Pierre Le Cloirec - Tec & Doc, Lavoisier, Paris (1998)
3. Traitement des fumées - Pierre Le Cloirec – Techniques de l’Ingénieur (2006)
4. Analyse et traitement physicochimique des rejets atmosphériques industriels – M. Popescou et Coll -
Tec & Doc, Lavoisier, Paris (1998)
5. La réduction des émissions de composés organiques volatils dans l’industrie - Guide et Cahier
Techniques, Ademe, Angers (1998) …
Assessment:
1 Final exam: questions from lesson + study of documents
Remarks:
CI 3Y
MODULE : ENVIRONMENT
SUBJECT:
WATER TREATMENT
Coordinator:
Edmond.payen@univ-lille1.fr
0320
0680539988Tel / Bureau
Semi-optional
Code: OP3901-32
Semester: 9
Lecture: 20 Hours
Directed studies:
Language: French
Coefficient: 4
ECTS: 2
Instructor(s):
Alain HURE
ahure@mexel.fr
+ 33 3 44 38 39 40
+ 33 6 62 00 75 24
Learning outcomes:
Cover the main problem of water treatment
Make the useful knowledge on pollution
Understanding the issues in its various aspects, prevention, conditioning and treatment
Prerequisite:
No special knowledge if its to have a good knowledge in chemistry
Contents:
1: raw water
2: industrial water
3: drinking water
4: treatment of urban and industrial waste water
5: waste management of sludge
Additional information:
Media: powerpoint presentation
Bibliographical references:
Memento technique de l’eau – Degremont ; Corosion des métaux et alliages – Beranger et Mazille ;
Heat echanger fouling – Muller Steinhagen ; L’épuration biologique des eaux – Edeline; Bactéries et
environnement - Pelmont
Assessment:
Remarks:
CI 3Y
MODULE : ENVIRONMENT
SUBJECT:
CONTAMINATED SOILS TREATMENT
Coordinator:
Edmond.payen@univ-lille1.fr
+33 320434949
Building C3 – ground floor
Phone +33 (0)680539988
Obligatoire
Code: OP3901-33
Semester: 9
Lecture: 8 Hours
Directed studies:
Language: French
Coefficient: 1.5
ECTS: 1
Instructor(s):
Nicolas PROIX
proix@arras.inra.fr
Laboratoire d’analyses des
sols,
273 rue de Cambrai
62000 Arras
Learning outcomes:
To acquire fundamental knowledge on soils, to know the methods of treatments of polluted soils and
the analytical tools.
Prerequisite:
General chemistry
Contents:
- Presentation of soils (2 hours): Notion of pedology, quality of the French soils
- Various pollutants (2 hours): Pollutants of mineral origin, organic pollutants
- Treatments (3 hours): The various methods of remediation, the stabilization, the management of
polluted sites
- Legislation and examples of case studies (1 hour)
Additional information:
Media: lecture manual.
Bibliographical references:
Guide des analyses en analyse pédologique, Denis Baize, ed Quae, 2000
Les éléments traces métalliques, approche fonctionnelle et spatiale, Denis Baize, ed Quae, 2002
Stratégie de remediation des sols pollués, jean Louis Morel,
Assessment:
A written examination
Remarks:
CI 3Y
MODULE : ENVIRONMENT
SUBJECT:
RECYCLABILITY AND RECOVERY OF INDUSTRIAL WASTES
YCLABILITE ET VALORISATION DES DECHETS INDUSTRIELS
Coordinator:
Edmond.payen@ensc-lille.fr
+33 320434949
Building C3 – ground floor
Phone +33 (0)680539988
Semi-optional
Code: OP3901-34
Semester: 9
Lecture: 12 Hours
Directed studies:
Language: French
Coefficient: 2
ECTS: 1
Instructor(s):
Caroline PIROVANO
Murielle RIVENET
Learning outcomes:
In the global context of the management of waste and in the respect for the criteria of sustainable
development, the objectives of this lecture are to present, from an economic, legislative and
technologic point of view, the principles of recycling and valorization of industrial wastes.
Prerequisite:
General chemistry
Contents:
- The global context of wastes: classifications of wastes, legislation…
- Wastes regulation and recovery: The actors and their problematic
- Thermal treatments methods and associated valorisations
- Recycling of metals (ferrous and non ferrous), the management of the steel-making by-products
- Recycling of oils and solvents
- Recycling of nuclear fuel cycle
Additional information:
Media:
Lecture manual.
Bibliographical references:
- Techniques de l'Ingénieur (http://www.techniques-ingenieur.fr/)
- Environmental Chemistry, 9th ed., Stanley E. Manahan, CRC Press, 2010
- ADEME publications, various documentations…
Assessment:
A written examination
Remarks:
CI 3Y
MODULE : FORMULATION PHYSICAL CHEMISTRY
SUBJECT:
FORMULATION PHYSICAL-CHEMISTRY
Coordinator:
Prof. Jean-Marie AUBRY
Jean-marie.aubry@ensc-
lille.fr
Tel + 3 (0)320 33 63 64
Office: C6 Ground floor
Obligatoire
Code: OP3902-11
Semester: 9
Lecture: 60 Hours
Directed studies:
Language: French
Coefficient: 12
ECTS: 4
Instructor(s):
Prof Jean-Marie AUBRY
Prof Jean-Louis SALAGER
(University of Merida)
Learning outcomes:
Learning fundamental concepts and basic techniques of colloidal chemistry
Understanding the physical origin of optical effects (opacity, dullness, color, pearlescent) utilized in
formulated products.
Master the tools for designing micro-and macro-emulsions with given characteristics (morphology,
particle size, stability, viscosity).
Prerequisite:
Light-matter interactions (scattering, refraction, diffraction)
Binary and ternary phase diagrams.
Superficial, interfacial and self-aggregative properties of surfactants
Contents:
A) Molecular solubilization
● HSE properties of conventional and eco-friendly solvents
● Hansen solubility parameters and novel solubilization theories
B) Colloids and dispersed systems Solid / Liquid:
● Physico-chemical and functional properties of surfactants
● DLVO theory, steric and electrostatic stabilization of dispersed systems
● Interaction of light with dispersed systems (particle size, opacity)
C) Phase diagram of binary and ternary systems Surfactant / Water / Oil
● Solubilization in water of hydrophobic compounds (application to perfumes and degreasing)
● Microemulsions, the HLD and the “optimal formulation” concepts
D) Emulsions
● Maps formulation-composition (correlation between micro- and macro- emulsions)
● Principles of emulsion formulation and characterization methods
Additional information:
Media: Handout of JL Salager’s slides
Bibliographical references: All articles of the section “Formulation” of the encyclopedia “Techinques de
l’Ingénieur”
Assessment: Written examination of 2 hours
Remarks:
CI 3Y
MODULE : EXPERIMENTAL DESIGN AND DATA ANALYSIS
SUBJECT:
EXPERIMENTAL DESIGN FOR MIXTURES
Coordinator:
Jean-marie.aubry@ensc-
lille.fr
Tél +33(0)3 20 33 63 64
Building C6
Semi-optional
Code: OP3902-21
Semester: 9
Lecture: 10 Hours
Directed studies:
Language: French
Coefficient: 2
ECTS: 1
Instructor(s):
Christel Pierlot
Christel.pierlot@univ-lille1.fr
Tél : 03-20-33-63-65
Bât C6, RdC, salle 21
Learning outcomes:
Provide basic notions for designing and analyzing experimental design mixtures
Prerequisite:
Contents:
Classical experimental design (screening matrix ,factorial and fractional factorial
matrix, Simplex, Surfaces responses)
Contents:
1. Introduction
2. Details of the approach
3. Scheffé Simplex Networks
4. Scheffé Simplex Networks (centroids)
5. Axial matrices
6. Mixtures with constraints
Additional information:
Media:
Distributed lecture notes, course on power point
Bibliographical references:
Techniques de l'ingénieur : Planification d’expériences en formulation, Didier MATHIEU, Roger PHAN-
TAN-LUU, J2241, (2001).
Assessment:
Submission of a report (15 pages) and oral presentation (15 min) on a project to
optimize recipes (chocolate mousses, marshmallows,nougat, ...) by the method of experimental
designs (classic or mixtures)
Remarks:
CI 3Y
MODULE : EXPERIMENTAL DESIGN AND DATA ANALYSIS
SUBJECT:
ADVANCED EXPERIMENTAL DESIGN AND PRINCIPAL COMPONENT ANALYSIS
Coordinator:
Jean-marie.aubry@ensc-
lille.fr
Tél +33(0)3 20 33 63 64
Building C6
Semi-optional
Code: OP3902-22
Semester: 9
Lecture: 5 Hours
Directed studies: 5 Hours
Language: French
Coefficient:
ECTS: 1
Instructor(s):
Christel Pierlot
Christel.pierlot@ensc-lille.fr
Tél : +33(0)3 20 33 63 65
Building C6, office 21
Learning outcomes:
Provide basic notions necessary to design and analyze
- advanced experiments designs (custom matrix, exchanges algorithm construction )
- A classical method of statistical analysis: the principal component analysis (PCA).
Prerequisite:
Contents: classical experimental design (screening matrix ,factorial and fractional factorial
matrix, Simplex, Surfaces responses)
Conventional statistics courses (mean, variance, standard deviation,normal distribution, ...)
Contents:
Course (5 hours):
1) Advanced Design of Experiments
1.1) matrix with factors at more than 3 levels
1.2) Custom Matrix, with constraints, algorithm exchanges construction
2) Principal Component Analysis
Directed studies (5h):
1) In classroom
Completion of design of experiments with constraints (optimization of a cocktail by sensorial analysis)
2) On the computer
Use of softwares (design of experiments and ACP)
-treatment data from the optimization of a cocktail, and a variety of situations encountered
in formulation area.
Additional information:
Media:
Distributed lecture notes, course on power point
Bibliographical references:
Techniques de l'Ingénieur : Analyse des données ou statistique exploratoire multidimensionnelle,
Philippe BESSE, Alain BACCINI, AF620 (2011).
Assessment: Test in computer room (1 hour) using two sofwares (design of experiments and ACP)
Remarks:
CI 3Y
MODULE : FUNCTIONAL INGREDIENTS AND FORMULATIONS
SUBJECT:
COLOR, DYES AND PIGMENTS
Coordinator:
Jean-marie.aubry@ensc-
lille.fr
Tél +33(0)3 20 33 63 64
Building C6
Semi-optional
Code: OP3902-31
Semester: 9
Lecture: 6 Hours
Directed studies:
Language: French
Coefficient: 5
ECTS: 1
Instructor(s):
Christel Pierlot
Christel.pierlot@ensc-lille.fr
Tél : +33 (0)3-20-33-63-65
Building C6, office 21
Learning outcomes:
Provide basic notions necessary to to understand the mechanisms ofcolor perception.To understand
the principles of color measurement. To know the main pigments and dyes used in industry.
Prerequisite:
Contents: classical organic, inorganic and general chemistry courses
Contents:
Mechanisms of color perception.
How do you measure a color (apparatus)?
Main dyes and pigments
Review of formulated products
Additional information:
Media:
Distributed lecture notes, course on power point
Bibliographical references:
Techniques de l'Ingénieur-Colorants et pigments-Alain Bondoux, AM3234, (2003).
Assessment:
Test without documents, 45 min
Remarks:
CI 3Y
MODULE : FUNCTIONAL INGREDIENTS AND FORMULATIONS
SUBJECT:
RHEOLOGICAL AGENTS
Coordinator:
Jean-marie.aubry@ensc-
lille.fr
Tél +33(0)3 20 33 63 64
Building C6
Semi-optional
Code: OP3902-32
Semester: 9
Lecture: 6 Hours
Directed studies:
Language: French
Coefficient: 5
ECTS: 1
Instructor(s):
Christel Pierlot
Christel.pierlot@ensc-lille.fr
Tél : +33 (0)3-20-33-63-65
Building C6, office 21
Learning outcomes:
Descriptions of the various organic and mineral rheological agents used in formulation
Prerequisite:
Contents: classical organic and polymer chemistry courses
Contents:
-Rheology: Reminder
-Emulsions
-Polymers (Thickening, reversible and irreversible Gelling)
- Minerals
- Surfactants
- Review of formulated products (cosmetic creams, shampoos, ...)
Additional information:
Media: Distributed lecture notes, course on power point
Bibliographical references: Techniques de l'Ingénieur :
Formulation des polymères synthétiques en cosmétique, Bernard LE NEINDRE, Patrick CANCOUËT, J 2
190 (2011).
Carraghénanes : agents gélifiants,épaississants et stabilisants+ Carraghénanes : agents gélifiants,
épaississants et stabilisants, Jaime ZAMORANO, F 5 080 (2006).
Mesure de la viscosité, Viscosimètres et rhéomètres, Dominique DUPUIS, R 2 351 (2008).
Assessment: Test without documents, 45 min
Remarks:
CI 3Y
MODULE: FUNCTIONNAL INGREDIENTS AND FORMULATIONS
SUBJECT:
BIO-BASED SUFRACTANTS AND SOLVENTS
Coordinator:
Jean-marie.aubry@ensc-
lille.fr
Tél +3 3 20 33 63 64
Office: Building C6
Ground flour
Semi-optional
Code: OP3902-34
Semester: 9
Lecture: 10 Hours
Directed studies:
Language: French
Coefficient: 2
ECTS: 1
Instructor(s):
Valérie MOLINIER
Valerie.Molinier@ensc-lille.fr
+33 3 20 33 63 66
Office 19, Building C6
Ground flour
Learning outcomes:
Knowing the solvents and surfactants obtained from biomass: their preparation, their properties, their
use and how they can substitute the petrochemical homologues
Prerequisite:
Contents:
Organic chemistry lessons of semesters S5, S6 and S7; Formulation physico-chemistry S7
Contents:
Solvents from biomass
- Definitions (solvents, biosolvents, solvents from biomass) - Families of “green” solvents on the market: preparation, volumes, industrial actors - Evolution of the solvents market / environmental regulations - Application fields for biosolvents: solvents (pharmacy, agrochemistry), lubrificants, plasticizers (paints, coatings) - Substitution of dangerous solvents / physico-chemical and predictive tools - Physico-chemical characteristics of “green” solvents; formulation of green solvents Surfactants from biomass
- Families of “green” surfactants on the market: volumes, industrial actors - Evolution of the surfactants market / environmental regulations - Sources of the lipophilic part: fatty esters / acids / alcohols: preparation, nomenclature - Surfactants from glycerol, sorbitol, glucose, sucrose:
Application fields Industrial and alternative (green chemistry) preparation Physico-chemical properties compared to petrochemical derivatives Bionotox properties
- Surfactants produced by micro-organisms: biosurfactants Additional information:
Media:
lesson documents
Bibliographical references:
Selected scientific articles corresponding to the keywords: biosolvents, biosurfactants
Nonionic surfactants (Surfactant science series)
Handbook of applied surface and colloid chemistry
Assessment:
Written exam (1h) at the end
Remarks:
/
CI 3Y
MODULE : PROCESS OF THE FORMULATION ENGINEERING
SUBJECT:
RHEOLOGY OF FLUIDS
Coordinator:
Jean-marie.aubry@ensc-
lille.fr
Tél : +33 3 20 33 63 64
Office : bât. C6 -RdC
Obligatoire
Code: OP3902-41
Semester: 9
Lecture: 10 Hours
Directed studies:
Language: French
Coefficient: 4
ECTS: 1
Instructor(s):
Guillaume Delaplace
Learning outcomes:
Students will be able:
- To distinguish different types of rheological behavior of liquid (Newtonian or not): purely viscous
fluids (shear thinning, yield stress, shear thickening), time-dependent fluid (thixotropic), with elastic
properties (viscoelastic),
- To implement adequate rheological tests to identify the rheological behaviour of unknown products.
- To take into account the rheological properties to model transfers (flow, heat and mass) in
continuous and discontinuous processes
Prerequisite:
Licence chemistry or physical
Contents:
1 Definition - fluid/solid - Newtonian and Non Newtonian - main problems related to non-newtonian
behaviour in chemical industry - rheology goal: a science to better identify the flow of the complex
fluid and associated transfer
2. Terminology standard for simple shear tests used in rheology - laminar shear movement - velocity
gradient, shear rate, shear stress, apparent viscosity - units, order of magnitude, dependent and the
pressure - viscosity, specific, intrinsic, dynamic...
3 Classification of rheological behaviour with pure shear tests: purely viscous fluids (shear thinning,
yield stress, shear thickening), time-dependent fluid (thixotropic), with elastic properties (viscoelastic),
4. Models typically used to describe the rheological behaviour of fluids
5. Devices for measuring the rheological properties - rheometer in steady mode- rheometer in transient
mode - oscillating tests
6. Interaction rheology - Processes - Velocity profile (friction in ducts and in vessel) , Residence time
distribution, heat transfer performances
7 Methods of modelling of transfers in real systems (batch and continuous) - Determination and use of
dimensionless numbers associated to rheological properties - concept of Metzner and Reed - concept
of Metzner and Otto
Additional information:
Media: Poly / slide show
Bibliographical references:Poly de Mécanique des fluides non-newtoniens – Initiation à la rhéologie,
Guy Couarraze et Jean-Louis Grossiord, 3ième Editions, Editions TEC&DOC, 2000 Mécanique des fluides
appliquée, Régis JOULIE, Edition ellipses, 1998 –Mécanique et rhéologie des fluides en Génie chimique,
N. MIDOUX, Editions TEC&DOC -Lavoisier, 1993 - Delaplace G , Guerin R (2006) Mélange des produits
pâteux – Caractéristiques d’un système agité (eds) les Techniques de l’Ingénieur [F 3 350], Traité
Opérations unitaires - Génie de la réaction chimiques, 1-20
Publications of Delaplace et al. on rheology aspects in various chemical engineering journal
Assessment: test 1 Hour with documents and Calculator on applied problem
Remarks:
CI 3Y
MODULE : PROCESS OF THE FORMULATION ENGINEERING
SUBJECT:
MIXING: CHEMICAL ENGINEERING
Coordinator:
Jean-marie.aubry@ensc-
lille.fr
Tél 03 20 33 63 64
Office: bât. C6 R de C
Obligatoire
Code: OP3902-42
Semester: 9
Lecture: 10 Hours
Directed studies:
Language: French
Coefficient: 4
ECTS: 1
Instructor(s):
Delaplace Guillaume
Learning outcomes:
Students will be able: - to understand the major importance of the mixing operation in industry and the
aims of this operation to accelerate transport phenomena - to design adequate mixing equipments for
various media (solid/liquid, liquid, liquid/liquid, gas/liquid, solid/solid) - to understand how determining
predictive process relationship for controlling batch output - to understand scale up problem and rules
Prerequisite:
Introduction to rheology
Contents:
1. Introduction: the difficulties to design accurately a mixing operation
2. Reminder: Classification of fluid according to their rheological behavior.
3. Main goals of mixing operations in relation with physical properties of media
4. Technical aspects – various flows induced by impellers and design of a mixing equipment.
5. Analysis of transport phenomena in agitated tank: theory of similarity and dimensional analysis
6 Example: determination of process relationships for various mixing systems: power consumption,
mixing time, heat and mass transfer with Newtonian liquid
7. Tools to characterize mixing operation: CFD and velocimeter (LDA, PIV…).
8. scale up
9. Impact of rheological behavior on the mixing process.
10.Process relationships in agitated tank for dispersed systems (S/L, L/L, G/L)
Additional information:
Media: Poly & slideshow
Bibliographical references:
Thesis Henri Poincaré university Nancy I 1998 - Guillaume Delaplace - Agitation de fluides fortement
visqueux, Newtoniens ou non, par des agitateurs de proximité types ancre et rubans hélicoïdaux.
Delaplace G , Guerin R (2006) Mélange des produits pâteux – Caractéristiques d’un système agité (eds)
les Techniques de l’Ingénieur [F 3 350], Traité Opérations unitaires - Génie de la réaction chimiques, 1-
20 Delaplace G, Guerin R, (2006) Mélange des produits pâteux – Performances des agitateurs (eds) les
Techniques de l’Ingénieur [F 3 352], Traité Opérations unitaires - Génie de la réaction chimiques , 1-10
Jeantet Romain, Brulé Gérard, Delaplace Guillaume 2011 Génie Des Procédés Appliques A l'Industrie
Laitiere Editeur : Tec & Doc, 196 pages ISBN : 978-2-7430-1359-1
Publications of Delaplace et al. on mixing topic in various chemical engineering journal
Assessment: Test 1 H with documents and Calculator: assessment of expertise
Remarks:
CI 3Y
MODULE : EXPERIMENTAL PRACTICES
SUBJECT:
FORMULATION CHEMISTRY
Coordinator:
Jean-marie.aubry@ensc-
lille.fr
Tél +33(0)3 20 33 63 64
Building C6
Semi-optional
Code: OP3902-51
Semester: 9
Lecture:
Directed studies: 36 Hours
Language: French
Coefficient: 4
ECTS: 1
Instructor(s):
Christel Pierlot
Christel.pierlot@ensc-lille.fr
Tél : +33(0) 320 33 63 65
Building C6, Ground floor-
Office 21
Learning outcomes:
To give practical notions necessary to design, prepare and characterize complex mixtures encountered
in formulation and specialties industries.
Prerequisite:
Contents: classical formulation courses
Contents:
Aqueous micellar solutions
Emulsion Formulation
Emulsion and phase inversion temperature (PIT)
Formulation of a white acrylic paint
Formulation of an colored acrylic paint
Colored cement
Microemulsion and theory of HLD (Hypophilic Lipophilic Deviation)
Color measurement and design of experiments
Formulation of lipsticks
Rheology, texturing agents xanthan and caroub gum
Additional information:
Media: Distributed practical works fascicules
Bibliographical references: Techniques de l'ingénieur : Formulation - Présentation générale, Jean-Marie
AUBRY, Gilbert SCHORSCH, J2110 ( 1999).
Assessment: Distributed practical works fascicules to be completed
Remarks:
CI 3Y
MODULE : PRACTICAL STUDIES
SUBJECT:
PHYSICO-CHEMISTRY OFOLYMERS
Coordinator:
Jean-marie.aubry@ensc-
lille.fr
Tél +33(0)3 20 33 63 64
Building C6
Semi-optional
Code: OP3902-52
Semester: 9
Lecture: 9 Hours
Directed studies:
Language: French
Coefficient: 4
ECTS: 1
Instructor(s):
Frédéric CAZAUX
Frederic.cazaux@ensc-
lille.fr/+33(0)3 20 43 43
40/Building C6 -office 120
Learning outcomes:
To learn to manipulate tools allowing to characterize covers with paint: thickness, adhesion, shine,
color, covering power, stripe.
To know how to determine a Minimal Film Formation Temperature (MFFT) using a specific equipment.
To approach the rheology of paints.
To characterize paints by ThermoGravimetric Analysis.
Prerequisite:
Courts on the "formulation of paints and varnish" of 3rd year
Contents:
2 practicals by student:
- Rheologic characterization of a paint
- Determination of the Minimal Film Formation Temperature (MFFT) of a latex
- Characterization of covers with paint: thickness, adhesion, shine, color, covering power, stripe, …
- Characterization of a paint by ThermoGravimetric Analysis
Additional information:
Media: Duplicated lecture note of practical class
Bibliographical references:
Assessment: A report by practical
Remarks:
CI 3Y
MODULE : EXPERIMENTAL PRACTICES
SUBJECT:
COLLOIDAL PHYSICAL AND MICROFLUIDIC CHEMISTRY
Coordinator:
Jean-marie.aubry@ensc-
lille.fr
Tél +33(0)3 20 33 63 64
Building C6
Semi-optional
Code: OP3902-53
Semester: 9
Lecture:
Directed studies: 16 Hours
Language: French
Coefficient: 4
ECTS: 1
Instructor(s):
Valérie Molinier
Valerie.molinier@univ-lille1.fr
Tél : +33(0)3-20-33-63-66
Christel Pierlot
Christel.pierlot@ensc-lille.fr
Tél : +33(0)3-20-33-63-65
Building C6, ground floor
Learning outcomes:
Knowing how to use different devices in the formulation industry: tensiometer, laser particle size
analyzer, zetameter, device for stability of emulsions and suspensions measurements.
Analysis of the measured physicochemical data with these devices (critical micellar concentration,
particle size, stability ...).
Understand the complementarity of these analyzes and the link with the formulated
product (appearance, viscosity ...)
Prerequisite:
Contents:
Practical works of:
Molecular chemistry and formulation (ENSCL-S8)
Formulation chemistry (ENSCL-S9)
Contents:
The following operations will be performed:
Measurement of surface tension or interfacial using tensiometers (drop profile, ring,
plate, rotating drop and in dynamic mode).
Measurement of contact angle (advancing and receding)
Measure of the stability of an emulsion by transmission or scattering of light
Size measurement by laser granulometry, dynamic light scattering (DLS)
Zeta potential measurement
An important part will be devoted to analyzing the results
Additional information:
Media: Practical works fascicle
Bibliographical references:
Assessment: Submission of a report (or / and) Oral presentation
Remarks:
CI 3Y
MODULE : BEHAVIOUR OF MATERIALS
SUBJECT:
RELIABILITY AND DAMAGE OF MATERIALS
Coordinator:
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
Semi-optional
Code: OP3903-11
Semester: 9
Lecture: 20 Hours
Directed studies:
Language: French/English
Coefficient: 6
ECTS:
Instructor(s):
Jean-Bernard VOGT
Learning outcomes:
The objective of the lecture is to identify and to understand damage mechanisms of structural
materials (especially those employed in the chemical industry) that result from mechanical
solicitations and from environmental effect.
From this knowledge, the students will be able to run industrial plants with safety conditions or
will be able to conduct fracture and corrosion analysis.
Prerequisite:
Metallurgy, mechanical properties, corrosion, analytical chemistry
Contents:
influence of temperature and stress on the different kind of fracture (monotonic loading): cleavage, ductile rupture, creep type rupture, ruptures maps
fatigue fracture: initiation and propagation; stress response to strain cycling, fatigue resistance diagrams , dislocations structures,
extrusions-intrusions and microcrack initiation, classification and behaviour of short
cracks , long crack propagation, Crack growth rate regimes, crack tip plasticity , fatigue
crack closure
Environmentally-assisted fracture mechanisms: liquid metal embrittlement, hydrogen
embrittlement, stress corrosion cracking, corrosion – fatigue
Wear: erosion, abrasion, adhesion Non destructive evaluation
Additional information:
Media: photocopies of slide figures
Bibliographical references:
Mechanical behaviour of materials, Thomas H. Courtney, McGraw-Hill Publishing Company (1990)
Stress-Corrosion cracking : materials performance and evaluation, Russel H. Jones, ASM International (1992)
Solution to Hydrogen Attack in Steels, P.F. Timmins, ASM International (1997) Fatigue of Materials, S. Suresh, Cambridge University Press (1991)
Assessment:
Joint written exam with metallic alloys, all documents permitted, 2h
Remarks:
CI 3Y
MODULE : BEHAVIOUR OF MATERIALS
SUBJECT:
METALLIC ALLOYS
Coordinator:
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
Semi-optional
Code: OP3903-21
Semester: 9
Lecture: 20 Hours
Directed studies:
Language: French/English
Coefficient: 6
ECTS:
Instructor(s):
Jean-Bernard VOGT
Learning outcomes:
The objective of the lecture is to identify the main families of metallic alloys, monolithic or assembled, which exhibit a high resistance to mechanical loading and to corrosion. The student will be able to optimize the choice of a material regarding the application in the field of chemical industry, energy industry, transportation, bio medical …. This unit is in good interaction with the subject “Reliability and damage mechanisms of engineering
materials”
Prerequisite:
Contents: Metallurgy, mechanical properties, corrosion, analytical chemistry
Contents:
The lecture comprises two parts.
The first part is devoted the main families of metallic alloys resistant to corrosion and stresses:
Stainless steels Nickel alloys Zirconium alloys Shape memory alloys Aluminium alloys
The second part deals with the concept of multimaterials which consists in assembling materials
at different scales:
Multiphased steels
Composites materials
Welding
Metallic foam
Cladding
Additional information:
Media: photocopies of slide figures
Bibliographical references: Les aciers inoxydables, P. Lacombe, B. Baroux, G. Béranger, Les éditions de physique (1990)
Le zirconium, G. Béranger, P. Lacombe, R. Tricot, Les éditions de physique (1990)
Matériaux industriels-matériaux métalliques, M. Colombié et coll., Dunod (2000)
Assessment:
Joint written exam with reliability and damage mechanism of structural alloys, all documents
permitted, 2h
Remarks:
CI 3Y
MODULE : MATERIALS SOLUTIONS
SUBJECT:
POWDER TECHNOLOGY AND SHAPING
Coordinator:
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
Obligatoire
Code: OP3903-22
Semester: 9
Lecture: 20 Hours
Directed studies:
Language: French/English
Coefficient: 6
ECTS: 2
Instructor(s):
Nouria Fatah
Learning outcomes:
The lectures on powder technology and coating within the “Ecole Nationale Supérieure de Chimie de Lille” covers the study of the physical properties: theory and the measurement techniques on sampling, porosity, real and apparent densities, particle size analysis (technique of diffraction and diffusion, image processing, sieving), definition of size and average diameters of particles, specific surface area, the shape factor, the phenomenon of agglomeration and flow behaviour in the system and their impact on the conception and the calculation of coating properties.
This course treats cohesive and non cohesive powders by showing the importance of interaction forces (Van Der Waals, electrostatic and capillary forces), the influence of the phenomenon of agglomeration, distribution of the strain within a powder and the different tests measurements of the powders flows properties such as the shearing cell, the tapping, the angle of slope, the angle of repose, the floodability and the consolidation.
This course presents the techniques and development of coating technology according to four systems: agitation, dispersion, consolidation and thermal system. The processes like the mixing granulator, spray-drying, prilling, sintering, mécanosynthèse and mécanofusion will be studied.
The teaching of the powders must be accompanied by selection of problems with numerical
calculations is proposed to illustrate the importance of the choice of the coating process and powder
technology.
Prerequisite:
heat transfer, mass transfer, fluids mechanics, solids physicals
Contents:
- Introduction: Particle technology - Particle Characterization and measurement - Fondamental properties of particle - Coating technology: objectives and products forms - Process and equipment - Applications
Additional information:
Media: copy of slides presentation
Bibliographical references:
M. RHODES, « PRINCIPLES OF POWDER TECHNOLOGY », John Wiley and Sons, 1990
Assessment: written exam
Remarks:
CI 3Y
MODULE : SOLUTIONS MATERIALS
SUBJECT:
SURFACE TREATMENT
Coordinator:
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
Semi-optional
Code: OP3903-23
Semester: 9
Lecture: 15 Hours
Directed studies:
Language: French/English
Coefficient: 5
ECTS: 2
Instructor(s):
Charlotte Becquart
Charlotte.becquart@ensc-
lille.fr, Building C6. Office 217
Tel +33(0)3 20 43 49 44
Learning outcomes:
At the end of the module, the students should have a good knowledge of the physical basis as well the technologies used in the different surface treatments that exist. Prerequisite:
2nd
year lectures in material science, in particular, the corrosion lecture
Contents: The purpose of this course is introducing the students to the various methods, physical,
mechanical, or electrochemical, which can be used to modify a materials’ surface. Most of the time,
these treatments aim at protecting the material from an external attack, however they can have other
purposes : increase wear, erosion or friction resistance, electrical properties modifications, optical
properties modifications...In a first part, the course presents what is a surface, which processes can be
responsible for its degradation, which methods can be used to improve the surface properties, what
are pre-treatments, what are the methods which can be used to characterize the surface.
In a second part, some of the most commonly used processes are studied in more details : Physical
Vapour Deposition (PVD) and Chemical Vapour Deposition (CVD), thermochemical treatments,
galvanization, ion Implantation, mechanical treatments ... This second part is done in the form of oral
reports prepared by the students from lecture material given by the instructor.
Additional information:
Media: copy of the slides
Bibliographical references: 1/ -Y. Adda, J.M. Dupouy, J. Philibert et Y. Quéré, Eléments de Métallurgie
Physique, Vol.6, INSTN, CEA, collection enseignement 2/ -S. Audisio, M. Cailler, A. Galerie et H. Mazille,
Traitements de Surface et Protection contre la Corrosion, Ecole d'été, Aussois 1987, les éditions de
physique. 3/ -Manuel des traitements de surface à l'usage des bureaux d'études, Club des traitements
de surface, CETIM. 4/ -J. Barralis et G. Maeder, Métallurgie, Tome 2: alliages ferreux, ENSAM (1983),
Editions communications actives, ISBN 2 85932 004. 5 / -Groupe de recherches sur l'usure des
matériaux industriels, Organisation de Coopération et de Développements Economiques, Glossaire des
termes et définitions dans le domaine du frottement, de l'usure et de la lubrification (tribologie). 6/ Le
livre de l'acier, éditeurs Gérard Béranger, Guy Henry, Germain Sanz (1994) 7/ -Principes de base du
traitement thermique, Pyc édition, Publications Yves Colombot. 8/ -Advances of surface treatments,
Proceedings of the AST World Conference Advances in Surface Treatments and Surface finishing (Paris
1986), A. Niku-Lari director, volume 5, Pergamon Press 9/ Surface Treatments for Improved
Performance and Properties, Edited by J.J. Burje and V. Weiss, Plenum Press, New York and London
(1982) 10/ -Friction and Wear, A.D. Sarkar, Academic Press, a Subsidiary of Harcourt Brace Jovanovitch,
Publishers, London . New York . Toronto . Sydney . San Fransisco (1980) 11/ -Tribology: Principles and
Design Applications, R. D. Arnell, P.B. Davies, J. Halling and T.L. Whomes, Published by Macmillan
Education Ltd (1991) 12/ -Surface Engineering, Edited by S.A. Meguid, Elsevier Applied Science, London
and New York (1990) 13/ -Théorie et pratique industrielle du frottement, J.J. Caubet, Technip Paris,
Dunod Paris (1964) 14/ -Matériaux : propriétés et applications, M.F. Ashby et D.R. Jones, Dunod Paris
1996 15/ -Articles divers dans "Traitement Thermique", "Galvano-Organo-Traitement de Surface",
"News on Coatings and Corrosion", "Annual Review of Material Science", "Journal of Metals", "MRS
Bulletin". 16/ -Les Aciers, Ben Simon, Pyc-édition, cours professé au C.E.S.T.O 17/ -Principles of the
surface treatments of steels, C.R. Brooks, Technomic publishing Co. Inc. Lancaster Basel
Assessment: The students will prepare a one hour lecture on one of the surface treatments by groups
of 2 and with documents provided by the instructorer
Remarks:
CI 3Y
MODULE : SOLUTIONS MATERIALS
SUBJECT:
GLASSES
Coordinator:
Jean Bernard Vogt
jean-bernard.vogt@ensc-
lille.fr
Phone : (+33) 03 20 43 40 35
Building C6 – room 223
Semi-optional
Code: OP3903-24
Semester: 9
Lecture: 10 Hours
Directed studies:
Language: French
Coefficient:
ECTS:
Instructor(s):
Nathalie TANCRET
nathalie.tancret@ensc-lille.fr
Phone : (+33) 03 20 33 64 35
Learning outcomes:
Know the glassy state, the chemical compounds capable of forming a glass and the rules governing the formation.
Know the role of modifier ions, in particular, the “mixed-alkali effect” and its impact on the glass properties: viscosity, thermal expansion coefficient, conductivity.
Know to look for information on a topic related to the glass industry, synthesize and report to a non-specialist audience.
Prerequisite:
Basics of Inorganic Chemistry, S7 course "Introduction to Materials", Part glass and ceramics, S8 course
"ceramics and glass" part on glasses, Notions of physical properties, Know how to conduct a
bibliographic research.
Contents:
The aim of this course is to deepen the notions viewed in the course "ceramics and glass" (S8), only the
part related to glasses. This teaching is divided into two parts:
1. a first in authoritarian pedagogy, provided by the teacher, which outlines the glassy state, formation,
why and how, the role of modifying oxides and their influence on the physical properties of the
manufactured glass.
2. a second part, participatory pedagogy, conducted by the students themselves in the form of
presentations, 1/2 hour group on a subject of their choice among the various concrete problems
related to the field of glass: the special role boron and its future replacement by other ions (REACH),
bubble problem in the manufacturing process, reducing emissions of pollutants out of glass factory
chimneys, forming, cutting of flat glass, ...
Additional information:
Bibliographical references:
Le verre, science et technologie, James Barton et Claude Guillemet, EDP Sciences (Les Ulis, 2005)
Introduction to glass science and technology, 2nd edition, James E. Shelby, The Royal Society of Chemistry (RSC) (Cambridge, 2009)
Assessment: Oral presentation in groups of 3 students, based on a summary of real cases
Remarks:
CI 3Y
MODULE : METHODS OF ANALYSIS
SUBJECT:
NUMERICAL TOOL FOR MATERIAL SELECTION
Coordinator:
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
Semi-optional
Code: OP3903-31
Semester: 9
Lecture: 4 Hours
Directed studies: 4 Hours
Language: French/English
Coefficient: 3
ECTS:
Instructor(s):
Charlotte Becquart
Charlotte.becquart@ensc-
lille.fr, Building C6. Office 217
Tel +33(0)3 20 43 49 44
Learning outcomes:
At the end of the class, the student should know how to write specifications as well as how to use CES
to chose the appropriate material for a given use.
Prerequisite:
Materials science, mechanical properties, reliability of materials, corrosion
Contents: the purpose of this lecture is to show the students how the software CES can be used to assist them in selecting a material for a given application.
-Introduction: designing a component implies 3 problems which are not independent: (i) selecting the materials, (ii) selecting the shape, and (iii) selecting the process to make the component. Writing the specifications is difficult as some criteria are hard to quantify (aesthetics …) and as there exists an hyper choice of materials and processes. - Materials: the four families
- Properties
- Shaping processes - Material indices.
What is a material index ? How do we determine a material index? case studies (CES selector)
Additional information:
Media: copy of the slides
Bibliographical references:
“Materials selection in Mechanical Design”, M.F. Ashby, Butterworth et Heinemann
“Matériaux : propriétés et applications”, M.F. Ashby et D.R. Jones, Dunod Paris 1996
Assessment: written report
Remarks:
CI 3Y
MODULE : METHODS OF ANALYSIS
SUBJECT:
PRACTICAL USE OF THE METHOD OF FINITE ELEMENTS METHODS
Coordinator:
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
Semi-optional
Code: OP3903-32
Semester: 9
Lecture: 10 Hours
Directed studies: 5 Hours
Language: French/English
Coefficient: 4
ECTS: 1
Instructor(s):
Jérémie BOUQUEREL
Maître de Conférences
jbouquerel@ensc-lille.fr
+33(0)3.20.43.42.29
Learning outcomes:
The objective of the course is to describe the use of the Finite Element Method (FEM) when predicting the behaviour of a component. The student will learn how to solve a problem with the FEM technique and make use of a FEM based
software
Prerequisite:
General knowledge in physics and in materials science
Contents:
1- Introduction
Positioning the FEM method when simulating the components behaviour
Introducing to the main numerical tools used in the industry
2- Application example : solving a problem with the FEM technique (selecting the
correct laws, discretization, boundary conditions, nodal approximation, finite
element concept, numerical solving, post-processing)
3- Training - applications :
Use of a FEM based software (RDM6 / Abaqus®)
Determining the behaviour of a material submitted to thermo-mechanical
constraints
Additional information:
Media:
Bibliographical references:
Introduction to Computational Plasticity, F. Dunne, N. Petrinic, Oxford University Press (2005)
Assessment:
Remarks:
No specific exam
CI 3Y
MODULE : METHODS OF ANALYSIS
SUBJECT:
TECHNIQUES OF CONVENTIONAL ANALYSES
Coordinator:
Jean-Bernard VOGT
Jean-bernard.vogt@ensc-
lille.fr
+33 (0)3 20 43 40 35
Building C6 -office 223
Semi-optional
Code: OP3903-32
Semester: 9
Lecture: 10 Hours
Directed studies: 5 Hours
Language: French
Coefficient: 4
ECTS: 1
Instructor(s):
Jérémie BOUQUEREL
(contact), assistant
professor
Séverine BELLAYER,
research engineer
Anne-Sophie MAMEDE,
assistant professor
Learning outcomes:
• The objective of the course is to describe the modern investigation techniques of materials
microstructure.
• The student will be able to assign the most suitable tool to be used to solve a problem of
material identification
Prerequisite:
General knowledge in physics, in analytical chemistry, in crystallography and in materials
Contents:
At first, physical phenomenons which are on the basis of the techniques are explained as well as a
description of their experimental procedure.
Then, technical sessions are organized in front of each equipment where the student can appreciate
the technique with an expert. The following techniques are considered:
Scanning electron microscopy (SEM),
Energy Dispersive X-ray Spectroscopy (EDX)
Electron Back Scattered diffraction (EBSD)
Transmission Electron Microscopy (TEM)
Atomic force Microscopy (AFM)
X-Ray Photoelectron Spectroscopy (XPS).
The technical sessions take place in laboratories of ENSCL, UCCS and UMET, for which the expertise is
largely recognized.
UCCS : Unité de Catalyse et Chimie du Solide
UMET : Unité Matériaux Et Transformations
Additional information:
Media:
Bibliographical references:
Méthodes usuelles de caractérisation des surfaces, D. David, R. Caplain, Eyrolles (1988)
Microcaractérisation des solides, M. Ammou, CRAM-LPSES-CNRS (1989) Assessment:
Remarks:
No specific exam
CI 3Y
MODULE : QUALITY, HEALTH, SAFETY
SUBJECT:
SUSTAINABLE DEVELOPMENT
Coordinator:
Jean Claude van Duysen
Jean-claude.van-
duysen@edf.com
Tel : 06 82 80 89 33
Compulsory
Code: FE3901-1
Semester: 9
Lecture: 10 Hours
Directed studies:
Language: French
Coefficient: 1
ECTS:
Instructor(s):
Jean Claude van Duysen
Learning outcomes:
The course has for objectives 1) to explain how the principles of sustainable development can be implemented in the industrial world and 2) to show the benefits of this implementation. At the end of the course, students will understand that sustainable development can be a mainspring
of growth for the industry, and will be able to define the outlines of a sustainable development policy
at the enterprise level.
Prerequisite:
The only prerequisite is to have mastered the concepts presented in the first year course on the fundamentals and indicators of sustainable development.
Contents:
The course is made of four parts
Reminder on sustainable development principles,
Sustainable development: a mainspring of growth for the industry,
Examples of application of sustainable development principles in industry,
Two ambitious concepts "zero CO2" factory and "ecofriendly" factory.
Additional information:
Support :
Regular reading of a daily newspaper or a societal magazine..
Bibliographical references :
J. C. van Duysen et Stéphanie Jumel, le Développement Durable, éditions l’Hamarttan, 2008. PME et développement durable :
http://ressources-rse.org/assets/files/1_RSE/1_1OUVRAGES/guide_pme_DD%20CCI.pdf
Guide du Développement Durable : http://publications.medef.com/guide/Entreprises-et-DD.pdf
Assessment method : assessment is based on mini-projects conducted in groups of two or three
students on a theme related to sustainable development. Each group gives a 4 to 5 page report which is
graded.
Remarks:
CI 3Y
MODULE : QUALITY, HEALTH, SAFETY
SUBJECT:
INDUSTRIAL SECURITY
Coordinator:
Serge.bourbigot@ensc-lille.fr
/ +33(0)3.20.43.48.88/ office
N°8
Compulsory
Code: FE3901-2
Semester: 9
Lecture: 20 Hours
Directed studies:
Language: French
Coefficient:
ECTS:
Instructor(s):
Serge.bourbigot@ensc-lille.fr
/ +33(0)3.20.43.48.88/
officeN°8
+ External speakers who are
experts in different fields of
safety of the industry - As an
example, IRSN - Auchan -
Univ. Haute Alsace - CREPIM -
Gendarmerie have given talks
in 2011/2012
Learning outcomes:
To learn safety applied to the industry and to learn how to quantify hazards
Prerequisite:
Chemical engineering at the undergraduate level Contents:
Survey of safety in the industry
Hazard process
Proportioning of safety valve
Atmospheric dispersion
Combustions – explosions
Dust explosions
Safety Controls for Chemical Reaction Hazards
Domino effect
Additional information:
Media: Powerpoint
Bibliographical references: Sécurité des procédés chimiques : Connaissances de base et méthode
d'analyse de risques by A. Laurent
Assessment: Project
Remarks:
CI 3Y
MODULE : ENGLISH
SUBJECT:
ENGLISH
Coordinator:
Anne GUEGAND
Abdelamar BENAÏSSA
office 965
Tel:+33(0)320336060
Compulsory
Code: LV3901
Semester: 9
Lecture:
Directed studies: 30 Hours
Language: English
Coefficient: 6
ECTS:
Instructor(s):
Anne GUEGAND
Abdelamar BENAÏSSA
Learning outcomes:
Language tuition at the ENSCL has a double objective:
-To help all students develop the communication skills they will need in professional situations through
interactive practice activities.
- To encourage prospective graduates to develop an international opening onto foreign companies and
universities to facilitate cross-cultural adaptability and adaptation.
Contents:
Professional Presentation Skills (presenting one's company, presenting a project, presenting one's research…)
Additional information:
Media: Various (newspaper articles, publications, video documents, case studies…)
Assessment: Continuous language assessment is carried out through one written test and a
presentation in English.
Remarks:
No English course for beginners
CI 3Y
MODULE : GERMAN
SUBJECT:
GERMAN
Coordinator:
Beate WINKLER
beate.winkler@ensc-lille.fr
Tel. +33(0)320336061
office 951
Compulsory
Code: LV3902
Semester: 9
Lecture:
Directed studies: 30 Hours
Language: German
Coefficient: 6
ECTS:
Instructor(s):
Beate WINKLER
Monika BERTOUT
Learning outcomes:
Prerequisites:
All levels.
Objectives and skills referred:
Progress in the four language skills, but especially in oral expression.
Ability to integrate in a professional environment (with regard to courses and internships at University
or in foreign companies) and to communicate in situations of everyday life.
Consolidation of knowledge of scientific and technical German in the field of chemistry
Contents:
Non-exhaustive list - all aspects are not always treated and some contents of CI 2Y may be continued. The company (continuation): business German; overview of companies in the various areas of chemistry.
Current news in the fields of chemistry, economy and politics - (mainly oral expression: presentations
and debates)
Additional information:
Media:
Various authentic media (print media, audio, video, movies, business documents, the internet).
Bibliographical references:
Books, movies in original version and journals are available on loan in a small German library.
Assessment:
Continuous language assessment is carried out through one written test (two hours) and at least one
oral test divided into two parts (a presentation and an interactive part).
Remarks:
Students who started learning German in the first year of CI 1Y are strongly encouraged to confirm
their level by a certification in cooperation with the Goethe-Institute:
"Zertifikat Start 2" (level A2 of the CEFR).
CI 3Y
MODULE : SPANISH
SUBJECT:
SPANISH
Coordinator:
Larabi Hakima
Compulsory
Code: LV3906
Semester: 9
Lecture:
Directed studies: 30 Hours
Language: Spanish
Coefficient: 6
ECTS:
Instructor(s):
Larabi Hakima
Learning outcomes:
Strengthening B2 level of the Frame Common reference European for Languages, preparation at C1
level. At the end of the third year, the student must have strung the level of the autonomous speaker.
Helping all students develop the condition skills they will need in professional situations (through
interactive practice activities).
Contents:
Linguistic, scientific and cultural aspects:
- Oral comprehension: multimedia language laboratory or video sequence.
- Oral expression: simulations and role play activities, to assess a situation, writing report, professional
project; managing a team; job and apparitional interviews.
- L’entretien d’embauche (les métiers de la chimie…)
- Written comprehension: scientific or cultural texts.
- Written grammatical competences.
- Written expression (writing an informal or definite letter, a dialogue…)
- Approfondir les connaissances: organiser une campagne de sensibilisation sécurité/environnement…).
Additional information:
Media: Various (Newspaper articles, audio and video documents…).
Bibliographical references: Marco Común Europeo C1.
Assessment: Continuous language assesment is carried out through a written test, an interview and a
presentation in spanish.
Remarks:
No Spanish course for beginners.
CI 3Y
MODULE : JAPANESE
SUBJECT:
JAPANESE
Coordinator:
Jean-Luc RIGAL
Jean-luc.rigal@enscl-lille.fr
Office 951
Optional
Code: LV3904
Semester: 9
Lecture:
Directed studies: 30 Hours
Language: Japanese
Coefficient:
ECTS:
Instructor(s):
Geoffrey DUCATILLON 1 2
Hitomi KIMURA 3
Aki KIUCHI 1
Nozomu MIZUKAMI 2
Shoko MORITA 4 5
Jean-Luc RIGAL 1 2 3
Maki TAMAOKI 1
Sachie WATANABE 2
Learning outcomes:
The main object of this course is to give basic communication tools to the students who intend to do
their first, second or/and third year industrial placements in Japan, but also to complete the curriculum
of future managers of a branch of industry which has many relations with Japan.
Contents:
One third of the course is devoted to civilization and two thirds to language. Because of the very
particular writing system of Japanese, in which two syllabaries and at least 2000 ideograms are
combined, reading and writing are given the same importance as oral work. In addition to the learning
and systematic use of the two syllabaries, strong emphasis is put on the logic of ideograms, the
objective being, through the study of a few hundreds of them, to facilitate the subsequent assimilation
of those - much more numerous - which are necessary to everyday life.
Level 3: In particular, Nihongo shoho 14-21, Bushu 101-214 , and a tale from the Meisaku anime
ehon series.
Additional information:
Media: Minna no nihongo, Nihongo shoho (1, 2, 3), Nihongo chûkyû, Kana nyûmon (hiragana 1)
(katakana 2), Nelson Kan’ei jiten (2, 3)
Bibliographical references: Nihon etoki jiten 1-16 (JTB), Nihongo notes 1-5 (The Japan Times),
Situational Japanese 1-5 (The Japan Times)
Assessment: oral and written exams, continuous assessment
Remarks:
The course is divided into 5 levels, and not according to the three years of the curriculum. As a matter
of fact, if Level I is mainly attended by first year students, Level II by second year students and Level III
by third year students, some students start the study of Japanese in their second/third year, whereas
other students - especially those who come from the "CPI" - may have been studying Japanese for two
years or more when they start their engineering studies.
Prerequisites: None, other than the desire to learn Japanese (WRITTEN INCLUDED)
CI 3Y
Recommended