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Career Profile
1
Mehul Shivadatta Dhonde
Self introduction
2
• Current Title: Test Engineering Manager, Quality
• Back Ground: Belong to Indian origin , Mumbai.38 year old married man.
• Bachelor of Engineering in Electronics and Telecommunication (University of Mumbai, India).
• Diploma in Industrial Electronics (Board of Technical Examinations, Mumbai, India)
• Skills –
Product Design Testing, Verification and Validation;
Failure Analysis;
Quality Assurance;
Experience
Has been working in China / Hong Kong for more than 6 years in an Electrical, Electronics and Telecommunication products related Industry with various roles.
Engineer or Leader Level experience of about 7+ Years.
Supervisory or Middle Management Experience of about 5 Years.
• Specific Roles of career –
Failure Analysis & Reliability Test Engineer ( Dongguan Elcoteq Electronics Ltd.)
Assistant Quality Assurance Manager (Chung Nam Electronics – Positioned in Hong Kong).
Group Quality Leader for supplier quality management (Newell Rubbermaid).
Senior Failure Analysis Engineer (Philips Solid State Lighting Solutions).
Current - Test Engineering Manager (Green Mountain Coffee Roasters – Electrical Appliances Technical Consultancy Shenzhen Ltd. Subsidy of Keurig Green Mountain , US).
Self introduction
3
• Highlights of Important Projects accomplished in career-----
Functional Test Yield Improvement (60% to 80%) on Set Top Box (Electronics and Telecom) Product;
Design and Implement Lab View based software for environmental test temperature chamber;
Green Belt Six Sigma Projects of improving common failure modes in mobile phone products (Average
defects reduced from 20% to 3% for LCD, Keypad, Small DC Electric Motor etc…);
Black Belt Six Sigma Project Support to peers for failure analysis & Design of Experiment
Touch LCD Gasket failures improvement (Especially from process contamination etc.)
(Average defect reduced from 10% to 2%);
Poly Carbonate Lens environmental stress cracks for lighting fixtures;
(Average defect reduced from 15% to 5%)
Wire Bond Process Improvement for Chip On Bond on LED Driver PCBAs;
(Average defect reduced from 7% to 1%)
Plastic Housing Cracks @Screw Boss for mobile phones, Lighting Fixtures;
(Average defect reduced from 15% to 3%)
Small DC Electric Motor used in Radio Frequency based Receiver for base station failed to operate
occasionally;
(Average defect reduced from 20% to 2%)
Current products
4
Involved with following products for providing design verification, validation and failure analysis services.
Set top boxes and its accessories
LED Lamps
LED Luminaries
Various Electrical Products and its sub assemblies
Solar panel chargers
GPS Bracelet
Mobile Phones
Remote Control
LCD’s
Coffee Brewers or Machines
Products Display –Set top boxes and
Accessories
SD & HD video reception
Supports MPEG-2 &
MPEG-4/H.264 AVC
Latest silicon offering
advanced performance &
features
High-quality HDMI™
output & USB connector
SPDIF output for high
quality audio loop through
such as Dolby ®Digital
Built in networking
capability
Optional support for HDD
upgrade to DVR
5
Products Display – LED Lamps
6
Products Display – LED Luminaries
7
Products Display – Mobile Phones
8
Products Display – Solar Strap Chargers
9
Products Display – GPS Bracelet
10
Products Display – Phone Accessories
11
Products Display – Telecom Network
12
Products Display – Mobile Phone
Mobile phones with normal features
Supports GSM 800/900
USB interface with computers
Text messaging
Call forwarding / call awaiting /
Talk time 180 to 480 minutes
Standby time 420 to 620 hours
13
Products Display – LED Luminaires
LED Luminaires with different LED Luminance
and Output Power Specifications.
Refer to www.colorkinetics.com
14
Innovative Coffee Brewers or Machines.
Refer to www.keurig.com or www.gmcr.com
15
Products Display – Coffee Brewers
15
Generic Testing and Validation Map Followed in Career
No. Items Brand Discription Model Qt'y Ref. Photo Reference
Unit Price
Sub
Tota l Reference Information
Availabilty in
Engineering
Lab
Sharing Possibility Insta lla tion Phase
Acquisition and
1 Oscilloscope Lecroy 200MHz, 4 channels,
.5GS/s, 5Mpst/CH
W aveSurfer
24Xs-A 1 44617 44617
es.aspx?mseries=49&capid
http://www.lecroy.com/Os Y
cilloscope/OscilloscopeSeri
=102&mid=504
Minimum 1st Phase
2 Current Probe Lecroy 50MHz, 30A, 7ns CP030 1 17850 17850 modelid=1130&categoryid= Y
http://www.lecroy.com/Op
tions/ProductDetails.aspx?
3&groupid=7&capid=102&m
id=508
Minimum 1st Phase
3 High-Voltage
Differential Probe Lecroy
1400Vpeak, 20MHz
and 100MHz ADP305 1 8480 8480
tions/ProductDetails.aspx? Y
http://www.lecroy.com/Op
modelid=300&categoryid=3
&groupid=148
Minimum 1st Phase
4 Portable
multimeter Fluke Digital multimeter FLK-289 1 6385 6385 cs_id=37737%28FlukeProdu Y
http://www.fluke.com.cn/cnzh
/products/specifications.htm-
cts%29&category=HMA%28
FlukeProducts%29.htm
Minimum 1st Phase
5 DC Power supplier Agilent
80W Power Supply,
35V/2.2A or 60V/1.3A, E3645A
1 output
1 6513 6513 35489.384192.00&cc=US&lc
Y
http://www.home.agilent.com/
agilent/product.jspx?nid=-
=eng
Minimum 1st Phase
6 Power Meter YOKOGA
W A
26A, 0.1%,
0.5Hz~100kHz W T210 1 18600 18600 analyzers/digital-power-
http://tmi.yokogawa.com/prod
ucts/digital-power-
analyzers/wt210wt230-digital-
power-meters/
Y Minimum 1st Phase
7 AC Power Source
IDRC 500VA, 0~300V 2.1A CF-500T 1 9300 9300 http://www.idrc.com.tw/big5_v
Y er/products/cf_t/cf_t.htm
Minimum 1st Phase
8 Desktop
Multimeter Agilent
Industry Standard
Digital Multimeter, 6½
Digits: dc & ac voltage,
dc & ac current, 2 & 4
wire resistance,
frequency & period,
continuity, diode test
34401A 1 7258 7258 agilent/product.jspx?nid=-
http://www.home.agilent.com/
536902435.536880933.00&cc
=US&lc=eng
Y Minimum 1st Phase
9 IR Thermometer Ryobi Measure surface
tempearure ZRIR001 1 1500 1500 /catalog/accessories/electr N
http://www.ryobitools.com
onic_hand_tools/IR001
NA 1st Phase
10 clamp meter
Leakage current 1 3500 3500 N NA 1st Phase
Sub Tota l
(1st Phase) 124004
16
Electronic Equipments utilized in career for testing and validation
Electronic Equipments for testing and validation
18
Lab Equipments for testing and validation
Note: Comprehensive knowledge of material characterization techniques such as FTIR, SAM, SEM, EDX, Cross Section,
Dye and Pry 19
1
6
Microscopes 300X to 1000X
high
magnification
microscopes
required
Leica
M3Z or
MZ6
1 271
74
271
74 http://www.leica-
microsystems.com/
product s/stereo-
microscopes-
macroscopes/routi
ne-
manual/details/pro
duct/lei ca-mz6/
N NA 2nd Phase
1
7
IV Tracer To measure
current voltage
charcteristics of
LED @ PCBA
2nd Phase
1
8 Extrusion
Plastometer
Melt Flow
Rate Test
Tini
us
Ols
en
Advanced melt
indexing
Extrusion
Plastometer
System
MP60
0 or
MP12
00
(http://
ww
w.tinius
ols
en.com/
1 759
40
759
40 http://www.tinius
olsen.co
m/tiniusimages/TD
914- MP600.pdf
N NA 2nd Phase
/TD-985-
4lr.pdf)
Sub
Total:
1031
14
№ Items Brand Discription PN Qt'y Ref. Photo Reference Sub Tota l
Unit Price Availabilty in
Engineering Lab
Sharing
Possibility
Acquisition and
Insta lla tion Phase
1 Hammer W iha No rebounding, 25x288 02092 7 1 236.00 236.00 N NA 1st Phase
2 File K it Cromwell
(Kennedy) 6 items - 1 162.00 162.00 N NA 1st Phase
3 W rench Cromwell
(Kennedy) FINISH ADJUSTABLE
150mm/6" PHOSPHATE - 1 88.00 88.00 N NA 1st Phase
4 Hammer Cromwell 16oz CLAW HAMMER
(Kennedy) STEEL TUBE SHAFT - 1 107.00 107.00 N NA 1st Phase
5 Hole Gauge SK 0.100-0.290mm - 1 N NA 1st Phase
6 Hole Gauge SK 0.300-1.525mm - 1 N NA 1st Phase
7 Filler Gauge Mi tutoyo 0.05-1.0mm - 1 380.00 380.00 N NA 1st Phase
8 Drilling & M illing
Kit Pro'sk it
E lectric (220V), drilling 5, -
mill ing 6 1 258.00 258.00 N NA 1st Phase
9 Tens ile testing
machine
Press ing, bending and
twis ting test 1 500.00 500.00 N NA 1st Phase
10 Tool Box Cromwell
(Kennedy) 450x250x325mm
PROFESSIONAL 4
DRAW ER, - 1 394.00 394.00 N NA 1st Phase
Sub Total (1st
Phase) 3445.00
1320.00 1320.00
19
Mechanical Equipments for testing and validation
R e p l y
F a i l u r e C o m p l a i n t
R e p l y
H a lt S h i p m e n t
R e p l y R o o t C a u s e
&
E n g i n e e r i n g
I n s t r u c t i o n s
C o r r e c t i v e A c t i o n
R e q u e s t f o r E n g i n e e r i n g M a n u f a c t u r e P r o b l e m C o r r e c t e d
C o u n t e r m e a s u r e
C u s t o m e r
S Q E
Q A D e p a r t m e n t
F a i lu r e A n a ly s i s
M a n u f a c t u r i n g
D e p a r t m e n t
E n g i n e e r i n g
D e p a r t m e n t D i s t r i b u t i o n
D e p a r t m e n t
P r o d u c t i o n , Q u a li t y , P r o c e s s ,
T e s t
C o m m e n t s :
T e s t a n d F a ilu r e A n a ly s is t e a m s a r e in t e r r e la t e d b y t h a t ; T e s t s v e r if y t h e f a ilu r e m e c h a n is m s t h a t h a p p e n a s e x p e c t e d ; T e s t s id e n t if y n e w f a ilu r e m e c h a n is m s w h ic h a r e n o t e x p e c t e d ; T e s t s v e r r f y t h e e f f e c t iv e n e s s o f a c t io n s t h a t p r e v e n t f a ilu r e ;
Failure Analysis Relationships with Other Teams
21
Basic Terms of Failure Analysis
22
Logical Approach
23
Generic Failure Analysis Process Followed
Failure Analysis Actions to be executed
Bad Sample Good Sample
A) Analytical Test --- Localization of failure using bench testing.
B) Identify failure component.
a) Test product.
b) Reproduce failure using highly accelerated life time test.
C) Test Mode --- FESEM, FTIR, MFR, SEM, SAM, DSC, etc… c) Analytical Test --- Analyze crack propagation and obtain surface analysis through fracto-graph
D) Task 1: Record results in tabular format both test modes Task 2: Both test mode tabular results comparison to be documented in analysis report.
d) Test Mode --- FESEM, FTIR, MFR, SEM, SAM, DSC,etc… e) Determine failure mechanisms.
f) Task 1: Record results in tabular format both test modes
Task 2: Both test mode tabular results comparison to be documented in analysis report.
SEM – Scanning Electron Microscope
FESEM – Field Emission Scanning Electron Microscope
FTIR – Fourier Transform Infrared Spectroscopy
MFR – Melt Flow Rate, DSC – Differential Scanning Calorimetry for Plastics failures
SAM – Scanning Acoustic Microscope
23
Logical Flow Diagram Failure Analysis Process
Bad Sample
25
Good Sample
A
B
C
a
b
c
d
Compare Results
& Analysis
Reporting
D e f
Die
Package
Examples
Die Scratch
Ball Lifting
Pictures Product Related
Optical SEM
Ball Lifting
Failure Modes Analyzed
26
Failure Modes, Technique and Equipments
V a r io u s F a i lu r e M o d e s
T e c h n i q u e : V is u a l &
M ic r o s c o p y T e c h n i q u e : F u n c t i o n a l T e s t i n g
i ) P a c k a g e d e la m in a t io n ;
i i ) P a c k a g e C r a c k in g ;
i i i ) M is s a l l ig n m e n t ;
i v ) S o ld e r b r id g e , c r a c k ;
i ) E S D / E O S ;
i i ) D ie c r a c k in g ;
i i i ) C o r r o s io n ;
i v ) E le c t r o m ig r a t io n ;
T e c h n i q u e :
M e c h a n i c a l
T e s t i n g
J e t E tc h e r fo r
D e c a p p i n g :
O u t S o u r c i n g
H i g h E n d M ic r o s c o p e
P l a n fo r In H o u s i n g
P h a s e 1
C r o s s S e c t i o n i n g E q u i p m e n t
In h o u s e ( E lc o te q B e i j i n g ) S c a n n i n g A c o u s t ic M ic r o s c o p e
P l a n fo r In h o u s i n g
P h a s e 2
C u r v e T r a c e r
P l a n fo r In h o u s i n g
P h a s e 2
P r o b i n g S ta t i o n
P l a n fo r In h o u s i n g
P h a s e 2
X - R a y
P l a n : O u ts o u r c i n g
S o l d e r a b i l i t y T e s t
S y s te m
P l a n : O u ts o u r c i n g
27
i) Corrosion;
ii) Deformation;
iii) Package Cracks;
iv) Damaged Joints;
i) Short Circuit;
ii) Open Circuit;
iii) Functional Failure;
iv) Contact Resis;
i) Broken bond wires;
ii) Missing solder ball;
iii) Miss allignment;
iv) Solder bridge, crack;
v) Solder Joints
Technique: X Ray &
Solderability Test
System Technique: Scanning Acoustic
Microscopy
i) Intermetallic Growth;
ii) Short Joints Cracking;
iii) PCB Cracks & Delamination;
Technique: Cross
Sectioning
i) W ire Pull;
ii) Die Shear;
iii) Ball Shear;
Technique :
Decapsulation
Failures resolved, Quality Improved No Product Component Failure Location Analysis Improvement
1 Coffee Brewer Exit Metal Needle 4%
(5000 DPPM)
• Consumer Simulation Test
/ Warranty claims.
Slide 28 to 32 <0.2%
(100 DPPM)
2 Display LCD 5 %
(6000 DPPM)
• Product Line.
• Consumer Simulation
Test.
Note: LCD condensed /
Electric Over stress.
Slide 33 to 37 <1%
(500 DPPM)
3 LED Product Control PCBA 3%
(3500 DPPM)
• PCBA Mfg. Lines.
Note: LED fast shutdown or
failures @ customers.
Slide 38 to 41 <0.5%
(600 DPPM)
4 LED Product Power PCBA 2%
(2900 DPPM)
• PCBA Mfg. Lines.
Note: Capacitor failed in
Accelerated Life Test.
Slide 42 to 45 < 0.2 %
(100 DPPM)
5 Coffee Brewer Micro-switch 19%
(20000 DPPM)
• Field failure returns for
warranty claims. Puncture
mechanism does not
activate for Brew.
Slide 46 to 50 < 0.3%
(200 DPPM)
6 LED Product Power Connector 10%
(4000 DPPM)
• Field failure returns Slide 51 to 54 <0.1% (100
DPPM)
7 LED Product Chip on Bond 7% (3000 DPPM) • Field failure returns Slide 55 to 63 < 0.2% (150
DPPM)
8 LED Product Plastics 11% (3400 DPPM) • Field failure returns Slide 64 to 76 <1% (500 DPPM)
9 LED Product Power Cord 2%
(2800 DPPM)
• Product Line. Slide 77 to 78 < 0.1%
(90 PPM)
10 Set Top Box Power PCBA 1.5%
(2300 DPPM)
• PCBA functional and life
test.
Slide 79 < 0.2%
(150 DPPM)
11 Coffee Brewer Boiling section 3%
(3200 DPPM)
• Consumer Simulation Test. Slide 80 to 81 < 0.1%
(90 DPPM)
28
Clogged Needle Needle Plate Check Valve Analysis
29
Vacuum created due to pressure difference between Exit Needle and Umbrella Valve. Coffee Grounds suck back to exit needle and clog.
Keurig Clogged Needle
Needle Plate Check Valve Analysis
30
Keurig Clogged Needle
Needle Plate Check Valve Analysis
31
Keurig Clogged Needles
• Verify the check valve function on 2.0 brewers returned for needle clogs in Triage
• Determine root cause of poor welds on check valve seats at CM’s. The needle plate/CV assy.
are functionally checked during manufacture.
• Verify Test Plans and Stage gate of tests after ultrasonic welding and induction welding for
puncture mechanism assembly.
Slow leakers escaped during testing after welding process. Did analysis pressure decay curves.
• Dimensional analysis of all parts/cavities.
• Review welding and post weld pressure test process at CM’s.
Needle Plate Check Valve Analysis
32
Failures resolved - LCD
Product: Flat panel display, that uses the light modulating properties of liquid crystals.
Product Construction: The displays are constructed with a reflector on the back, a polarizer, glass with electrodes on the inside,
a seal with liquid crystal, glass, and top polarizer.
Failure Mode: Light display fading issues closest to the seal.
Failure Location: Closest to the seal @ LCD Assembly between glass layers.
Failure Analysis Test: Moisture Ingress Analysis Test.
Failure Mechanism: Moisture Ingress. Liquid Crystal had lost interfacial wetting. The seals were cut to open the sandwiched
LCDs, and SEM-EDS analysis was performed. The black spots occurred the LC had lost contact with the interface of
the glass. It is most likely that moisture in very low quantities, was the cause of the problem. Water vapor, however,
will not show in SEM-EDS or FTIR in a single digit ppm level. There was definitely a contamination or moisture issue
inside the LCD, which could be analyzed with mass spectrometry. Note: EDS of Micrograph can be referred at next slide. Failure Cause: Moisture Ingress. Cause for the fading is inherently inside the liquid crystal or ingress through the seal
over time. Resolution: Liquid Crystal with better high viscosity and process optimization of controls such as pressure sealant
coating.
Good LCD SEM Micrograph Black Spots in LCD
33
Failures resolved - LCD
34
Failures resolved - LCD
Product: LCD controller/drivers mounted directly on glass and connected via a 24 pad polyimide flex circuit to a FRU controller
card
Product Construction: The displays are constructed with a reflector on the back, a polarizer, glass with electrodes on the inside, a seal with liquid crystal, glass, and top polarizer.
Failure Mode: Short Circuit.
Failure Location: Chip with blown I/O.
Failure Analysis Test: Cross Section / SEM .
Failure Mechanism: Electric Over Stress. There is a direct correlation between the failures and the EOS found on the die
at the test point pads. The good die had no EOS on any of the test point pads with the same date code. Since these
test points are output pins, this would imply the circuitry associated with these test pads have seen too much power
also. This would inherently raise a concern over reliability and latent damage on the die prior to use. Since these test
pins are not connected in any way to the application and a connection must have been made to make them fail, then
the testing must have occurred at the manufacturer.
Resolution: Not Applicable as it showed some malfunction by manufacturer during testing.
Interconnects to Chip Chip with blown I/O
35
Failures resolved - LCD
Material Analysis: Thinner Multi-layer materials and polymers (especially the adhesive layers in polymer laminates). Failure
Analysis Technique: Micro and Macro Attenuated Total Reflection Focal Plane Array (FPA) imaging system. Analytical
Information: Chemical information about product failure of functional films in LCD screens. A high spatial resolution from
several small beads and their surroundings providing a comprehensive means of troubleshooting product defects in the
manufacturing process.
Critical Analysis: 3 micron adhesive layers in multilayer laminates, the orientation of surface -bound monolayer species on
silicon, or the identification of contaminants such as METAL CONTAMINATION.
Resolution: Process Optimization for Silk Printing and / or Etching.
36
Failures resolved - LCD
Material Analysis: Thinner Multi-layer materials and polymers (especially the adhesive layers in polymer laminates). Failure
Analysis Technique: Micro and Macro Attenuated Total Reflection Focal Plane Array (FPA) imaging system. Analytical
Information: Chemical information about product failure of functional films in LCD screens. A high spatial resolution from
several small beads and their surroundings providing a comprehensive means of troubleshooting product defects in the
manufacturing process.
Critical Analysis: METAL CONTAMINATION as Skin Flake during Etching and / or Screen Printing.
Resolution: Process optimization and controls for Etching and Screen Printing.
37
Failures Resolved – LED Defect
38
Failures Resolved – LEDs Fast Shut Down or LEDs Out
39
Failures Resolved – LEDs Fast Shut Down or LEDs Out
40
Material Characterization Analysis Processed through SGS and LED Suppliers such as NICHIA,
Samsung, CREE. Usually such defects result of
Failure Mode: Crack or damage to Epitaxial Layer, MESA structure damaged.
Failure Mechanism: mechanical stress, inherent defect to LED Chip
Failure Location: Hi-pot Testing, Field Installations etc…
Failure Cause: Pick and Place force @ SMT Process >>> 3 Newton's (General). When Reflow Profile
not meet optimization under
heat zone could cause stress @ LEDs during thermal cycles in reflow oven. If Reflow oven process is
air reflow based it would be much easier to avoid stress and inherent defect s to LED chip getting
worst and prolong the LED performance in the field.
Quality Control Test: Environmental Testing of LED Fixtures @ AQL under stringent temperature /
humidity conditions to see effectiveness of corrective actions.
Failures Resolved – LEDs Fast Shut Down or
LEDs Out
41
Failures Resolved – Ceramic Capacitor
42
Failures Resolved – Ceramic Capacitor
43
Failures Resolved – Ceramic Capacitor
44
Failures Resolved – Ceramic Capacitor
45
Electrical Circuit failed in burn in test with full resistive load.
Bench level diagnosis depicted some semiconductor JFET’s as well as critical location ceramic
capacitor found short in every inspected.
Further fault isolation as per design analysis ceramic capacitor crack is root cause of failure.
Designed and executed Highly Accelerated Life Test “High Temperature Testing” using
temperature chamber to reproduce defect.
Determine “Mean Time Between Failure (MTBF)”.
Locate same symptoms of failures.
Evaluate product design using “Design for Reliability” Software.
Failure Mechanism identified as BaTiO3 as ceramic ferroelectric material inside capacitor
which will always tend to develop impurities at various temperature of operations, tending to
create possibility of increment in leakage current inside capacitor walls.
Suggested the design changes from 1206 to 1210 package size of capacitor component
reduce defect percentage.
Design changes resulted in considerable increment in First Pass Yield from 68% to 95% @
burn in test.
All these actions are conceived by my self and leaded by myself. Physical activities done by
support team.
M o b i l e C o n t a c t o f S w i t c h F i x e d C o n t a c t o f S w i t c h
A b o v e & B e l o w i n s p e c t i o n a f t e r 1 0 8 C y c l e s u n d e r h o t s w i t c h i n g o f 3 V / 1 0 M i c r o A m p o p e r a t e d u n d e r 2 0 0 M i c r o N f o r c e
S c a n n i n g E l e c t r o n M i c r o s c o p i c I n s p e c t i o n f o r G o l d / S i l v e r c o a t e d c o n t a c t s
S c a n n i n g E l e c t r o n M i c r o s c o p i c I n s p e c t i o n f o r R u t h e n i u m c o a t e d c o n t a c t s
1
2
M o b i l e C o n t a c t o f S w i t c h F i x e d C o n t a c t o f S w i t c h
- - - B l a c k c i r c l e s o b s e r v e d m o s t l y o n t h e e d g e s o f c o n t a c t . B l a c k t r a c e s o r c i r c l e s c a l l e d " F r i c t i o n a l P o l y m e r s " g e n e r a t e d w h e n c a t a l y t i c c o n t a c t m a t e r i a l s s u c h a s R u t h e n i u m a r e b r o u g h t i n t o c o n t a c t i n p r e s e n c e o f
c a r b o n a c e o u s c o n t a m i n a t i o n . - - - T h e s e f r i c t i o n a l p o l y m e r s a r e r e s i s t i v e c a n d e v e l o p r e s i s t a n c e > 1 0 K O h m r e s u l t i n g i n t o s t i c t i o n f a i l u r e o f m i c r o s w i t c h . - - - S c a n n i n g E l e c t r o n i c M i c r o s c o p i c i n s p e c t i o n a t e n d o f h o t s w i t c h i n g t e s t i n g s h o w s R u t h e n i u m c o n t a c t s a r e b e s t s u i t e d d e v e l o p i n g l e s s f r i c t i o n a l p o l y m e r s .
C o n c l u s i o n - - - G o l d , S i l v e r o r i t s a l l o y s p l a t e d / c o a t e d c o n t a c t s a r e p r o n e t o s t i c t i o n f a i l u r e o v e r p e r i o d o f t i m e
a n d u s a g e e s p e c i a l l y i n f i e l d a s h i g h c o n t a c t r e s i s t a n c e i s d e v e l o p e d i n t e r m s o f f r i c t i o n a l p o l y m e r s
I n d u s t r y s t a n d a r d s s u g g e s t c o m b i n e d m e t a l c o a t i n g / p l a t i n g s u c h a s g o l d a n d r u t h e n i u m 46
Micro Switch Advanced Failure Analysis
(Reference: A Practical Guide for Component Manufacturers of Electronic Components and Systems--- Page 275 to 278 @ link in this box in F5 Run Slide Show m ode
47
Fishbone Diagram for Micro Switch Failure
Cause Effect Analysis
Electro performance of base
material or plating material
(Silver) degrades over time
No contact
resistance
measurement @
IQC or in
functional testing
@ assembly level
No system to make sure silve plated contacts are
degraded or contaminated from foreign particles such
as dust, etc...
Process Materials
Process
Personnel
Degrade the silver plated contacts
such that and lower the electro
performance of the silver plated and
the base material contacts
Defect
Switch Failure e.g. Stiction
Failure
Measurement
Enviornment
No Passivation in the electro-
plate process. Silver plated
surfaces are not protected, will
act with Sulfate,Chloride ion
and Hydrogen sulfide. Electro
performance of silver
sulfate and silver sulfide is poor
Performance of
passivation
oxidation film is
poor for silver
plated contacts
1
2
3
4
5 6
(√-) Not likely to cause failure
(√) Likely to cause failure
(√+) Most Likely to cause
failure
48
Fishbone Rating for Micro Switch Failure
Cause and Effect Rating Target Materials - performance of base material or plating material (Silver) degrades over time such that fails 90 90
Materials - Degrade the silver plated contacts such that and lower the electro performance 90 90
Process - No Passivation in the electro-plate process. 70 90
Process - Performance of passivation oxidation film is poor for silver plated contacts 70 90
Measurement - No contact resistance measurement @ IQC or in functional testing 20 90
Environment - No system to make sure silver plated contacts are degraded or contaminated 20 90
Note: Rating provided is an assumption, there is no any mathemetical calculations involved
Rating of each failure factor has no calculations but follows an approach similar to “Risk Priority Number Calculations as in FMEA”
49
Fishbone Chart for Micro Switch Failure
30 20 10
0
40
100
90
80
70
60
50
Materials -
performance of base material or plating
material (Silver)
degrades over time such that fails
Materials - Degrade the Process - No silver plated contacts such that and lower
the electro
performance
Passivation in the electro-plate process.
Process - Performance of passivation
oxidation film is poor measurement @ IQC or silver plated contacts for silver plated
contacts
Measurement - No contact resistance
in functional testing
Environment - No system to make sure
are degraded or
contaminated
Target
Rating
50
Micro Switch Supplier Visit Observations
No. Observations and Corrective Actions from visit @ Micro Switch Supplier
Red Factor 1 Electro performance of base material or plating material (Silver) degrades over time such that
fails.
Corrective Action - Define the electro performance for base material and plate material. Add the
testing of electro performance of material including base material and plate material into the
Quality control process.
Red Factor 2 Degrade the silver plated contacts such that and lower the electro performance.
Corrective Action - To silver plating, base should be pre-plated by some other metal whose plate
voltage is less than silver and then plate silver. And add the test of the pre -plate's material's
performance into the Quality control process.
Red Factor 3 No Passivation in the electro-plate process. Silver plate is not protected and It will act with
Sulfate,Chloride ion and Hydrogen sulfide. Electro performance of silver sulfate and silver
sulfide is very poor.
Corrective Action – Add passivation process into the plate process.
Red Factor 4 Performance of passivation oxidation film is poor for silver plated contacts.
Corrective Action - identify what kind of passivation file is and test its electro performance.
Yellow Factor 5 No contact resistance measurement @ IQC or in functional testing.
Corrective Action – Electronic tests to implement contact resistance (should be < 0.5 Ohms).
Yellow Factor 6 No system to make sure silver plated contacts are degraded or contaminated.
Corrective Action – Same as in Red Factor 3
Out Put Connector View - On the connector edge, there seems to be material that may possibly obstruct with fully mating of the connector
The fixture looked new with no signs of use nor overheating
Input Connector - It looks like the female receptacle has spread open more than normal.
Failures Resolved – Power Cable bringing on safety hazard fire incidents
51
Cross Section of Distorted Output (Male) Connector
The burned pin is the LINE connection Here it is shown Male connector mated with the female connector. Looks like misalignment
It appears the LINE pin is pushed into the connector and is visibly burned. The pin does not appear to be broken. Suspect the female connector is only making partial contact with the mating male pin
52
Failures Resolved – Power Cable bringing on safety hazard fire incidents
The burned pin is the LINE connection – Cross Section Here it is shown Male connector mated with the female connector. Looks like misalignment
It appears the LINE pin is pushed into the connector and is visibly burned. The pin does not appear to be broken. Suspect the female connector is only making partial contact with the mating male pin
53
Manufacturing Process Pictorial Presentation – Improvement through Molding Process
5/31/2013 ©2007 PHILIPS
SOLID STATE LIGHTING
SOLUTIONS. ALL RIGHTS Pag
RESERVED. PRIVATE AND e 48
CONFIDENTIAL
54
Failures Resolved – Chip on Bond
55
55
Concept of Advanced Failure Analysis Tests for Chip on Bond
56
Non Destructive 3D X-Ray Failure Analysis
57
Non Destructive 3D X-Ray Failure Analysis
58
Non Destructive 3D X-Ray Failure Analysis
59
IC Destructive Failure Analysis (De-Capsulation / Scanning Electron Microscope)
(Please click on picture below for further details)
60
Peculiar Observations
(Please click on picture below for further observations)
61
5 Why Analysis
I C o lor C ov e Q LX F ixtures
1) W hy U nits found to be inoperativ e 1 s t W hy
N o LE D Illum ination
2) W hy no LE D Illum ination for R ed or B lue LE D ’s 2 nd W hy
P C B A inac tiv e in ternally @ c ritical com ponents
3) W hy P C BA inac tiv e inside 3 rd W hy
IC U 2 output v oltage or current fall short of th resho ld lev el
4) W hy IC U 2 output fall short of th resho ld lev el 4 th W hy
IC U 2 fails e lec tronically
5) W hy IC U 2 fails e lec tron ically 5 th W hy
S igna ls of ov erheating incidents possib ly constitu ing failu re during therm al perform ance.
F ailu re Code – N o R e d or B lue LE D Illum ination or U nits are inoperativ e .
F ailu re M ode – IC U 2 fails e lectronically due to wire bonds open @ pads for respec tiv e LE D failu re .
F ailu re E ffect – O pen circuit @ bond pads for respec tive LE D failu re .
F ailure M echanism – 1st W ire bonds suffer sev ere frac ture or cracks @ heel of bonds .
P o ssible cau se s :
1 ) S igna ls of ov erheating incidents possib ly constitu ting failu re of bonded wires @ wafer ch ip.
P ro b able/Ro o t cau se :
1 ) S am e as abov e. T h is is just a hypothetical assum ption, no prov en fac t. DO E is under conception phase to v erify th rough v arious product sam ples suc h as forward /bonded rev erse bonded, short w ire bonds e tc. D eta ils of DO E with resu lts to be dec lared at la ter stage s..
(T entativ ely resu lts w ill be av ailab le by W k 2 3).
62
Proposed Corrective Actions for Contract Manufacturer
63
1) Confirm wire bonding setup is correct. Wire bond machine should be calibrated.
2) Confirm wire in the spool or machine is of correct size and alloy.
3) Confirm secured and not corrupted copy of wire bond program in machine.
4) Using calibrated thermometer verify heated stage has correct temperature.
5) Bond surfaces must be smooth , clean (no – contamination).
6) PCBA must be held rigidly (not allowed to move) during wire bonding.
7) Check consistency of free wire bond related free air balls, diameter is 1.5 X wire diameter.
Failures resolved – Water Ingress due to Poly Carbonate Lens crack demonstration
@ LED Luminaires
Prone to crack due to various factors
1) Environmental Stress Corrosion Cracking, 2) Severe Chemical Attack 3) Lens Manufacturing due to
improper molding process or no annealing. Extensive analysis done by PCK Burlington and SZ FAE Team.
64
Node of LED Fixture
Above cracks are random and propagate through the length or width of Back Clip
Cracks analyzed due to ---
a) Plastics molding process and b) Polymers break @ different temperatures during storage of finished goods in ware house
c) Moisture effect
Back Clip Crack
Cracked PC Plastic chipped off
Back Clip
Failures resolved - PC Plastic Cracks @ Back Clip
65
Failures resolved – PC Plastic Cracks @ Screw Boss
Separation
Above cracks are random and propagate through the length or width of Back Clip
Cracks analyzed due to ---
66
a) b)
c)
Plastics molding process and Polymers break @ different temperatures during storage of finished goods in ware house
Moisture effect
Failure Reproduction: Results of Accelerated Testing (Vibration Testing)
67
Failure Reproduction: Results of Accelerated Testing (Vibration Testing)
68
Material Analysis --- FTIR and SEM Results
1)The FTIR analysis indicates that the materials of the cracked or good, housing are highly similar
with BPA as one of key Plasticizer.
2)Micro cracks were not found in the selected cracked housings. However cracked screw bosses
were severe.
3)The cracks are not necessarily located near the main crack. It may lie independently on the surface
away from the edge. The length is in the order of tens of micrometer.
69
Material Analysis --- MFR and DSC Report for failure samples
1) Few comments from SGS Report --- a) Environmental Stress Cracks. b) Plastic material not dried or have moisture. c) Plastic material storage malpractice as partially opened bags. d) Plastic material contains brittle transparent thermoplastic (PMMA) amounting to about
2%.
e) Plastic molding over processed or over-cooked. f) Melt screw position and weight of molding shot every cycle.
g) Average Molecular Weight reduction of plastic housing.
70
Material Analysis --- MFR Results for failure samples
e x t e n d e d r e s i d e n c e t i m e , a n d i n s o m e c a s e s i n a d e q u a t e m o i s t u r e r e m o v a l p r i o r t o p r o c e s s i n g .
R F H
Sample No. Test
item
Test
method
Test
condition
Result Specs of Melt Flow
Rate
Date
code
Sample Description Material of
housing
Result
#1 Melt ASTM D1238-
10
Drying
condition:
17.7g/10min > 15 g/10min 1135 No crack RFH Fail
Specs
#2 10.4g/10min < Specs 15 g/10min 1212 Crack RFH Pass
#3 10.7g/10min within Specs 10-12 g/10min 1217 No crack RFG Pass
#4 12.6g/10min > Specs 10-12 g/10min 1214 No crack RFG ---
#5 17.7g/10min > 15 g/10min 1134 Crack RFH Fail
Specs
#6 17.9g/10min > 15 g/10min 1134 No crack RFG Fail
Specs
mass Procedure 1 to 6 Extracted from Finished Goods of V-Tech Warehouse. Fixtures housing manufactured in Gold Asia
Test
flow A and
#7 rate 8.83g/10min<Specs 10-12 g/10min NA Resin of Top Housing (W H) Resin and
Housing samples
collected from
Good View from
product line (RFG
Material)
Fail 250℃,
requirement
2.16kg #8 8.13g/10min<Specs 10-12 g/10min NA Resin of Housing (GR) Fail
#9 (10.5+/-0.8)g / 10
min
10-12 g/10min NA Top Housing (W H) ---
#10 10.5+/-0.2)g / 10
min
10-12 g/10min NA Top Housing (GR) ---
#11 10.8+/-0.7)g / 10
min
10-12 g/10min NA Bottom Housing (GR) Pass
#12 12.2+/-0.5)g / 10
min
10-12 g/10min NA Bottom Housing (W H) ---
Yellow colored
shows f ailed test
Indications –
“---“Very close to specs that cannot be concluded, “WH” – White, “GR” – Gray Implications –
a) The basic property measured is the melt viscosity or flow resistance of the polymer at a particular shear stress (related to the applied load) and temperature. b) Polymer chains of short length and simple geometry “slide” past one another relatively easily and offer little flow resistance. In contrast, long chains of high
molecular weight and more complex structure yield greater flow resistance or viscosity. E.g. The MFR, an indicator of average molecular weight and is inversely related to it. A resin with an MFR of 50 g/10 min indicates a lower molecular weight than one with an MFR. of 10 g/10 min. While a higher MFR material may be easier to process, physical properties related to molecular weight, such as impact resistance, are often lower…
Conclusion -
1) Every failure sample tested for MFR has lower molecular weight…
2) This indicates material is prone to degrade over period of time which usually is the case when material is over cooked or over processed.
3) The most common cause of brittle behavior is polymer degradation, the reduction in the average
71
Material Analysis --- FTIR Results for failure samples
N o T e s t I t e m T e s t
M e t h o d
T e s t
C o n d i t i
o n
M a jo r C o m p o s i t i o n
D a t e c o d e S a m p l e
D e s c r i p t i o n
M a t e r i a l o f
h o u s in g
1 M a jo r
C o m p o s i t
i o n
Q u a l i t a t i v
e
A n a l y s i s
F T I R a n d
P G C - M S
N A P o l y c a r b o n a t e ( P C ) a n d a c r y l o n i t r i l e - b u t a d i e n e - s t y r e n e
( C o p o l y m e r A B S ) 1 1 3 5 N o c r a c k R F H
2 P o l y c a r b o n a t e ( P C ) , P o l y ( M e t h y l M e t h a c r y l a t e ) ( P M M A )
a n d a c r y l o n i t r i l e - b u t a d i e n e - s t y r e n e c o p o l y m e r ( A B S ) 1 2 1 2 C r a c k R F H
3 P o l y c a r b o n a t e ( P C ) , P o l y ( M e t h y l M e t h a c r y l a t e ) ( P M M A )
a n d a c r y l o n i t r i l e - b u t a d i e n e - s t y r e n e c o p o l y m e r ( A B S ) 1 2 1 7 N o c r a c k R F G
4 P o l y c a r b o n a t e ( P C ) , P o l y ( M e t h y l M e t h a c r y l a t e ) ( P M M A )
a n d a c r y l o n i t r i l e - b u t a d i e n e - s t y r e n e c o p o l y m e r ( A B S ) 1 2 1 4 N o c r a c k R F G
5 P o l y c a r b o n a t e ( P C ) a n d a c r y l o n i t r i l e - b u t a d i e n e - s t y r e n e
( C o p o l y m e r A B S ) 1 1 3 4 C r a c k R F H
6 P o l y c a r b o n a t e ( P C ) a n d a c r y l o n i t r i l e - b u t a d i e n e - s t y r e n e
( C o p o l y m e r A B S ) 1 1 3 4 N o c r a c k R F H
1 t o 6 E x t r a c t e d f r o m F i n i s h e d G o o d s o f V - T e c h W a r e h o u s e . F i x t u r e s h o u s i n g m a n u f a c t u r e d i n G o l d A s i a
7 P o l y c a r b o n a t e ( P C ) , P o l y ( M e t h y l M e t h a c r y l a t e ) ( P M M A )
a n d a c r y l o n i t r i l e - b u t a d i e n e - s t y r e n e c o p o l y m e r ( A B S ) N A
R e s in o f T o p
H o u s i n g ( W H )
R e s i n a n d
H o u s i n g
s a m p l e s
c o l l e c t e d f r o m
G o o d V i e w
f r o m p r o d u c t
l i n e ( R F G
M a t e r i a l )
8 P o l y c a r b o n a t e ( P C ) , P o l y ( M e t h y l M e t h a c r y l a t e ) ( P M M A )
a n d a c r y l o n i t r i l e - b u t a d i e n e - s t y r e n e c o p o l y m e r ( A B S ) N A
R e s in o f
H o u s i n g ( G R )
9 P o l y c a r b o n a t e ( P C ) , P o l y ( M e t h y l M e t h a c r y l a t e ) ( P M M A )
a n d a c r y l o n i t r i l e - b u t a d i e n e - s t y r e n e c o p o l y m e r ( A B S ) N A
T o p H o u s in g
( W H )
1 0 P o l y c a r b o n a t e ( P C ) , P o l y ( M e t h y l M e t h a c r y l a t e ) ( P M M A )
a n d a c r y l o n i t r i l e - b u t a d i e n e - s t y r e n e c o p o l y m e r ( A B S ) N A
T o p H o u s in g
( G R )
1 1 P o l y c a r b o n a t e ( P C ) , P o l y ( M e t h y l M e t h a c r y l a t e ) ( P M M A )
a n d a c r y l o n i t r i l e - b u t a d i e n e - s t y r e n e c o p o l y m e r ( A B S ) N A
B o t t o m
H o u s i n g ( G R )
1 2 P o l y c a r b o n a t e ( P C ) , P o l y ( M e t h y l M e t h a c r y l a t e ) ( P M M A )
a n d a c r y l o n i t r i l e - b u t a d i e n e - s t y r e n e c o p o l y m e r ( A B S ) N A
B o t t o m
H o u s i n g ( W H )
Y e l l o w c o l o r e d i n d i c a t e s s a m p l e s t e s t e d c o n t a i n P M M A , W H = W h i t e , G R = G r a y
C o n c l u s i o n –
1 ) Y e l l o w c o l o r e d t e s t e d s a m p l e s i n d i c a t e F T I R S p e c t r a o f P M M A .
2 ) P M M A - - - i s a t r a n s p a r e n t t h e r m o p l a s t i c , o f t e n u s e d a s a l i g h t w e i g h t o r s h a t t e r - r e s i s t a n t a l t e r n a t i v e t o g l a s s . P M M A i s a n e c o n o m i c a l a l t e r n a t i v e t o p o l y c a r b o n a t e ( P C ) w h e n e x t r e m e
s t r e n g t h i s n o t n e c e s s a r y . A d d i t i o n a l l y , P M M A d o e s n o t c o n t a i n t h e p o t e n t i a l l y h a r m f u l b i s p h e n o l - A s u b u n i t s f o u n d i n p o l y c a r b o n a t e
3 ) P M M A h e a t r e s i s t a n c e i s n o t g o o d e n o u g h . T h e t h e r m a l d e f o r m a t i o n t e m p e r a t u r e i s b e t w e e n
( 7 4 ~ 1 0 2 ) ℃ . 4 ) T h e m e l t v i s c o s i t y i s h i g h , p o o r l i q u i d i t y ; c o o l i n g s p e e d i s t o o f a s t , e a s y t o h a v e t h e i n t e r n a l
s t r e s s o f p r o d u c t .
5 ) P M M A p r o d u c t s i n s t o r e d a n d d u r i n g t h e u s e w i t h e a s y t o o c c u r s i l v e r s t r e a k s ;
S i l v e r s t r e a k s a r e g l a s s s t a t e p o l y m e r b r i t t l e f r a c t u r e o f t h e p r e r e q u i s i t e s , s i l v e r s t r e a k s o f
m a t e r i a l i n t h e c r a c k c a u s e d b y a c r a c k i n g a n d e x p a n s i o n , s o t h a t l e a d t o c r a c k i n g .
6 ) A s p e r M S D S o f R F G a n d R F H m a t e r i a l s P M M A i s n o t m e n t i o n e d . H e n c e t h i s i s a n a d d i t i o n a l
o r e x t e r n a l l y a d d e d s u b s t a n c e .
RFG
72
Material Analysis --- DSC Results for failure samples
o T e
s t
I t e
m
T e s t
M e t h o
d
T e s t C o n d i t i o n R e s u l t ( d e g r e e C ) < S p e c s o f 1 5 0 d e g r e e C
D a t e
c o d e
S a m p l e
D e s c r i p t i o n
M a t e r i a l o f
h o u s i n g R e s u l t
G l
a s
s
T r a
n s i
t i o
n
T e
m p
e r a
t u r
e
( T g
)
W i t h r e f e r e n c e t o
A S T M D 3 4 1 8
- 0 8 , a n a l y s i s w a s
p e r f o r m e d b y
E n d o t h e r m i c D S C
T e m p e r a t u r e
R a n g e :
0 t o 2 0 0
d e g r e e C
R a m p : 2 0
d e g r e e C / m i n
N 2 : 5 0 m l / m i n
F i r s t h e a t s c a n 1 0 7 . 8
S e c o n d h e a t s c a n 1 0 3 . 7 1 1 3 5 N o c r a c k R F H F a i l
F i r s t h e a t s c a n 1 1 3 . 1
S e c o n d h e a t s c a n 1 1 1 . 9 1 2 1 2 C r a c k R F H P a s s
F i r s t h e a t s c a n 1 1 3 . 9
S e c o n d h e a t s c a n 1 1 2 . 0 1 2 1 7 N o c r a c k R F G P a s s
F i r s t h e a t s c a n 1 1 1 . 2
S e c o n d h e a t s c a n 1 0 6 . 5 1 2 1 4 N o c r a c k R F G - - -
F i r s t h e a t s c a n 1 0 8 . 0
S e c o n d h e a t s c a n 1 0 5 . 9 1 1 3 4 C r a c k R F H F a i l
F i r s t h e a t s c a n 1 0 6 . 8
S e c o n d h e a t s c a n 1 0 5 . 6 1 1 3 4 N o c r a c k R F H F a i l
1 t o 6 E x t r a c t e d f r o m F i n i s h e d G o o d s o f V - T e c h W a r e h o u s e . F i x t u r e s h o u s i n g m a n u f a c t u r e d i n G o l d A s i a
F i r s t h e a t s c a n T g 1 = 1 0 3 . 1 , T g 2 = 1 1 5 . 0
S e c o n d h e a t s c a n = 1 1 1 . 7 N A
R e s i n o f T o p
H o u s i n g ( W H ) R e s i n a n d
H o u s i n g
s a m p l e s
c o l l e c t e d
f r o m
G o o d
V i e w f r o m
p r o d u c t
l i n e ( R F G
M a t e r i a l )
F a i l
F i r s t h e a t s c a n = 1 1 0 . 6
S e c o n d h e a t s c a n = 1 0 9 . 7 N A
R e s i n o f
H o u s i n g ( G R ) F a i l
F i r s t h e a t s c a n = 1 1 2 . 6
S e c o n d h e a t s c a n = 1 1 1 . 5 N A
T o p H o u s i n g
( W H ) - - -
0 F i r s t h e a t s c a n = 1 1 0 . 2
S e c o n d h e a t s c a n = 1 1 0 . 9 N A
T o p H o u s i n g
( G R ) - - -
1 F i r s t h e a t s c a n = 1 1 2 . 2
S e c o n d h e a t s c a n = 1 1 0 . 6 N A
B o t t o m
H o u s i n g ( G R ) P a s s
2 F i r s t h e a t s c a n = 1 1 1 . 6
S e c o n d h e a t s c a n = 1 1 0 . 0 N A
B o t t o m
H o u s i n g ( W H ) - - -
Y e l l o w c o l o r e d s h o w s T g l o w e r t h e n s p e c i f i c a t i o n , W H = W h i t e , G R = G r a y
I m p l i c a t i o n s –
1 ) D i f f e r e n t i a l S c a n n i n g C a l o r i m e t r y ( D S C ) m e a s u r e s t h e t e m p e r a t u r e s a n d h e a t f l o w s a s s o c i a t e d w i t h T r a n s i t i o n s i n m a t e r i a l s a s a f u n c t i o n o f t i m e a n d t e m p e r a t u r e i n a c o n t r o l l e d a t m o s p h e r e .
2 ) T h e s e m e a s u r e m e n t s p r o v i d e q u a n t i t a t i v e a n d q u a l i t a t i v e i n f o r m a t i o n a b o u t p h y s i c a l a n d c h e m i c a l C h a n g e s t h a t i n v o l v e e n d o t h e r m i c o r e x o t h e r m i c p r o c e s s e s o r c h a n g e s i n h e a t c a p a c i t y .
3 ) D S C c a n m e a s u r e G l a s s T r a n s i t i o n s , M e l t i n g a n d B o i l i n g P o i n t s , C r y s t a l l i z a t i o n t i m e a n d t e m p e r a t u r e , P e r c e n t C r y s t a l l i n i t y , H e a t s o f F u s i o n a n d R e a c t i o n s , S p e c i f i c H e a t , O x i d a t iv e / T h e r m a l S t a b i l i t y , R a t e a n d D e g r e e o f C u r e R e a c t i o n K i n e t i c s , P u r i t y .
4 ) A c a l o r i m e t e r m e a s u r e s t h e h e a t i n t o o r o u t o f a s a m p l e . A d i f f e r e n t i a l c a l o r i m e t e r m e a s u r e s t h e h e a t o f a s a m p l e r e l a t i v e t o a r e f e r e n c e . A d i f f e r e n t i a l s c a n n i n g c a l o r i m e t e r d o e s a l l o f t h e a b o v e a n d h e a t s t h e s a m p l e w i t h a l i n e a r t e m p e r a t u r e r a m p . E n d o t h e r m i c h e a t f l o w s i n t o t h e s a m p l e . E x o t h e r m i c h e a t f l o w s o u t o f t h e s a m p l e .
5 ) A m o r p h o u s p o l y m e r u s u a l l y h a s t h r e e p h y s i c a l f o r m s : G l a s s y s t a t e , H i g h - e l a s t i c s t a t e a n d t h e v i s c o u s f l o w s t a t e , f r o m t h e G l a s s y s t a t e t r a n s i t i o n t o t h e H i g h - e l a s t i c , t h e t e m p e r a t u r e p o i n t i s c a l l e d G l a s s t r a n s i t i o n t e m p e r a t u r e .
C o n c l u s i o n – 6 ) E v e r y f a i l u r e s a m p l e t e s t e d f o r D S C h a s l o w e r G l a s s T r a n s i t i o n T e m p e r a t u r e t h e n
s p e c i f i c a t i o n … 7 ) D i f f e r e n t i a l S c a n n i n g C a l o r i m e t r y ( D S C ) m e a s u r e d l o w e r t e m p e r a t u r e s a n d h e a t f l o w s
a s s o c i a t e d w i t h t r a n s i t i o n s i n m a t e r i a l s a s a f u n c t i o n o f t i m e a n d t e m p e r a t u r e i n a c o n t r o l l e d a t m o s p h e r e . T h i s i n d i c a t e s f o r t e s t e d s a m p l e s s o f t e n i n g , m e l t i n g a n d r e c r y s t a l l i z a t i o n c a n
h a p p e n a t T g < S p e c s .
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Fishbone Diagram
74
Fishbone Diagram Rating
75
Cause and Effect Rating Target Environment - Environment Stress Cracks 90 90
Plastic material not dried or have moisture 70 90
Plastic material storage malpractice as partially opened bags 40 90
Plastic material contains brittle transparent thermoplastic (Such as PMMA) 70 90
Screw Boss has micro cracks after manufacturing 1 90
Machines - Plastic Molding over processed or Over Cooked 90 90
Plastic Molding Machine - Melt Screw Position and weight of molding shot every cycle 80 90
Plastic Housing are highly stressed due to design 20 90
Average Molecular Weight reduction of Plastic Housing 40 90
Good and Cracked samples have different chemical compositions (Recycled or fake materials used) 1 90
Storage conditions of finished good cause cracks 10 90
Personnel - Screw Assembly Process - Operators not trained enough for assembly 2 90
Process & Methods - Screw Assembly Process exerts force to produce cracks 2 90
Note: Rating provided is an assumption, there is no any mathemetical calculations involved
Fishbone Diagram Chart
76
NIKON ECLIPSE LV 150 Microscope Zoom In for contamination
It emphasizes on failure mechanism as “Blooming”. Viscous liquidity deposits on PVC materials is often results of plasticizers blooming to the surface. (Refer next slide for “Blooming”) The blooming out of adipate plasticizers from PVC Cable insulation is commonly observed especially in warm operating environments… Since blooming leads to an increase in the surface concentration of additive surface IR Technique called ATR (Attenuated Total Reflectance) FTIR could be most applicable to find out failure causes…
PVC Cable Contamination Advanced Failure Analysis
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PVC Cable Contamination Advanced Failure Analysis
Logical Explanation of Blooming an excerpt from “Compositional and Failure Analysis of Polymers: A
Practical Approach” Page No. 485, 486 78
Failures resolved - PCB Cold Solder Joint
Broken Metal Lines
Metal Traces – Thorough process quality auditing and
highlighting critical malpractices in PCB helped
reductions in defect %
79
Higher Magnification of Metallographic Cross Section of corroded part of material.
Corrosion is due to ---Improper Electropolishing > pitting > stress > crack >leakage.
Pitting and Stress Corrosion Cracking between Tank and Baffle Clip. Between spot
welds of Clip and Tank body.
HOT WATER TANK comprising SS304 Material - Stress CORROSION Cracks and
leakage during consumer simulation testing.
Energy Dispersive Spectroscopy Chemical Analysis of Corrosion Failure: High
Concentration of Oxides.
Failures resolved - Corrosion
80
Failures Resolved – Corrosion
81
Metallographic Cross Sectional Analysis of Stainless Steel which corrodes @ Hot Water Tank Body
Failure Mode: Stress Corrosion Cracking
Failure Mechanism: Improper Electro polish causing
--- > Critical areas of Tank not benefiting (i.e. Not polished area act as anode, polished area act as
cathode, exacerbating corrosion)
--- > Phosphoric acid trapped between critical joints left over due to Electro-polishing process.
Failure Location: Hot Water Tank Body
Failure Cause: Stainless Steel Material used is SS 304 and not L Grade. Should be SS 316Lor above.
Quality Control Test: Exaggerated Salt-Spray Testing (e.g. Hot Water Tanks subjected to 50 degree
c conditions and salt water conditions for > 75 Hrs.
Corrective Actions:
1) Modify design of Hot Water Tank to avoid stress.
2) Change material to SS316L
3) Long term testing with metallurgical assessment that includes periodic checks on pitting /
corrosion / stress corrosion cracking.
General Failure Analysis Role @ Organization
APAC Team: Mehul and one more engineer.
USA / Europe Team: Based in Various Locations.
CM
SM
QM
82
5 0
10
15
20
25
Complaints Reported
30
Complaints Responded at 1st Line (CM)
35
40
45
50
Oct-11 Nov-11
Quarter 4 - 2011
Dec-11 Jan-12 Feb-12
Quarter 1 - 2012
Mar-12
No
. Of
Co
mp
lain
ts /
Ave
rag
e T
AT
(da
ys
)
Month
Complaints Responded at 2nd Line (SM)
Complaints Responded at 3rd Line QM
Average Turn Around Time (TAT) in Days for QM
to SM
Target Turnt Around Time (TAT) in Days for QM
to SM
Vaya Flood flicker failure @ Batumi Russia. Complaint ‘s massive time
line (to respond back) was dependant on replacement of reworked
products from China to site as well as first satisfactory performance.
Achievements --- Failure Analysis / Quality Improvement Cycle Improvement @
Philips
Complaints Reported Vs. Responded (QM to SM)
PC Lens Crack failure for
Color Graze 4 FT @
Singapore
83
Pag
e
77
0.00
2.00
6.00
Average Turn Around Time (TAT)
Target Turn Around Time (TAT) 4.00
8.00
10.00
12.00
Quarter 4 - 2011
Quarter 1 - 2012
Month
Total till date
Tu
rn A
rou
nd
Tim
e in
da
ys
Achievements --- Failure Analysis / Quality Improvement Cycle Improvement @
Philips
Turn Around Time (to respond QM to SM) Vs. Month
84
Pag
e
78
performance results took long time to realize. Service Management
did not want to accept complaint back until results declared.
0.00%
20.00%
40.00%
60.00%
80.00%
100.00%
120.00%
Oct-11 Nov-11
Quarter 4 - 2011
Dec-11 Jan-12 Feb-12
Quarter 1 - 2012
Mar-12
Eff
icie
nc
y in
Pe
rce
nta
ge
Month
Complaints resolving (Responding QM to SM) efficiency
Target efficiency
Vaya Flood flicker failure @ Batumi Russia. Complaint ‘s took down
efficiency to valley point. Responding time line affected as
reworking of units and replacement @ site and first hand
Color Blast 12 Power Core failure from New Zealand. Time line
was affected on response as necessary info from customer care
did not arrive first hand.
PC Lens crack failure for Color Graze 4 Ft due to chemical
attacks, environmental stress etc..@ Singapore OUB.
Complaint took efficiency down to 2nd Vale y Point until
70% replacements arrived @ site.
Achievements --- Failure Analysis / Quality Improvement Cycle Improvement @
Philips
85
Recognition --- Nomination for Key Award “I-Rock” by Director Of Quality Assurance
86
Recognition --- Nomination for Key Award “I-Rock” by Sr. Manager of Engineering
87
Recognition --- PHILIPS Certified Corporate Team Auditor for Mfg. Sites
88
Keurig Green Mountain --- Milestone Achievement.
89
To Replace contract manufacturers based expensive consumer tests : • Outsource and setup a Multi-Million Dollar Consumer Simulation Test Center. • Realize 1.6 M USD cost savings for FY2014.
74