AAnalyst 200 User’s Guide - 國立臺灣大學 200 .pdf · AAnalyst 200 User’s Guide 2-3 Chapter…

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  • AAnalyst 200 Users Guide

  • Release History

    Part Number Release Publication Date

    0993 6594 E April 2006

    Any comments about the documentation for this product should be addressed to: User Assistance PerkinElmer, Inc. 710 Bridgeport Avenue Shelton, Connecticut 06484-4794 U.S.A. Or emailed to: info@perkinelmer.com Notices The information contained in this document is subject to change without notice. Except as specifically set forth in its terms and conditions of sale, PerkinElmer makes no warranty of any kind with regard to this document, including, but not limited to, the implied warranties of merchantability and fitness for a particular purpose. PerkinElmer shall not be liable for errors contained herein for incidental consequential damages in connection with furnishing, performance or use of this material. Copyright Information This document contains proprietary information that is protected by copyright. All rights are reserved. No part of this publication may be reproduced in any form whatsoever or translated into any language without the prior, written permission of PerkinElmer, Inc. Copyright 2006 PerkinElmer, Inc. Trademarks Registered names, trademarks, etc. used in this document, even when not specifically marked as such, are protected by law. PerkinElmer is a registered trademark of PerkinElmer, Inc. AAnalysts and e-ssentials are trademarks of PerkinElmer, Inc.

  • Table of Contents Chapter 1 Introduction About This Manual...................................................................................... 1-3 Conventions Used in this Manual................................................................ 1-5 Warning Labels on the Instrument .............................................................. 1-6 Chapter 2 Safety Practices Chapter Overview........................................................................................ 2-3 Working Safely with the AAnalyst 200 ...................................................... 2-4 Precautions .................................................................................................. 2-5 Hazards with Flame Atomization................................................................ 2-6 Safety Conventions in the Hardware Guide ................................................ 2-8 Symbols Used on the Instrument................................................................. 2-9 Safety Practices for Flame Atomization.................................................... 2-10 High Temperatures .................................................................................... 2-12 Electrical Safety ........................................................................................ 2-13 Compressed Gases..................................................................................... 2-14 Safe Handling of Gas Cylinders ................................................................ 2-15 Operating Conditions ................................................................................ 2-18 Exhaust Venting ........................................................................................ 2-19 Safe Handling of Chemicals...................................................................... 2-20 Decontamination ....................................................................................... 2-21 Waste Disposal .......................................................................................... 2-22 Electromagnetic Compatibility (EMC) ..................................................... 2-23 WEEE Instructions for PerkinElmer Products .......................................... 2-24 References for Laboratory Safety Practice................................................ 2-25 Chapter 3 Preparing Your Laboratory Introduction ................................................................................................. 3-3 Environmental Conditions........................................................................... 3-4 General Laboratory Requirements .............................................................. 3-5 Location and Space Requirements .............................................................. 3-7 Exhaust Vent Requirements ...................................................................... 3-12 Electrical Requirements ............................................................................ 3-20 Lamps ........................................................................................................ 3-21 Chapter 4 System Description Introduction ................................................................................................. 4-3 AAnalyst 200 Overview.............................................................................. 4-4 The AAnalyst 200 Spectrometer System .................................................... 4-5 General Lamp Information .......................................................................... 4-6 The Deuterium Arc Background Corrector ............................................... 4-11 The Burner System.................................................................................... 4-12 Connecting the Electrical Supply .............................................................. 4-19 Mercury/Hydride Determination System (MHS-15)................................. 4-21

  • Chapter 5 Installation Introduction to the Installation Procedure ................................................... 5-3 When the Spectrometer Arrives .................................................................. 5-4 Placing the Spectrometer on the Bench....................................................... 5-6 AAnalyst 200 Shipping List ........................................................................ 5-8 AAnalyst 200 Spares Kit ............................................................................. 5-9 Installing the Touch Screen ....................................................................... 5-10 Connecting the Gas Hoses......................................................................... 5-14 Setting up the Burner System.................................................................... 5-19 Installing the Burner Door......................................................................... 5-21 Installing the Sample Tray......................................................................... 5-22 Connecting to the Electrical Supply .......................................................... 5-23 Switches and Connectors on the E-Box .................................................... 5-24 Setting Up the AutoSampler...................................................................... 5-25 Connecting the Foot Switch ...................................................................... 5-26 Chapter 6 Operation of Instrument Starting up the System................................................................................. 6-3 Setting up the Burner System...................................................................... 6-5 Installing Solvent-Resistant Components in the Burner............................ 6-11 User Interface ............................................................................................ 6-19 Installing Lamps ........................................................................................ 6-21 Switching on the Spectrometer.................................................................. 6-25 Safety Checks ............................................................................................ 6-26 Using the Background Corrector............................................................... 6-27 Optimization Procedures ........................................................................... 6-28 Aligning Lamp .......................................................................................... 6-29 Setting the Burner Height.......................................................................... 6-33 Igniting the Flame ..................................................................................... 6-35 Preadjusting the Nebulizer ........................................................................ 6-37 Optimizing the Burner System .................................................................. 6-39 Rinsing the Burner System........................................................................ 6-43 Chapter 7 Touch Screen User Interface .............................................................................................. 7-3 Startup Dialog.............................................................................................. 7-5 Lamp Page................................................................................................... 7-6 Flame page ................................................................................................ 7-11 Parameters Page ........................................................................................ 7-14 Analyze Page: Manual Data Display......................................................... 7-20 Analyze Samples Page: Manual Continuous Display ............................... 7-23 Analyze Page: Autosampler ...................................................................... 7-25 Tools Dialog .............................................................................................. 7-27 Recommended Conditions......................................................................... 7-31 Network Dialog ......................................................................................... 7-32 Download .................................................................................................. 7-41 Importing AAnalyst 200 into Microsoft Excel.......................................... 7-47

  • Chapter 8 Analyzing Samples Sequence of Operations.........................................