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    O R I G I N A L A R T I C L E

    Influence of soil grading on the characteristics of cement

    stabilised soil compacts

    B. V. Venkatarama Reddy M. S. Latha

    Received: 6 December 2012 / Accepted: 9 July 2013 / Published online: 19 July 2013

    RILEM 2013

    Abstract The paper deals with experimental inves-

    tigations aiming at specifying optimum soil grading

    limits for the production of cement stabilised soil

    bricks (CSSB). Wide range of soil grading curves

    encompassing both fine and coarse grained soils were

    considered. Strength, durability and absorption char-

    acteristics of CSSB were examined considering 14

    different types of soil grading curves and three cement

    contents. The investigations show that there is opti-

    mum clay content for the soil mix which yields

    maximum compressive strength for CSSB and theoptimum clay content is about 10 and 14 % for fine

    grained and coarse grained soils respectively. Void

    ratio of the compacted specimens is the lowest at the

    optimum clay content and therefore possesses maxi-

    mum strength at that point. CSSB using fine grained

    soils shows higher strength and better durability

    characteristics when compared to the bricks using

    coarse grained soils.

    Keywords Cement stabilisation Stabilised

    soil brick

    Soilcement

    Compressive strength

    Optimum clay content

    1 Introduction and scope of the investigation

    Stabilised soils find applications in the construc-

    tion of roads and buildings. Since the last 67

    decades stabilised soils are being exploited for the

    construction of structural components of buildings

    and other structures. Stabilised soil blocks (SSB)

    and stabilised rammed earth represent the two

    forms of compacted stabilised soil used for the

    structural applications in buildings. Manufacture of

    SSB involves compaction of the processed soilmixed with stabiliser (such as cement) at optimum

    moisture into a dense block. Cement stabilised soil

    brick (CSSB) is energy efficient and low embod-

    ied carbon material [13]. CSSB has been used for

    load bearing masonry buildings across the world

    [410]. The characteristics of CSSB are influenced

    by the cement content, brick density, soil grading,

    and type and percentage of clay mineral in the soil

    [2, 1116]. Cement stabilisation is ideally suited

    for coarse grained sandy soils with non-expansive

    clay minerals [9, 13, 1719] and hence the bestresults for CSSB are obtained when such soils are

    used. Major challenge in the production of CSSB

    is in specifying the optimum soil grading limits

    which will yield maximum strength and durability

    characteristics for the brick. A brief review of the

    literature on influence of soil composition/grading

    on characteristics of CSSB is as follows.

    Investigations by Mitra [17] revealed that soils

    containing high silt and clay fractions are not suitable

    B. V. Venkatarama Reddy (&) M. S. Latha

    Department of Civil Engineering, Indian Institute of

    Science, Bangalore 560012, India

    e-mail: [email protected]

    M. S. Latha

    e-mail: [email protected]

    Materials and Structures (2014) 47:16331645

    DOI 10.1617/s11527-013-0142-1

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    for CSSB production. This study emphasised the use

    of sandy soils for CSSB in order to achieve satisfac-

    tory strength and durability characteristics. Fitzmau-

    rice [4] conducted tests on machine pressed CSSB. His

    studies revealed that the soils with low clay fraction

    and high sand/gravel fraction are best suited for CSSB.

    Importance of soils with high sand content wasemphasised in the investigations of Dietz [20] and

    Bokhari [21]. Olivier and Ali [11] conducted detailed

    investigations in understanding the role of soil grading

    on the strength of CSSB and concluded that the CSSB

    with 70 % sand and 20 % clay gives maximum

    strength.

    Reddy and Jagadish [22] examined the influence of

    soil composition (using coarse grained soils) on the

    strength and durability of CSSB. They concluded that

    soils with non-expansive clay minerals having sand

    content of 70 5 % and clay content of\15 % yieldmaximum strength for CSSB. Walker and Stace [12]

    investigated the properties of CSSB using a number of

    reconstituted coarse grained soils with different soil

    grading limits. They noticed considerable decrease in

    strength and increased mass loss in the durability test

    as the clay content of the mix was increased. The

    findings showed that for cement contents of 5 and

    10 %, soils with 15 and 30 % clay are best suited.

    Reddy and Walker [23] examined the strength and

    durability characteristics of CSSB and recommend an

    optimum clay content of 1012 %.Houben and Guillaud [9] recommend gravely sand

    than silty clay soils for CSSB production. Consoli

    et al. [14] determined unconfined compressive

    strength of soilcement cylindrical specimens consid-

    ering a range of density and cement contents. They

    concluded that strength is sensitive to the density of

    the specimen, and the effectiveness of cement is

    greater in high density specimen. Reddy et al. [15]

    made a comprehensive study on arriving at optimum

    soil grading limits for the manufacture of CSSB

    considering both strength and durability characterises.A coarse grained soil was considered and it was

    reconstituted by diluting with sand in order to vary the

    soil grading. CSSBs prepared using the natural soil

    and reconstituted soils were examined for strength,

    durability and bond characteristics. The study con-

    cludes that 16 % clay fraction in the mix yields

    maximum strength with good durability characteris-

    tics for CSSB. Reasons for the optimum clay content

    of 16 % are not stated.

    Considering Unified Soil Classification (USC)

    system the soils can be broadly classified into two

    groups: (1) Coarse grained soils and (2) Fine grained

    soils. Both of these soil types can be used for the

    production of CSSB. The gaps found in the literature

    for recommending optimum soil grading limits for the

    CSSB production are as follows.

    (a) There are only limited studies which attempt to

    specify the exact soil grading limits for CSSB

    manufacture. These studies specify optimum

    clay fraction for only coarse grained soils,

    (b) The reasons for the optimum clay fraction

    yielding maximum strength are not discussed.

    (c) There are no attempts to specify optimum

    grading limits considering fine grained soils

    (especially soils with high silt fraction) for the

    production of CSSB.The present investigation is aimed at understanding

    the influence of clay and silt size fractions of both

    coarse grained and fine grained soils on strength and

    durability characteristics of CSSB, and to arrive at

    optimum soil grading limits considering wide range of

    soil grading limits. Gradation of a natural soil with

    31.6 % clay fraction was varied by reconstituting it

    with sand and silt size fractions to obtain wide range of

    grading limits representing both coarse and fine

    grained soils. Strength characteristics were examined

    by testing small cylindrical specimen, while thedurability characteristics were examined by testing

    CSSB bricks. Cement content used (by the industry)

    for the CSSB production is in the range of 610 %.

    Therefore, in the present study three cement contents

    (4, 7 and 10 % by weight) were considered.

    2 Materials used in the study

    2.1 Natural soil

    Locally available red soil was used in the experimental

    studies. Figure1 shows the grain size distribution

    curve for the soil and Table2gives various charac-

    teristics of the soil. Figure2shows the XRD analysis

    for the soil. The soil has 31.6, 18.1 and 50.3 % clay,

    silt and sand size fractions respectively. The soil

    contains predominantly kaolinite clay mineral. The

    liquid limit, plasticity index and shrinkage limit values

    for the soil is 40, 21 and 14 %, respectively. The soil is

    1634 Materials and Structures (2014) 47:16331645

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    a coarse grained soil belonging to class SC in USC

    system.

    2.2 Sand and silt

    Natural river sand was used in the investigations,

    whose grain size distribution curve is shown in Fig. 1.Also, the grain size distribution curve for the silt is

    shown in Fig. 1. The silt was obtained by sieving

    (washing) manufactured sand through 0.075 mm

    sieve.

    2.3 Reconstituted soils

    The natural red soil was reconstituted by mixing

    different percentages of sand and silt, and the details of

    the mix proportions along with the designation of the

    mix are given in Table1. Grain size distributioncurves of reconstituted soils are displayed in Fig.1.

    The properties of reconstituted soil mixtures are given

    in Table2. Totally 14 different soil variants were

    generated representing wide range of grain size

    distributions representing both coarse and fine grained

    soils. The clay, silt and sand fractions of the 14 soil

    samples vary over wide limits (clay: 4.531.6 %; silt:

    4.888.3 %; sand: 7.287.3 %). Also, the Atterbergs

    limits of the natural soil and its reconstituted variants

    vary over a wide range (Liquid limit: 23.740 %;

    Plasticity Index: 9.621; shrinkage limit: 1.6214 %).

    2.4 Cement

    Ordinary Portland cement conforming to IS 8112 [24]

    code was used in the manufacture of CSSB and

    cylindrical specimens. The cement composition: Alu-

    mina iron ratio of 1, Magnesium oxide 1.4 %,

    Sulphuric anhydride 1.9 %, Alkalies 0.6 % and Chlo-rides 0.01 %. The initial setting time of the cement

    was 46 min and the mean 28 day compressive strength

    of 50.7 MPa.

    3 Casting test specimens and testing procedure

    3.1 Casting specimens

    Strength of compacted cement stabilised soils were

    examined through the compression tests on compactedcylindrical specimens. The study involves preparation

    of large number of specimens considering fourteen

    soil grading curves and three cement percentages.

    Hence, use of compacted bricks for such a parametric

    study necessitates handling huge quantities of mate-

    rials (soil, sand, silt and cement). Therefore, smaller

    cylindrical specimens of size 76 mm height and

    38 mm diameter were considered for examining the

    strength. Durability characteristics of compacted

    cement stabilised soil as the soil grading was

    changed was examined through tests on CSSB of

    Fig. 1 Grain size distribution curves for natural soil, sand, silt and reconstituted soils

    Materials and Structures (2014) 47:16331645 1635

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    size 230 9 108 9 75 mm considering 7 % cement

    content.

    3.1.1 Casting cylindrical specimens

    The following procedure was followed for casting the

    cylindrical specimens.

    (a) Soil was oven dried (at 60 C) and then blended

    with requisite quantity of Portland cement in a

    small ball mill (for 10 min) to ensure uniform

    mixing of the cement.

    (b) Requisite quantity of potable water was sprayed

    onto the dry soilcement mixture and mixed

    thoroughly (manually) in order to ensure uniform

    distribution of the moisture in the entire mix.(c) Partially saturated soilcement mixture was fed

    (known weight) into an open-ended cylindrical

    mould. Then the mould was mounted horizon-

    tally in a screw-jack set-up and then compaction

    was carried out from both ends using a mechan-

    ical screw-jack set-up.

    (d) The specimen was extruded from the mould

    immediately after the compaction. Compacted

    specimens were kept for curing under wet burlap

    after 24 h of casting. Curing is continued inside

    the laboratory and was ensured that the specimenis always saturated. Temperatures inside the wet

    burlap varied in a narrow range of 2427 C.

    3.1.2 Casting CSSB specimens

    Manually operated machines are employed in the field

    for the manufacture of CSSB. One such machine was

    used to prepare CSSB of size 230 9 108 9 75 mm.

    Oven dried soil (at 60 C) was powdered and then

    blended with requisite quantity of sand/silt. Uniform

    dry mixture is then blended with 7 % cement (by

    weight). Requisite quantity of potable water was

    sprayed on to the uniform dry mixture of soil, sand/silt

    and cement, and thoroughly mixed to get a uniform

    partially saturated mixture. Known weight of the

    partially saturated soilcement mixture is fed into themachine mould, compacted, extruded and kept in a

    stack for curing. CSSB is cured for 28 days and then

    air dried for 7 days. Air dried specimens were

    then oven dried at 50 C to attain constant weight

    and then used for the testing. Figure3 shows the

    cylindrical as well as CSSB specimens.

    3.1.3 Moulding water content, specimen density

    and compaction energy

    Moulding water content and density influence thestrength of CSSB. Hence, moulding water content and

    the dry density of the compacted cement stabilised soil

    specimens have to be kept constant in order to make a

    comparison of strength and other characteristics across

    different cement percentages and clay contents of the

    mixes. Compressive strength of cement stabilised

    compacted specimens increases with the increase in

    dry density [13,14,16,25]. In the present investiga-

    tion dry density was kept in a narrow range of

    Fig. 2 XRD analysis for the natural soil

    Table 1 Mix proportions of natural and reconstituted soils

    Mix proportion (by weight) Designation

    of the mixNatural soil (NS) Sand Silt

    0 1 0 Sand

    0 0 1 Silt

    1 0 0 NS

    1 3 0 CG1

    1 2 0 CG2

    1 1.25 0 CG3

    1 0.75 0 CG4

    1 0.5 0 CG5

    1 0.25 0 CG6

    1 0 6 FG1

    1 0 3 FG2

    1 0 2 FG3

    1 0 1.25 FG41 0 0.75 FG5

    1 0 0.5 FG6

    1 0 0.25 FG7

    1636 Materials and Structures (2014) 47:16331645

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    Table2

    Characteristicsofnaturalsoil,sand,siltandreconstitutedsoils

    Typeofsoil

    Properties

    Sand

    Silt

    NS

    CG1

    CG2

    CG3

    CG4

    CG5

    CG6

    FG1

    FG2

    FG3

    FG4

    FG

    5

    FG6

    FG7

    Texturalcomposition(%)

    Sand(4.750.075mm)

    100

    0

    50.3

    87.3

    83.2

    77.7

    71.4

    66.7

    60.2

    7.2

    12.6

    16.8

    22.4

    28

    .8

    33.6

    40.2

    Silt(0.0750.002mm)

    0

    100

    18.1

    4.8

    6.3

    8.3

    10.6

    12.3

    14.5

    88.3

    79.5

    72.7

    63.6

    53

    .2

    45.4

    34.5

    Clay(\0.002mm)

    0

    0

    31.6

    7.9

    10.5

    14

    18

    21

    25.3

    4.5

    7.9

    10.5

    14.0

    18

    .0

    21.0

    25.3

    Atterbergslimits

    Liquidlimit(%)

    40.0

    23.7

    25.6

    26.9

    29.7

    32.0

    35.0

    24.2

    25.8

    26.5

    28.0

    29

    .5

    31.1

    33.5

    Plasticlimit(%)

    19.0

    8.6

    9.3

    9.4

    11.2

    12.3

    14.8

    15.9

    16.1

    16.4

    17.8

    18

    .1

    18.4

    18.9

    Plasticityindex

    21.0

    15.1

    16.3

    17.5

    18.5

    19.7

    20.2

    8.24

    9.6

    10.1

    10.2

    11

    .4

    12.7

    14.5

    Shrinkagelimit(%)

    14.0

    1.6

    2.7

    4.6

    6.4

    7.4

    11.0

    1.1

    2.6

    3.5

    6.9

    8.0

    9.4

    12.1

    USCclassification

    SC

    SC

    SC

    SC

    SC

    SC

    SC

    CL

    CL

    CL

    CL

    CL

    CL

    CL

    Predominantclayminerals

    K

    K

    K

    K

    K

    K

    K

    K

    K

    K

    K

    K

    K

    K

    pH

    9.11

    8.43

    7.75

    8.57

    8.35

    8.07

    7.94

    7.82

    7.79

    8.35

    8.26

    8.21

    8.16

    8.09

    8.03

    7.97

    Specificgravity

    2.68

    2.67

    2.68

    2.68

    2.68

    2.68

    2.69

    2.50

    2.50

    2.51

    2.53

    2.53

    2.54

    2.54

    Compactioncharacteristics

    Withoutcement

    StandardproctorOMC(%)

    15.60

    8.50

    8.69

    9.15

    9.58

    10.81

    11.26

    17.10

    18.90

    19.80

    20.60

    21

    .40

    21.90

    22.03

    MDD(kN/m3)

    17.95

    19.03

    19.15

    19.21

    18.93

    18.74

    18.57

    19.45

    19.73

    20.26

    20.14

    20

    .13

    20.07

    20.02

    With7%cement

    StandardproctorOMC(%)

    13.16

    8.00

    8.50

    8.61

    9.37

    10.04

    10.93

    13.52

    14.24

    16.26

    17.02

    17

    .79

    18.31

    18.45

    MDD(kN/m3)

    18.28

    19.36

    19.42

    19.57

    19.45

    19.36

    19.29

    20.91

    21.19

    21.72

    21.60

    21

    .59

    21.51

    21.43

    NSNaturalsoil,SCclayeysand,C

    Linorganicclaysoflowandmediumplasticity,Kkaoliniteclaymineral,MD

    Dmaximumdrydensity

    Materials and Structures (2014) 47:16331645 1637

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    16.917.1 kN/m3 for specimens using coarse grained

    soils and 16.616.9 kN/m3 for specimens using fine

    grained soils.

    Moulding moisture content to be used need not

    depend upon the standard Proctor OMC. This is

    because static compaction process was employed in

    the preparation of cylindrical and CSSB specimens,

    whereas the Proctor test is a dynamic one. Also, thecompaction energy inputs are different in these two

    types of compaction processes. For example to

    compact a soil block of size 230 9 190 9 76 mm to

    a dry density of about 17.5 kN/m3 the energy required

    is 0.3 MJ/m3 when static compaction process was

    employed. The energy input in Standard Proctor

    compaction test is 0.60 MJ/m3. Energy required in

    the compaction process decreases with increase in

    moulding moisture content of the soil mix. Soil

    grading also influences the energy required to achieve

    a particular density. More information on the staticcompaction of soils can be found in the studies of

    Reddy and Jagadish [26]. In the commercial opera-

    tions, CSSB are produced either using a manually

    operated or mechanised machine. In both the types of

    machines static compaction process is used. Such

    machines produce constant volume bricks/blocks and

    hence to achieve a specified dry density for the brick/

    block the machines have adequate capacity to supply

    the required energy.

    It has been shown that compaction on the wet side

    of standard Proctor OMC yields better results for

    cement stabilised soil compacts [25]. After making

    few trial mixes moulding moisture content was fixed at

    12.5 and 18 % by weight for the coarse and fine

    grained soils respectively. Fine grained soils need

    more water to get the required consistency to compactthe specimens using static compaction process in the

    screw-jack set-up employed for casting the cylindrical

    specimens. For both the cases the moulding water

    content chosen is on the wet side of Standard Proctor

    OMC, except for FG6 and FG7 soils where the

    moulding water content is close to Standard proctor

    OMC. It should be noted here that moulding water

    content for a particular soil type (either coarse grained

    or fine grained soil series) is kept constant so that the

    influence of moulding water content on strength

    characteristics is minimised.

    3.2 Testing

    3.2.1 Testing cylindrical specimens

    Compressive strength tests were performed in both

    saturated and dry condition. The wet compressive

    strength (i.e. strength in saturated state), was deter-

    mined by testing the cured and oven dried specimen

    soaked in water for 48 h prior to testing, The drycompressive strength was obtained by testing the

    cured and oven dried specimen. The testing procedure

    is as follows.

    (a) The dimensions of the cylindrical specimens

    were measured using a callipers and the mass of

    the specimen noted (either wet or dry) at the time

    of testing.

    (b) The specimens were subjected to compression in

    a loading frame through the application of

    uniform concentric load at a piston displacementrate of 1.25 mm/min. The load at failure was

    recorded and the compressive strength assessed.

    (c) After the compression test, moisture content of

    the failed specimen (especially the saturated

    ones) was ascertained by drying at 110 C in an

    oven for 24 h.

    Based on the experimental data generated, wet and

    dry compressive strength, dry density and water

    absorption values of the specimen were calculated.

    Fig. 3 Compacted cylindrical specimens and CSSB bricks

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    3.2.2 Testing CSSB specimens

    3.2.2.1 Compressive strength of CSSB (wet and

    dry) Cured and oven dried CSSB bricks were soaked

    in water for 48 h prior to testing for determining the wet

    compressive strength, whereas dry compressive

    strength was obtained by testing the oven driedspecimen. IS 3495-Part I [27] code guidelines were

    followed for determining the compressive strength.

    3.2.2.2 Rate of water absorption and saturated water

    content Cured and air dried CSSB was oven dried at

    50 C to constant weight. The weight of the dry CSSB

    was recorded and then soaked in water. Weight of the

    CSSB was noted at the end of different time intervals

    (i.e. 1, 2, 4, 6, 8, 10, 15, 20, 30, 60, 240, 360, 1,440 and

    2,880 min). The percentage of moisture absorbed by

    the CSSB was determined with respect to the dryweight. A plot of moisture content with the soaking

    duration was obtained.

    Water absorption (saturated water content) of

    CSSB was determined using 24-h immersion cold

    water test as per the guidelines of IS 3495-Part II [28]

    code.

    3.2.2.3 Weight loss after cyclic wetting and drying

    test The cyclic wetting and drying test was carried

    out by following the ASTM D559 [29] code

    guidelines.

    3.2.2.4 Linear expansion on saturation A length

    comparator was used to measure the linear expansion

    on saturation. The procedure outlined in IS 17252011

    code [30] was followed to measure the linear

    expansion value for CSSB.

    4 Results and discussion

    4.1 Compressive strength and soil grading

    Apart from sand and silt fractions, clay mineral type

    and its percentage controls the characteristics of a soil

    mix. Therefore, compressive strength of cement

    stabilised soil compacts was obtained by varying the

    soil gradation over wide limits. Figures4and5 show

    the compressive strengths of cylindrical specimen

    plotted against clay contents of the mix for wet and dry

    compressive strength cases respectively, whereas

    Fig.6 shows a similar plot for CSSB. The results

    shown in these plots represent the mean of six

    specimens, and the density as well as moulding

    moisture contents have been controlled while gener-

    ating the strength results. Following points emerge

    from the results shown in these Figures.

    The strength increases with the increase in claycontent of the soil mix, reaches a peak value and then

    decreases for further increase in clay content. This

    behaviour is noticed for both the types of soil groups

    (coarse and fine grained) in dry as well as saturated

    condition irrespective of cement content and the

    specimen type. The optimum clay content corresponds

    to about 10.5 % for the fine grained soils and 14.0 %

    for the coarse grained soils. Investigations of Reddy

    et al. [15] show optimum clay content of 1416 % for

    coarse grained soils. There is a considerable difference

    between the maximum strength at optimum claycontent and the lowest strength for any given case.

    For 410 % cement content the difference between

    peak strength (at optimum clay content) and lowest

    strength vary in the range of 2050 % for the dry

    strength case and 50130 % for the wet strength case.

    The grain size curves of CG3 and FG3 soils (Fig.1)

    represent the optimum grading curves corresponding

    to the optimum clay content for coarse and fine grained

    soils respectively. The optimum grading curve for

    coarse grained soils (i.e. CG3 curve in Fig.1)

    indicates 14, 8 and 78 % of clay, silt and sand sizefractions respectively. Similarly for fine grained soil

    0

    1

    2

    3

    4

    5

    6

    7

    0 4 8 12 16 20 24 28 32

    Clay content (%)

    Wetcompressiv

    estrength(MPa)

    Coarse grain soil 4%CCoarse grain soil 7%CCoarse grain soil 10%CFine grain soil 4%CFine grain soil 7%CFine grain soil 10%C

    Fig. 4 Wet compressive strength versus clay content of the mix

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    the optimum grading curve (i.e. FG3 curve in Fig. 1)

    shows 10.5, 72.7 and 16.8 % clay, silt and sand size

    fractions respectively. From these results it is possible

    to specify a narrow range for the grain size curves

    leading to maximum strength for CSSB. For example

    2 % from the optimum clay content (Figs. 4, 5, 6)

    will give a band close to optimum value, with marginaldeviation from the maximum strength.

    For fine grained soils the maximum wet compres-

    sive strength (of cylindrical specimen) at optimum

    clay content varies between 2.25 and 6.0 MPa for the

    cement content in the range of 410 %. The corre-

    sponding values for dry compressive strength are in

    the range of 4.710 MPa. The wet strength to dry

    compressive strength ratio is in the range of 0.480.60.

    For coarse grained soils the maximum wet com-

    pressive strength (of cylindrical specimen) at optimum

    clay content varies between 1.0 and 4.7 MPa for the

    cement content in the range of 410 %. The corre-

    sponding values for dry compressive strength are in

    the range of 2.46.5 MPa. The wet to dry strength ratio

    is in the range of 0.420.70. The wet to dry compres-sive strength ratio increases as the cement content

    increases.

    Maximum brick (CSSB) compressive strength (at

    optimum clay content) is 6.3 and 10.8 MPa in wet and

    dry state respectively for fine grained soil (Fig.6)

    using 7 % cement. The corresponding values using

    coarse grained soil are 5 and 9 MPa in wet and dry

    cases respectively.

    The compressive strength of specimens using fine

    grained soils is much higher than those using coarse

    grained soils irrespective of cement content. Consid-ering 410 % cement content range, the compressive

    strength of specimens (at optimum clay content) using

    0

    2

    4

    6

    8

    10

    0 4 8 12 16 20 24 28 32

    Clay content (%)

    Drycompressivestrength(MPa)

    Coarse grain soil 4%CCoarse grain soil 7%CCoarse grain soil 10%CFine grain soil 4%CFine grain soil 7%CFine grain soil 10%C

    Fig. 5 Dry compressive strength versus clay content of the mix

    1

    3

    5

    7

    9

    11

    4 8 12 16 20 24 28 32

    Clay content (%)

    Compressivestr

    ength(MPa)

    Coarse grain soil CSSB (Wet)Coarse grain soil CSSB (Dry)

    Fine grain soil CSSB (Wet)Fine grain soil CSSB (Dry)

    Fig. 6 Strength versus clay content for CSSB with 7 % cement

    0

    1

    2

    3

    4

    5

    4 8 12 16 20 24 28 32

    Clay content (%)

    Compressivestrength(MPa)

    0.53

    0.54

    0.55

    0.56

    Void-ratio

    Wet strength

    Dry strength

    Void-ratio

    Fig. 7 Strength, clay content and void ratio relationships for

    coarse grained soil with 7 % cement

    0

    1

    2

    3

    4

    5

    6

    7

    8

    4 8 12 16 20 24 28 32

    Clay content (%)

    Compressivestren

    gth(MPa)

    0.46

    0.47

    0.48

    0.49

    0.50

    0.51

    0.52

    Void-ratio

    Wet sterngthDry strengthVoid - ratio

    Fig. 8 Strength, clay content and void ratio relationships for

    fine grained soil with 7 % cement

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    fine grained soil is 30110 % higher when compared

    with the strength of specimens using coarse grained

    soils. The reasons for higher compressive strength at

    optimum clay content and higher strengths obtained

    for specimens using fine grained soils are discussed in

    the following sections.

    4.2 Strengthclay contentvoid ratio relationships

    The question arises as to why there is an optimum clay

    content yielding maximum strength, even though the

    densities of the specimens are nearly equal. This can

    be explained through an analysis of void ratio of the

    specimens. Void ratio of the compacted cylindrical

    specimens was estimated based on the density of the

    specimen and specific gravity of the mix. Figures 7

    and8show typical relationships between strength and

    clay content, and void ratio and clay content forcylindrical specimens (with 7 % cement) using coarse

    grained and fine grained soils respectively. These

    results represent the mean of six specimens. These

    relationships clearly indicate that the void ratio is the

    lowest at the optimum clay content of the specimen for

    both the types of soils. Lower void ratio at optimum

    clay content indicates better packing density and

    contacts among the particles leading to maximum

    strength.The specimens with fine grained soils possess lower

    void ratio than those using coarse grained soils. At

    optimum clay content (for 7 % cement specimen) the

    void ratio values are 0.465 and 0.532 for fine and

    coarse grained soil specimens respectively. There-

    fore, for a given combination of density and cement

    content the specimens with fine grained soil show

    lower void ratio and hence result in higher strength.

    Strength and void ratio are linearly related as

    illustrated in Fig.9for CSSB using different cement

    contents. The strength decreases with the increase invoid ratio of the specimen. For 4 % cement CSSB, the

    wet compressive strength increases by 175 % as the

    void ratio reduces from 0.63 to 0.38, whereas for 10 %

    CSSB the strength increase is about 50 %. Strength of

    CSSB at lower cement contents (4 %) is more

    sensitive to the void ratio of the brick.

    4.3 Surface porosity and void ratio

    The pore structure of the broken surface of the cured

    and dried specimen was examined through SEMimaging. Figures10and11show typical SEM images

    of the surface pore structure of the specimen having

    different clay contents with 7 % cement for coarse

    grained and fine grained soils respectively. The

    surface porosity was determined from these images

    using image processing and analysis software.

    0

    1

    2

    3

    4

    5

    6

    7

    8

    9

    0.35 0.40 0.45 0.50 0.55 0.60 0.65

    Void ratio

    Wetcompressivestrength(MPa)

    4% cement

    7% cement

    10% cement

    Fig. 9 Strength versus void-ratio for CSSB

    C1 C2 C3 C4

    Fig. 10 SEM images of compacted cylindrical specimen using coarse grained soil with 7 % cement (C17.9 % clay, 22.7 % surface

    porosity;C2 14.0 % clay, 19.6 % surface porosity; C3 21 % clay, 25.3 % surface porosity; C4 31.6 % clay, 27 % surface porosity)

    Materials and Structures (2014) 47:16331645 1641

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    Figure12shows the surface porosity plotted against

    strength for the specimens using both coarse and fine

    grained soils with 7 % cement. These results again

    confirm that the surface porosity is the lowest for

    specimens having optimum clay content (10.5 % for

    fine grained soil and 14.0 % for coarse grained soil).

    The surface porosity at optimum clay content is 14.5

    and 20 % for the specimens using fine grained and

    coarse grained soils respectively. The specimens using

    fine grained soils show a lower value of porosity when

    compared with those using coarse grained soils. Thisexplains the reason for higher compressive strength

    values for specimen with fine grained soils when

    compared with those of coarse grained soil specimens.

    4.4 Strength and Atterberg limits

    Atterbergs limits of a soil indicate the plasticity and

    shrinkage characteristics of the soil mix. Liquid limit,

    plastic limit, shrinkage limit and plasticity index of all

    the soil mixtures used in the experimental investiga-

    tions are given in Table2. Typical relationship

    between plasticity index (PI) and the compressive

    strength of cement stabilised compacted cylindrical

    specimen is shown in Fig. 13. Plots have been made

    for both wet and dry compressive strengths and using

    both coarse and fine grained soils using 7 % cement.

    Each point in the plot represents mean of six

    specimens. The trend lines indicate decrease in

    strength as the PI increases. The PI value for theoptimum clay contents yielding maximum strength are

    17.5 and 10.1 for coarse grained and fine grained soils

    respectively.

    4.5 Durability characteristics of CSSB

    Satisfactory durability or long term performance of

    CSSB is an important issue to be addressed apart from

    examining the strength. Structures using CSSB are

    F4F1 F2 F3

    Fig. 11 SEM images of compacted cylindrical specimen using fine grained soil with 7 % cement (F1 7.9 % clay, 18.44 % surface

    porosity; F2 10.5 % clay, 14.5 % surface porosity; F3 14 % clay, 15.1 % surface porosity; F4 25.3.6 % clay, 19.32 % surface porosity)

    12

    14

    16

    18

    20

    22

    24

    26

    28

    4 8 12 16 20 24 28 32

    Clay content (%)

    Surfaceporosity

    (%)

    Coarse grained soil-7%Cement

    Fine grained soil-7%Cement

    Fig. 12 Relationship between surface porosity and clay content

    0

    1

    2

    3

    4

    5

    6

    7

    8

    6 8 10 12 14 16 18 20 22

    Plasticity index

    Compressivestreng

    th(MPa)

    Wet compressive strength

    Dry compressive strength

    Fig. 13 Relationships between compressive strength and plas-

    ticity index

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    prone for the cyclic exposure to rain or hygroscopic

    environment and drying due to the changes in the

    surrounding climate. Since the CSSB contains certain

    amount of clay minerals even after cement stabilisa-

    tion [31], hence there is a possibility for cyclic

    expansion and shrinkage phenomenon taking place in

    CSSB due to the variations in the surrounding climaticconditions. Therefore, evaluation of the durability of

    CSSB should address the issue of cyclic wetting and

    drying and dimensional stability. ASTM D559 [29]

    code suggests monitoring the weight loss of the brick

    after subjecting to 12 cycles of cyclic wetting and

    drying including scratching the surface with metal

    wire brush. Linear expansion on saturation gives an

    idea of the dimensional stability of CSSB [15]. IS1725

    [30] has adopted this test and specifies limits for

    weight loss (\3 %) and linear expansion on saturation

    (\0.10 %) for satisfactory performance of CSSBmasonry walls.

    Weight loss after the cyclic wetting and drying test,

    and linear expansion on saturation were monitored for

    the CSSB using both coarse grained and fine grained

    soils with 7 % cement. Figure14 shows a typical

    variation in weight loss after the cyclic wetting and

    drying test with the clay content of CSSB. The lowest

    value of the weight loss for the CSSB occurs at the

    optimum clay content yielding maximum strength.

    The optimum value of clay content giving least weight

    loss is 10.5 and 14 % for the CSSB using fine grainedand coarse grained soils respectively.

    Linear expansion on saturation for the CSSB using

    7 % cement and with coarse and fine grained soils is

    shown in Fig.15. Linear expansion increases with

    increase in clay content irrespective of the soil type.

    The linear expansion varies in the range of

    0.030.20 % as the clay content changes from 8 to

    31.6 %. At the optimum clay content the linear

    expansion values are 0.04 and 0.045 % for the bricks

    using fine and coarse grained soils respectively. These

    values are well within the accepted value of 0.1 %

    [30].Based on the strength and durability tests it can be

    concluded that the optimum clay content of the soil

    mix yielding best results for CSSB is about 10 and

    14 % for the fine grained and coarse grained soils

    respectively. It may be difficult to adjust the clay

    fraction of the soil mix precisely in the field/factory

    while producing the CSSB. Therefore, a narrow band

    for optimum clay fractions can be defined for field

    applications. Hence, the optimum clay content can be

    10 2 and 14 2 % for fine grained soils and coarse

    grained soils (containing non-expansive clay miner-als) respectively for the cement content in the range of

    410 %.

    4.6 Absorption characteristics of CSSB

    The rate of water absorption and saturated water

    content (designated as water absorption) were deter-

    mined for the CSSB manufactured using both coarse

    and fine grained soils. The rate of water absorption

    with the soaking duration in water for CSSB is

    displayed in Fig.16. Relationship between waterabsorption and clay content of CSSB is shown in

    Fig.15. The following points emerge from the results

    of Figs. 15and 16.

    (a) The dry CSSB absorbs water at a faster rate

    initially up to 60 min of soaking duration and

    0

    2

    4

    6

    8

    10

    12

    4 8 12 16 20 24 28 32

    Clay content (%)

    Weightloss

    (%)

    Coarse grained soil CSSB

    Fine grained soil CSSB

    Fig. 14 Weight loss versus clay content of the mix for CSSB

    using 7 % cement

    0

    5

    10

    15

    20

    25

    4 8 12 16 20 24 28 32

    Clay content (%)

    Waterabsorptio

    n(%)

    0

    0.05

    0.1

    0.15

    0.2

    0.25

    Linearexpansio

    n(%)

    Water absorption of CSSB - Coarse soilWater absorption of CSSB - Fine soilLinear expansion of CSSB - Coarse soilLinear expansion of CSSB - Fine soil

    Fig. 15 Variation of water absorption and linear expansion

    with clay content for CSSB using 7 % cement

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    later on the absorption rate reduces. CSSB using

    fine grained and coarse grained soils attain 85

    and 90 % saturation respectively in about 60 min

    of soaking in water. The bricks saturate com-

    pletely when soaked in water for 24 h.

    (b) The water absorption increases with increase in

    clay content. This is on the expected lines

    because the clay has more affinity for water,

    more clay means more water absorption.

    (c) Water absorption values range between 18 and

    20 % for CSSB using fine grained soil as the clay

    content changes from 8 to 31.6 %. For bricks

    with coarse grained soils the range is 1316 %.

    (d) At optimum clay content the water absorption is14 and 18 % for CSSB using coarse grained and

    fine grained soils respectively.

    These results clearly indicate that CSSB absorbs

    water and attains 8090 % saturation in about an hour

    after soaking in water. The bricks attain complete

    saturation in 24 h of immersion in cold water.

    5 Conclusions

    Influence of soil grading especially the clay sizefraction of the soil in controlling the strength, dura-

    bility and absorption characteristics of cement stabi-

    lised soil compacts and bricks was examined in great

    detail considering both coarse and fine grained soils.

    The investigations show that clay fraction of the

    soil mixture and the void ratio (density) of the

    compacted specimen play crucial role in influencing

    the characteristics of cement stabilised soil compacts.

    There is optimum clay content leading to maximum

    strength and lowest mass loss (in the durability test)

    for CSSB. The optimum clay content is about 10 and

    14 % for fine grained soils and coarse grained soils

    respectively for cement contents in the range of

    410 %. Large deviations from the optimum clay

    content value results in considerable loss in strength

    for cement stabilised soil compacts. Void ratio of thecompacted specimen is the lowest at the optimum clay

    content and therefore possesses maximum strength at

    optimum clay content. Void ratio of specimens using

    fine grained soils is lower than those using coarse

    grained soils. Hence, the CSSB using fine grained soils

    possess higher strength than those with coarse grained

    soils. In order to achieve optimum clay fraction for a

    particular soil, the soil grading can be adjusted by

    reconstitution with sand.

    The mass loss after the durability test is lowest for

    the bricks having optimum clay content. CSSB absorbwater rapidly in the initial 1 h of soaking in water and

    attain complete saturation in 24 h. Bricks with fine

    grained soils show higher value of water absorption

    when compared to the bricks using coarse grained soils.

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