-
7/25/2019 Exemple Spectre
1/41
9.0 8.5 8.0 7.5 7.0
2.102.00 1.981.87
6.
82
6.
82
6.8
5
6.
85
6.
90
6.
91
7.
50
7.
53
9.2
7
OH1
2
3
4
5
6
7
8
9
10
11
OH12
220 200 180 160 140 120 100 80 60 40 20 0 -20
0.
00
39.
01
39.
29
39.
56
39.
86
40.
1
378.
00
78.
43
78.
87
107.
34
115.
20
122.
67
128.
85
136.
27
155.
52
-
7/25/2019 Exemple Spectre
2/41
7.55 7.50 7.45 7.40 7.35 7.30 7.25 7.20 7.15 7.10 7.05 7.00 6.95
6.90 6.85 6.80 6.75
2.102.00 1.98
6.
82
6.
82
6.
85
6.
85
6.
90
6.9
17.
50
7.
53
OH1
2
3
4
5
6
7
8
9
10
11
OH12
-
7/25/2019 Exemple Spectre
3/41
7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0
4.11 3.062.00 0.78
O1
CH3
2
3
4
5
6
7
8
9
10
11
12
OH13
160 152 144 136 128 120 112 104 96 88 80 72 64 56
5
5
.2
5
7
6
.5
9
7
7
.0
1
7
7
.4
3
1
0
4
.7
5
1
0
8
.8
6
1
1
5
.2
0
1
1
6
.2
2
1
2
4
.3
7
1
2
9
.2
5
1
2
9
.5
6
1
3
5
.9
2
1
5
3
.9
1
1
5
8
.1
6
-
7/25/2019 Exemple Spectre
4/41
7.70 7.65 7.60 7.55 7.50 7.45 7.40 7.35 7.30 7.25 7.20 7.15 7.10
7.05 7.00 6.95 6.90 6.85 6.80
2.032.00 1.96
O1
CH3
2
3
4
5
6
7
8
9
10
11
12
OH13
-
7/25/2019 Exemple Spectre
5/41
INTA
OO
OO
NN
O
N
N
O
-
7/25/2019 Exemple Spectre
6/41
7.85 7.80 7.75 7.70 7.65 7.60 7.55 7.50 7.45 7.40 7.35 7.30 7.25
7.20 7.15 7.10 7.05Chemical Shift (m!
0
0.05
0.10
0.15
0.20
0.25
I"te"#it$
2.02 1.00 0.990.98 0.95
Chl%&%f%&m-'
7.
82 7
.80
7.
77 7
.74 7
.55
7.
54
7.
25
7.
24
7.
23
7.
21
7.
21
7.
12
7.
11
7.
09
7.
08
7.
07
7.
06
O)O
1* 1
2
33*
2*
4+ , 22 H3, H3'
3+ , 85
1 1*2 2/
3+ , 85 4+ , 2.5
-
7/25/2019 Exemple Spectre
7/41
8.4 8.3 8.2 8.1 8.0 7.9 7.8 7.7 7.6 7.5 7.4 7.3 7.2 7.1
7.0Chemical Shift (m!
0
0.05
0.10
0.15
0.20
0.25
0.30
0.35
0.40
0.45
I"te"#
it$
3.91 2.02 1.951.95 1.00 0.990.98 0.95
Chl%&%f%&m-'
8.
37
8.
35
7.
99
7.
97
7.
97
7.
95
7.
82
7.
80
7.
77
7.
74
7.
55 7
.54
7.
25
7.
24
7.
23
7.
21
7.
21
7.
12
7.
11
7.
09
7.
07
7.
03
7.
01
-
7/25/2019 Exemple Spectre
8/41
8.40 8.35 8.30 8.25 8.20 8.15 8.10 8.05 8.00 7.95 7.90Chemical
Shift (m!
0
0.05
0.10
0.15
0.20
0.25
0.30
0.35
0.40
I"te"#it$
3.911.95
7.9
5
7.
97
7.
97
7.
99
8.
35
8.
37
7.05 7.00 6.95Chemical Shift (m!
0
0.05
0.10
0.15
0.20
0.25
0.30
I"te"#it$
1.950.99
7.
06
7.0
3
7.
01
-
7/25/2019 Exemple Spectre
9/41
170 165 160 155 150 145 140 135 130 125 120 115 110 105Chemical
Shift (m!
-0.01
0
0.01
0.02
0.03
0.04
0.05
0.06
0.07
0.08
0.09
0.10
0.11
0.12
0.13
I"te"
#it$
164.9
6
162.6
3
156.
06
154.
23
149.
54
147.
11
135.
34
131.
28
130.
65
129.
82
129.
40
127.
18
125.
35
122.
60
118.
89
117.
77
117.
32
115.
00
109.5
8
19 C A#imet&ic
-
7/25/2019 Exemple Spectre
10/41
3.0 2.5 2.0 1.5 1.0
5.09 3.002.202.09
0.
90
0.
92
0.
95
1.
331.
36
1.
38
1.
411
.53
1.
56
1.
58
3.
33
3.
37
3.
39
C512O
85 80 75 70 65 60 55 50 45 40 35 30 25 20 15 10 5 0
1
3
.9
4
1
9
.3
6
3
1
.8
0
5
8
.5
2
7
2
.6
9
7
6
.6
9
7
7
.1
1
7
7
.5
3
3.375 3.350 3.325
2.882.21
3.
33
3.
35
3.
37
3.
39
-
7/25/2019 Exemple Spectre
11/41
1
23
O4
CH35
CH3
6
-
7/25/2019 Exemple Spectre
12/41
4.2 4.1 4.0 3.9 3.8 3.7 3.6 3.5 3.4 3.3 3.2 3.1 3.0 2.9 2.8 2.7
2.6 2.5
6.104.00
3.
39
3.
54
86 84 82 80 78 76 74 72 70 68 66 64 62 60 58 56 54
59.
01
71.
88
76.
82
77.
24
77.
66
C410O2
-
7/25/2019 Exemple Spectre
13/41
1
2O3
O4
CH35
CH3
6
22
-
7/25/2019 Exemple Spectre
14/41
3.5 3.0 2.5 2.0 1.5 1.0 0.5 0 -0.5
3.002.01
0.
00
1.
19
1.
2
1.
24
3.
01
3.0
3
3.0
6
3.
08
170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 10 0
0
.0
0
9
.9
6
4
6
.3
9
7
6
.6
4
7
7
.0
6
7
7
.4
9
1
7
0
.4
5
C35&O
-
7/25/2019 Exemple Spectre
15/41
1
2
Br3
O4
CH3
5
-
7/25/2019 Exemple Spectre
16/41
5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0
3.24 3.002.02
1.
26
1.
28
1.
31
3.
02
3.
05
3.
07
3.
10
4.
84
50 45 40 35 30 25 20 15 10 5
1
4
.6
7
3
7
.7
5
C28ClN
-
7/25/2019 Exemple Spectre
17/41
1
CH32
NH3
+
3Cl
-
4
-
7/25/2019 Exemple Spectre
18/41
3.0 2.5 2.0 1.5 1.0
3.012.962.00 1.971.00
0
.8
8
0
.9
1
0
.9
3
1
.0
4
1
.0
6
1
.1
5
1
.2
9
1
.3
01
.3
2
1
.3
21
.3
4
1
.3
6
1
.3
7
2
.7
42
.7
62
.7
8
2
.8
1
2
.8
3
2
.8
5
88 80 72 64 56 48 40 32 24 16 8 0
0
.0
0
1
0
.6
4
2
3
.5
7
3
2
.9
8
4
8
.5
4
7
6
.8
2
7
7
.2
4
7
7
.6
6
C411N
1.45 1.40 1.35 1.30
2.07
1.
34
1.
32
-
7/25/2019 Exemple Spectre
19/41
1
2 CH3
3
NH24
CH35
-
7/25/2019 Exemple Spectre
20/41
5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0
3.002.122.03 2.001.03
0.
91
1.
40
1.
42
2.02
2
.04
4.
92
4.9
6
5.
02
5.
80
.18
-
7/25/2019 Exemple Spectre
21/41
6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0 -0.5
6.143.042.00
0.
00
2
3.
35
5.
75
C711N
136 128 120 112 104 96 88 80 72 64 56 48 40 32 24 16 8 0
0
.0
0
1
2
.5
0
2
9
.9
4
7
6
.6
5
7
7
.0
7
7
7
.5
1
1
0
4
.6
8
1
2
7
.7
5
-
7/25/2019 Exemple Spectre
22/41
CH31
N2
34CH
35
6
CH37
8
2
.1
-
7/25/2019 Exemple Spectre
23/41
8.5 8.0 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0
0.5 0
6.001.910.95
0
.0
0
2
5
.7
3
5
.7
3
128 1 20 1 12 104 96 88 80 72 64 56 48 40 32 24 16 8 0 -8
0
.0
0
1
2
.9
1
7
6
.6
7
7
7
.0
9
7
7
.5
1
1
0
5
.7
5
1
2
6
.1
3
C69N
5.775 5.750 5.725 5.7005.675
1.82
5
.7
3
5
.7
3
-
7/25/2019 Exemple Spectre
24/41
CH3
12
N
H
3
4
5
6
CH37
4
-
7/25/2019 Exemple Spectre
25/41
6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0
3.002.081.020.99
1
.12
1.
1
1.
17
2.
21
2
.24
2.
26
2.
29
6.
24
6.
57
180 160 140 120 100 80 60 40 20 0
0
.0
0
9
.7
1
2
8
.9
5
7
6
.8
0
7
7
.2
4
7
7
.6
61
7
7
.3
9
C37NO
-
7/25/2019 Exemple Spectre
26/41
1
2NH23
O4
CH35
-
7/25/2019 Exemple Spectre
27/41
-
7/25/2019 Exemple Spectre
28/41
-
7/25/2019 Exemple Spectre
29/41
-
7/25/2019 Exemple Spectre
30/41
-
7/25/2019 Exemple Spectre
31/41
-
7/25/2019 Exemple Spectre
32/41
-
7/25/2019 Exemple Spectre
33/41
-
7/25/2019 Exemple Spectre
34/41
-
7/25/2019 Exemple Spectre
35/41
-
7/25/2019 Exemple Spectre
36/41
-
7/25/2019 Exemple Spectre
37/41
-
7/25/2019 Exemple Spectre
38/41
-
7/25/2019 Exemple Spectre
39/41
-
7/25/2019 Exemple Spectre
40/41
-
7/25/2019 Exemple Spectre
41/41
