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Dr. Wiesner Steuerungstechnik GmbH Weststraße 4 D-73630 Remshalden Phone +49 7151/9736-0 Fax +49 7151/9736-36 [email protected] www.drwiesner.de Industrial Leakage Testing • What does “tight” really mean? • Selecting the suitable test-method Influencing factors • Overview of leakage-test methods

Dr. Wiesner Steuerungstechnik GmbH...Dr. Wiesner Steuerungstechnik GmbH Weststraße 4 D-73630 Remshalden Phone +49 7151/9736-0 Fax +49 7151/9736-36 [email protected] Industrial Leakage

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Page 1: Dr. Wiesner Steuerungstechnik GmbH...Dr. Wiesner Steuerungstechnik GmbH Weststraße 4 D-73630 Remshalden Phone +49 7151/9736-0 Fax +49 7151/9736-36 info@drwiesner.de Industrial Leakage

Dr. WiesnerSteuerungstechnik GmbH

Weststraße 4D-73630 RemshaldenPhone +49 7151/9736-0Fax +49 7151/[email protected]

Industrial Leakage Testing

• What does “tight” really mean?• Selecting the suitable test-method • Influencing factors• Overview of leakage-test methods

Page 2: Dr. Wiesner Steuerungstechnik GmbH...Dr. Wiesner Steuerungstechnik GmbH Weststraße 4 D-73630 Remshalden Phone +49 7151/9736-0 Fax +49 7151/9736-36 info@drwiesner.de Industrial Leakage

Tight or untight?

Change in the tire pressure of your car amounts to

• 0.1 bar per minute• 0.1 bar per hour• 0.1 bar per day• 0.1 bar per week• 0.1 bar per month• 0.1 bar per year

Is your tire tight or not?

Page 3: Dr. Wiesner Steuerungstechnik GmbH...Dr. Wiesner Steuerungstechnik GmbH Weststraße 4 D-73630 Remshalden Phone +49 7151/9736-0 Fax +49 7151/9736-36 info@drwiesner.de Industrial Leakage

Pressure drop Leakage rate

0.1 bar/minute rough untight 3880 cm³/min

0.1 bar/hour unacceptable 64.7 cm³/min

0.1 bar/dayacceptable in somesituations

2.7 cm³/min

0.1 bar/week tolerable 0.39 cm³/min

0.1 bar/month acceptable 0.09 cm³/min

0.1 bar/year tight 0.0074 cm³/min

Pressure drop in a car tire

Tire diameter 630 mm; rim-base diameter 350 mm; width 180 mm; filling volume 38.8 l; (215/65 R15)Loss of pressure from 2.5 to 2.4 bar

Holding your tire underwater, you find within oneminute• 100 air bubbles• 10 air bubbles• one air bubble• no air bubble

Is your tire tight or not?

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0.1 bar/minute 3880 cm³/min ~924.000 air bubbles/min

0.1 bar/hour 64.7 cm³/min ~15.400 air bubbles/min

0.1 bar/day 2.7 cm³/min ~640 air bubbles/min

0.1 bar/week 0.39 cm³/min 93 air bubbles/min

0.1 bar/month 0.09 cm³/min 21 air bubbles/min

0,1 bar/year 0,0074 cm³/min 1.8 air bubbles/min

Pressure drop in a car tire

Assumed diameter of air bubble d=2 mm; V = 0.0042 cm3

(at d=1 mm: V= 0.00052 cm3 / at d= 3mm: V= 0.014 cm3)

Comparison of admissible leakage rates

Pressure drop in a car tire

Leakage rate Examples appliedto:

0.1 bar/minute 3.880 cm³/min car exhaust muffler(or catalytic converter)

0.1 bar/day 2.7 cm³/min water pump(also applicable to AdBlue®)

0.1 bar/year 0.009 cm³/min fuel tank(gasoline)

0.1 bar/~150 years 0.00006 cm³/min coolant circulationsystem (refrigerator)

Page 5: Dr. Wiesner Steuerungstechnik GmbH...Dr. Wiesner Steuerungstechnik GmbH Weststraße 4 D-73630 Remshalden Phone +49 7151/9736-0 Fax +49 7151/9736-36 info@drwiesner.de Industrial Leakage

• Required tightness dependents on the application and usage of the component

• The admissible leakage rate requires to be defined

“tight” only means

measured leakage rate < admissible leakage rate

Admissible leakage ratesIn the industrial testing sector, leakage is tested against various types of medium applying air or other gases.

The following standard values are used:

CharacteristicAir leakagefrom to

waterproof 0.5 cm³/min 12 cm³/min

oil-proof 0.6 cm³/min 4.5 cm³/min

gasoline-proof0.0006 cm³/min(benzol gas)

3 cm³/min(liquid)

gas-tight derived from application

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Definition of leakage rate:

Admissible current of (air)volume per unit of time Units:- cm³/min or ml/min- l/min- mbar l/s

Admissible change in pressure per unit of timeUnits:- mbar/s- mbar/min

Additional information requirements:

• Height of test-pressure or -vacuum

• Where admissible pressure drop is specified: test volume

• Special loads, if any, in the course of testing

Where the admissible leakage rate and test conditions are not specified, these must be derived from the real conditions under which the component will be used.

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Conversion: leakage rate / change in pressure

To assess the required test resolution when selecting a pressure-test method or in order to standardize any admissible change in pressure in alignment with a leakage rate, an approximate 1 conversion is carried out based on the Boyle-Mariotte Law.

1 Not taking into account changes in temperature occurring in the course of testing and disregarding real air pressure.

cm³/minml/min l/min mbar l/s Pa m³/s

1 cm³/min1 ml/min 1 0.001 0.0167 0.00167

1 l/min 1 000 1 16.667 1.667

1 mbar l/s* 60 0.060 1 0.1

1 Pa m ³/s* 6 0.006 10 1

Leakage-rate conversion

* 1 mbar l/s (1 Pa m 3/s) corresponds to the amount of leakage causing change in pressureof one mbar (Pa) per second in a volume of one liter (m3).

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Test-method identification

This takes place on the basis of:

• leakage rate• properties of test specimen• production conditions• aspects relating to specific field of application• testing costs• required test documentation

Leakage rates and suitable test methods

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Properties of test specimen

• Elasticity of test specimen• Hermetically sealed test volume• Highly heat-conductive materials

Production conditions• Special temperature conditions?

• Necessity to carry out leakage detection?• Influencing ambient processes?

Other criteria for selecting suitable test methods

Aspects relating to specific field of application

• Pressure ratios relating to specific application?• Mechanical stress relating to specific application?• Is it necessary to incorporate functional testing?

Testing costs• Unit costs in respect of jigs and fixtures

• Cost of consumption per test• Personnel costs• Unit costs in respect of maintenance, calibration and upkeep

Other criteria for selecting suitable test methods

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Other criteria for selecting suitable test methods

Required proof of quality

• Precise quantification of leakage rate required?• Manual rating allowed?• Documentation of test data required?

Influencing variables

Is 0.1 bar change in pressure detectable in this way?

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Influencing variables

• Different test methods

• Inadequate measuring accuracy• Non-reproducible adaptation• Operator influences• Physical influences• Behavior of test specimen• Process-specific influences

Clamping and sealing devicesDesign guidelines

No stress on testing area caused by tensional or sealing forces

Implementation:

Fork beds incorporating counter-holding functionSealing head fitted with expanding gasket

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Clamping and sealing devicesDesign guidelines

Adaptation corresponding as far as possible to specific field of application

Implementation:

Inflatable gasket sleeve, fitted to a hose nipple from outside

Clamping and sealing devicesDesign guidelines

Minimization of wear on the sealing components of the clamping and sealing deviceto prevent pseudo-rejections

Implementation:Use of a gasket corresponding to the original, but manufactured from material extremely resistant to wear

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Clamping and sealing devicesDesign guidelines

Closed flux of force at point of adaptation at high testing pressure(Example: Bursting-pressure test).

Low influence on test specimen as a result of adaptation

Rating criteria for the both principle different leakage-test methods

Air-pressure measuring and testing methods

+ Low investment and running costs, simple operation.- Sensitive to changes in temperature, depending on behavior of test

specimen, sensitivity depends on test pressure and test volume.

Gas verification methods – sniff test / integral test+ Very low leakage rates detectable, insensitive to changes in temperature- High investment and running costs, mostly unsuitable for big leakages

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Pressure-testing methodsAir-under-water testing

Method: Test specimen is filled with pressure and moved under water. Bubbles at points of leakage are mostly observed visually or, in seldom cases detected by a ultrasonic sensor equipment.

Pressure-testing methodsAir-under-water testing

Test medium: Compressed air or nitrogenDetectable leakage rates: > 0.1 cm³/minAdvantages: - simple leakage detectionDisadvantages: - test specimens get wet

- often high costs caused by water preraration- operator-dependent- quantitative leakage-rate determination

difficult

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Pressure-testing methodsBubbling through method

Method: Test specimen is filled with pressure. Air escaping at points of leakage is refilled and made visible through bubbles appearing in a water inspection glass.

Pressure-testing methodsBubbling through method

Test medium: Compressed air, nitrogen or vacuumDetectable leakage rates: > 0.1 cm³/min (depending on pressure)Advantages: - robust, simple and extremley low-cost

method- no wetting of test specimens

Disadvantages: - operator-dependent rating- quantitative leakage-rate determination

difficult

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Pressure-testing methodsBubbling through method

Bubbling throughtest unit

Pressure-testing methodsGeneral features

Method: The test chamber is filled with compressed air (or in more seldom cases with pressurised nitrogen or other gases) or evacuated and shut off. The change occurring in pressure due to leakage is measured and evaluated .

Advantages: - automatable- operator-independent evaluation - low costs - quantifiable leakage-rate determination - automatic documentation capability of test results

Disadvantages: - test result influenced by thermal and elastic changesoccurring to test specimen

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Pressure-testing methodsRelative -pressure method

(absolute-pressure or pressure-differential method)

Detectable leakage rates:Volume- and pressure-depending >1 cm³/min

Advantage:Simple, low-cost method

Disadvantage:Test resolution dependent on test pressure

Pressure-testing methods Relative -pressure method

(absolute-pressure or pressure-differential method)

Simple, low-cost relative-pressure test unit

LTScompact

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Pressure-testing methodsDifferential-pressure method

Detectable leakage rates:Volume- and pressure-depending>0.1 cm³/min

Advantage:Test resolution independent of test pressure

Disadvantage:Testing technology involves higher complexity

Pressure-testing methods

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Pressure-testing methodsDifferential-pressure method

State-of-the-art differential-pressure

test unitINTEGRA DD6

Pressure-testing methodsPressure-rise method

Special feature: pressure-rise is measured inside a hood surrounding the test specimen

Detectable leakage rates: volume-depending >0.1 cm³/min

Advantages: - faster tests possible- suitable for tests with very high testing

pressure

Disadvantages: - high mechanical complexity- evaluation uncertain if test hood is untight

(additional effort for supervision)

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Pressure-testing methodsTesting of hermetically sealed components under a test hood

Special feature: The volume inside a hood surrounding the testspecimen is filled with pressure or evacuated. The pressure change, caused by the specimen inthis volume is measured and evaluated.

Detectable leakage rates: volume-depending >0.1 cm³/min

IMPORTANT: Requires an additional pre-test against roughleakage. In addition, the internal volume of the testspecimen must be at least 5 – 10% of the sum total resulting from the dead volume of thetest hood + tube volume + test-circuit volume.

Pressure-testing methodsTesting of hermetically sealed components under a test hood

Basic diagram showing relative-pressure test implementation

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Pressure-testing methods Testing of hermetically sealed components under a test hood

Gas verification methods

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Gas verification methodsSniff test – general features

Method: Pressurised test gas is filled into a test chamber. The test gas escaping at points of leakage is detected by a probe, primarily operated on manual lines.

Advantages: - independent of temperature and elasticity- leakage point detection is possible

Disadvantages: - operator-dependent evaluation- quantitative leakage-rate determination difficult - risk of working area contamination

Gas verification methodsHydrogen sniff test

Test medium: Forming gas (5% hydrogen / 95% nitrogen)

Detectable leakage rates: >0.0001 cm³/min

Advantages: - simple applicationDisadvantages: - natural constituent of hydrogen in

atmosphere restrictive (0.5 ppm) - sometimes unsuitable for testing plastic

parts due to high hydrogen permeation - risk of cross-sensitivity when testing

anodised aluminum components

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Gas verification methodsHydrogen sniff test

Hydrogen sniffer

Gas verification methodsHelium sniff test

- natural constituent of helium in atmosphererestrictive (5 ppm)

- sometimes unsuitable for testing plasticcomponents due to high helium permeation

Disadvantages:

- very low leakage rates verifiableAdvantages:

>0.00001 cm³/minDetectable leakage rates:

Helium, pure or mixed with N2 or airTest medium :

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Gas verification methods

Helium sniffer

Gas verification methodsIntegral test – general features

Method: Pressurised test gas is filled into a test chamber. Slightest traces of test gas escaping at points of leakage into a test hook are automatically detected.

Advantages: - operator-independent evaluation - no influence on test result due to thermal and elastic changes occurring to test specimen

- quantifiable leakage-rate determination - automatic documentation capability of test results

Disadvantages: - high mechanical complexity - risk of test-gas contamination due to maloperation orcoarse leakage

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Gas verification methodsHydrogen test method (integral test)

Test medium: Forming gas (5% hydrogen / 95% nitrogen)non-combustible

Sensitivity: 1-2 ppmAdvantages: - no vacuum inside test hook

- low effort for sensory and mechanical systems

- test gas easily removableDisadvantages: - 0.5 ppm hydrogen present in natural atmosphere

- sometimes unsuitable for testing plastic components due to high hydrogen permeation

Gas verification methodsHydrogen test method (integral test)

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Gas verification methodsLaser leakage-test method (integral test)

- sensory system costlyDisadvantages:

- very low leakage rates verifiable- no high-vacuum necessary - robust, sensory system insensitive to

interference- in most cases low gas consumption costs - no disturbing influences through natural

constituent in atmosphere

Advantages:

>0.0001 cm³/minDetectable leakage rates:

Gas mixture from air or N2 primarily with very low proportion of sulfur hexafluoride (SF6).

Test medium:

Gas verification methodsLaser leakage-test method (integral test)

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Gas verification methodsLaser leakage-test method (integral test)

Complete system forlaser leakage-test method

Gas verification methodsHelium mass-spectrometer method (integral test)

- sensory system costly and sensitive- very high outlay for peripherals and test

chambers- 5 ppm helium present in natural

atmosphere- sensitive to moisture and dirt- in most cases unsuitable for leakage rates

above 0.1 cm3/min

Disadvantages:

- extremely low leakage rates verifiable- oldest and most widespread gas

verification method

Advantages:

>10-10 mbar l/sDetectable leakage rates:

Gas mixture from air or N2and heliumTest medium:

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Gas verification methodsHelium mass-spectrometer method (integral test)

Diagram illustrating helium integral leakage-test method

Other leakage-test methods

• Flow test method (volume flow)Specially for larger admissible leakage rates

• Flow test method (mass flow)Also for minor leakage rates. Disadvantage: critical applied to rough leakage

• Laser scan methodGas detection verification method for automatically leakage localisation of leakage rates > 0.01 cm3/min. Disadvantage: very costly

• Ultrasonic leakage-test methodManually applied method for detecting sound generated by escaping gas. As an alternative, ultrasonic sources are deployed in the interior of the test specimen. Suitable for localisation of major leakages on very large test objects.

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Other leakage-test methods

From practically all the methods previously specified, special applications can be derived catering for better simulation of the conditions to which the test specimens are subjected in actual practice or even for making the test possible at all:

• Pressure or test-gas admittance internally or externally• Internal or external vacuum testing• Special pressure-testing methods for hermetically sealed

components• Cambering for test-gas testing of hermetically sealed components