1
EUV Mask Observation Result Using Coherent EUV Scatterometry Microscope with High-Harmonic-Generation EUV Source Tetsuo Harada 1 , Takahiro Fujino 1 , Yusuke Tanaka 1 , Yutaka Nagata 1,2 , Takeo Watanabe 1 , and Hiroo Kinoshita 1 1. Center for EUV Lithography, LASTI, University of Hyogo 2 RIKEN 2. RIKEN Introduction Coherent EUV Scatterometry Microscope (CSM) We have developed THREE types of coherent EUV scatterometry microscopes (CSM), which was based on coherent diff ti i i th d (SR CSM Mi CSM HHG CSM) z An EUV mask should be inspected at-wavelength, because the mask has 3D structure of absorber and Mo/Si multilayer There are some wavelength- and E-mail: [email protected] z Sample was exposed with coherent EUV light. 1. SR-CSM 2. Micro-CSM Wavelength: 13.5 nm (EUV) Source: Synchrotron (NewSUBARU) Focusing sizeΦ5 μm NA: 0.14 diffraction imaging method. (SR-CSM, Micro-CSM, HHG-CSM) Wavelength: 13.5 nm (EUV) Source: Synchrotron (NewSUBARU) Focusing sizeΦ230 nm NA: 0.27 z Illumination EUV is focused using Fresnel zone plate to Φ230 nm. Mo/Si multilayer . There are some wavelength- and structure-specific issues of a phase defect, shadowing effect, and absorber phase, for example. z An EUV microscope is a key tool for EUV mask development. z We have been developed EUV microscopes for EUV mask evaluation using a synchrotron radiation z Diffraction signal is recorded with CCD camera directly. z Pattern image is reconstructed with iterative calculation with the diffraction image. NA: 0.14 Cross line 128 nm Line/space Phase defect L NA: 0 14 li li ) Relation with phase defect shape Detection limit of phase defect 2 1 z For phase defect imaging. (Phase imaging) (Phase imaging result will be presented in MNC2014 conference next week.) EUV mask evaluation using a synchrotron radiation source of NewSUBARU. z This poster is about coherent EUV scatterometry microscope (CSM) using coherent diffraction imaging method without objective. The CSM can image phase distribution. z Since we would like to apply the CSM for order diffractions 0th +1st -1st order diffractions Log NA: 0.14 linear linear Diffraction image (Reciprocal Space) + 4 μm -1 4 μm -1 4 μm -1 20 30 40 50 60 70 80 90100 10 20 30 40 50 60 S/N ratio (dB) and diffraction shape. 25 nm, D1.4 nm JVST B 2013 JVST B 2013 z Since we would like to apply the CSM for industrial use, a laboratory source of high-harmonic- generation (HHG) EUV source has been developed with a laser group in RIKEN. At-wavelength EUV mask evaluation of Objective μm Sq. Phase Defect Cross W2 μm Reconstructed image (Amplitude + Phase) Defect width on glass substrate (nm) Relation of defect signal and substrate speckle Defect signal variation 2013 2013 3D effect with laboratory source. Coherent EUV Scatterometry Microscope (CSM) High-harmonic-generation PHASE imaging + High Harmonic Generation EUV S JJAP 2014 JJAP 2014 z CSM system images phase distribution. z Absorber phase and shadowing effect in phase were actually observed. z Quantitative phase value of phase defect was achieved. High-harmonic-generation (HHG) EUV source Laboratory coherent EUV source EUV Source 3. HHG-CSM Specification z High-harmonic-generation (HHG) source emits coherent EUV light. z The brilliance of the HHG is higher than the NS synchrotron (Bending) light. z The source is LAB SCALE source, which can apply industrial tool. Wavelength: 13.5 nm (EUV) Source: HHG EUV source Focusing sizeΦ4.3 μm NA: 0.14 Pumping l Focusing ti HHG ll EUV Output HHG Source Size Stability 0 7 um (rms) Position Stability Improvement (New) z Feedback system corrects the beam position. (Piezo Mirror x 2, PSD x 2) z Position stability is very high of 0.7 μm (rms) in an hour. z We upgraded relay optics to “single laser optics gas cell Output Wavelength: 800 nm Near Infrared 6 mJ/pulse 30 fs duration R3 m Concave φ85 μm focus 10 15 W/cm 2 Helium gas ~ 17 kPa Non-linear Interaction 59th wavelength conversion 800/59 ~ 13.5 nm HHG emission HHG position stability (1hr) 0.7 um (rms) Previous Result relaysystem. The source image was directly relayed on the mask surface using a concave mirror. z Previous system used two concave, and a pinhole. (Twice RELAY) (Twice relay system) HHG spectrum 0.2 TW Brilliance HHG Performance (Current status) 200 nW, φ48 μm, 0.18 mrad, δλ 0.1 nm HHG (13.5 nm) 1.3 × 10 14 NewSUBARU Bending 6 × 10 12 NewSUBARU Undulator 6 × 10 17 photons/sec/0.1%BW/mm 2 /mrad 2 HP 45 nm (180 nm on Mask) hole pattern array Center hole is bigger than other. EXP.time: 1,000s too long time for detection Differenial SEM CSM O i df t HHG spectrum Absorber Defect Observation Result Without defect With defect Over size defect 40 nm SEM CSM Defect signals from various size Diffraction from Defect Without Defect With Defect SEM Over size defect 40 nm HP 45 nm (180 nm on Mask) hole pattern array z Absorber defects in hp 45 nm hole pattern (180 nm on mask) were detected using HHG-CSM. z This experiment is for detection-limit evaluation. z Exposure time was dramatically improved 0th order diffraction 1st order diffractions Line end over defect EXP.time: 10 s Defect with 12 nm width was detected! to 10 s compared to previous result. z Various type of defects were detected. Absorber defects detection from diffraction pattern z Detection limit of the defect was 12-nm line-end over size, which area was 2,160 nm 2 . This area was equivalent to the square Diffraction from Defect Summary Line end over defect 80 nm defect with area of 46 x 46 nm 2 . Without Defect With Defect z We have developed CSM with HHG EUV source. This HHG-CSM is for at-wavelength EUV mask evaluation of 3D effect with laboratory source. z The beam position was stabilized to 0.7 μm (rms) in an hour using feedback system. Thus, we upgraded the relay optics from twice relay to single relay system. zExposure time and the detection size limit were dramatically improved to 10 s and 12-nm with line –end over defect. This defect area size of 2,160 nm 2 was equivalent to the square defect with area of 46 x 46 nm 2 . z The CSM system has high capability to evaluate small structure. We will continuously evaluate the EUV mask structure with amplitude and “PHASE image”.

EUV Mask Observation Result Using Coherent EUV ...euvlsymposium.lbl.gov/pdf/2014/4a9897e45aa744f2850b65346aa59055.pdf · 1st order diffractions Line end over defect 40 nm EXP.time:

  • Upload
    others

  • View
    2

  • Download
    1

Embed Size (px)

Citation preview

Page 1: EUV Mask Observation Result Using Coherent EUV ...euvlsymposium.lbl.gov/pdf/2014/4a9897e45aa744f2850b65346aa59055.pdf · 1st order diffractions Line end over defect 40 nm EXP.time:

EUV Mask Observation Result Using Coherent EUV Scatterometry Microscope with High-Harmonic-Generation EUV Source

Tetsuo Harada1, Takahiro Fujino1, Yusuke Tanaka1, Yutaka Nagata1,2, Takeo Watanabe1, and Hiroo Kinoshita1

1. Center for EUV Lithography, LASTI, University of Hyogo2 RIKEN2. RIKEN

Introduction Coherent EUV Scatterometry Microscope (CSM)

We have developed THREE types of coherent EUV scatterometry microscopes (CSM), which was based on coherent diff ti i i th d (SR CSM Mi CSM HHG CSM)

An EUV mask should be inspected at-wavelength, because the mask has 3D structure of absorber and Mo/Si multilayer There are some wavelength- and

E-mail: [email protected]

Sample was exposed with coherent EUV light.

1. SR-CSM 2. Micro-CSMWavelength: 13.5 nm (EUV)Source: Synchrotron (NewSUBARU)Focusing size: Φ5 μmNA: 0.14

diffraction imaging method. (SR-CSM, Micro-CSM, HHG-CSM)Wavelength: 13.5 nm (EUV)Source: Synchrotron (NewSUBARU)Focusing size: Φ230 nmNA: 0.27

Illumination EUV is focused using Fresnel zone plate to Φ230 nm.

Mo/Si multilayer. There are some wavelength- and structure-specific issues of a phase defect, shadowing effect, and absorber phase, for example.

An EUV microscope is a key tool for EUV mask development.

We have been developed EUV microscopes for EUV mask evaluation using a synchrotron radiation

Diffraction signal is recorded with CCD camera directly.

Pattern image is reconstructed with iterative calculation with the diffraction image.

NA: 0.14Cross line 128 nm Line/space Phase defect

LNA: 0 14 lili) Relation with phase defect shape  Detection limit of phase defect 2 1

For phase defect imaging. (Phase imaging)(Phase imaging result will be presented in MNC2014 conference next week.)

EUV mask evaluation using a synchrotron radiation source of NewSUBARU.

This poster is about coherent EUV scatterometry microscope (CSM) using coherent diffraction imaging method without objective. The CSM can image phase distribution.

Since we would like to apply the CSM for

order diffractions0th +1st-1st

order diffractions

LogNA: 0.14 linearlinear

Diff

ract

ion

imag

e (R

ecip

roca

l Spa

ce)

+

4 μm-1 4 μm-1 4 μm-1

20 30 40 50 60 70 80 9010010

20

30

40

50

60

S/N

rat

io (

dB

)

and diffraction shape. 25 nm, D1.4 nm

JVST B2013

JVST B2013

Since we would like to apply the CSM for industrial use, a laboratory source of high-harmonic-generation (HHG) EUV source has been developed with a laser group in RIKEN.

At-wavelength EUV mask evaluation of Objective

1μm Sq.Phase Defect

CrossW2 μmR

econ

stru

cted

im

age

(Am

plitu

de +

Pha

se)

Defect width on glass substrate (nm)

Relation of defect signal and substrate speckleDefect signal variation

201320133D effect with laboratory source.

Coherent EUV Scatterometry Microscope (CSM)

High-harmonic-generation

PHASE imaging+

High Harmonic Generation EUV S

JJAP2014

JJAP2014

CSM system images phase distribution.Absorber phase and shadowing effect in phase were actually observed.Quantitative phase value of phase defect was achieved.

High-harmonic-generation (HHG) EUV source

Laboratory coherent EUV source

EUV Source

3. HHG-CSMSpecification High-harmonic-generation (HHG) source emits coherent EUV light.

The brilliance of the HHG is higher than the NS synchrotron (Bending) light.

The source is LAB SCALE source, which can apply industrial tool.

Wavelength: 13.5 nm (EUV)Source: HHG EUV sourceFocusing size: Φ4.3 μmNA: 0.14

Pumpingl

Focusingti

HHG ll

EUVOutput

HHG Source Size

Stability0 7 um (rms)

Position Stability Improvement (New) Feedback system corrects the beam position. (Piezo Mirror x 2, PSD x 2)

Position stability is very high of 0.7 μm (rms) in an hour.

We upgraded relay optics to “single ”laser optics gas cell Output

Wavelength:800 nm

Near Infrared

6 mJ/pulse30 fs duration

R3 m Concaveφ85 μm focus

1015 W/cm2

Helium gas~ 17 kPa

Non-linearInteraction

59th wavelength conversion

800/59 ~ 13.5 nm HHG emission

HHG position stability (1hr)

0.7 um (rms)

Previous Result

relay” system. The source image was directly relayed on the mask surface using a concave mirror.

Previous system used two concave, and a pinhole. (Twice RELAY)(Twice relay system)

HHG spectrum0.2 TW

Brilliance

HHG Performance (Current status) 200 nW, φ48 μm, 0.18 mrad, δλ 0.1 nm

HHG (13.5 nm) 1.3 × 1014

NewSUBARU Bending 6 × 1012

NewSUBARU Undulator 6 × 1017

photons/sec/0.1%BW/mm2/mrad2

HP 45 nm (180 nm on Mask) hole pattern arrayCenter hole is bigger than other.EXP.time: 1,000stoo long time for detection

DifferentialSEM CSM

O i d f t

HHG spectrum

Absorber Defect Observation Result

Without defect With defectOver size defect40 nm

SEM

CSMDefect signals from various sizeDiffraction from Defect

Without Defect With Defect

SEM

Over size defect40 nm

gHP 45 nm 

(180 nm on Mask)hole pattern array

Absorber defects in hp 45 nm hole pattern (180 nm on mask) were detected using HHG-CSM.

This experiment is for detection-limit evaluation.

Exposure time was dramatically improved

0th order diffraction

1st order diffractionsLine end over defect

40 nm

EXP.time: 10 s

Defect with 12 nm width was detected!

p y pto 10 s compared to previous result.

Various type of defects were detected.

Absorber defects detection from diffraction pattern

Detection limit of the defect was 12-nm line-end over size, which area was 2,160 nm2. This area was equivalent to the square

Diffraction from Defect

Summary

Line end over defect80 nm

q qdefect with area of 46 x 46 nm2.

Without Defect With Defect

We have developed CSM with HHG EUV source. This HHG-CSM is for at-wavelength EUV mask evaluation of 3D effect with laboratory source.The beam position was stabilized to 0.7 μm (rms) in an hour using feedback system. Thus, we upgraded the relay optics from twice relay to single relay system.Exposure time and the detection size limit were dramatically improved to 10 s and 12-nm with line –end over defect. This defect area size of 2,160 nm2 was equivalent

to the square defect with area of 46 x 46 nm2.The CSM system has high capability to evaluate small structure. We will continuously evaluate the EUV mask structure with amplitude and “PHASE image”.