島津GLC総合カタログ2017【GC充てん剤パックド …. n-Buta e カラム：ステンレ 1 0 .( 5+ ) mx 3 I D 分析温度：40 検出器：TCD サンプル：C1 ～C5

C1 C2

C1 C2 C1 C2

C1 C2

LPJIS K2240 LPJIS K2240

1

5 10 15 20

2

3

45

6

7

8

25 30 35 40

1. Hydrogen2. Oxygen 3. Nitrogen4. Carbon Monoxide5. Methane6. Carbon Dioxide7. Ethylene8. Ethane

Column : SHINCARBON ST 50/80 mesh6.0m x 3.0mm I.D., SUS

Column temp : 40 (12min hold) 200 Program rate 10 /min

Injection temp : 200 Detector : TCD (200 )Carrier gas : He, 50 mL/minSample Volume: 0.5mL

1

5 10 15 20

2

3

4

56 7

8

25 30 35 40

1. Hydrogen2. Oxygen 3. Nitrogen4. Carbon Monoxide5. Methane6. Carbon Dioxide7. Ethylene8. Ethane

Column : SHINCARBON ST 50/80 mesh6.0m x 3.0mm I.D., Stainless


Injection temp : 200 Detector : TCD (200 )Carrier gas : Ar, 50 mL/minSample Volume: 0.5mL

1

2 4 6 8

2

3

4

5 6

78

10 12 14

9

1. Oxygen2. Nitrogen 3. Carbon Monoxide4. Methane5. Carbon Dioxide

6. Nitrous Oxide7. Acetylene8. Ethylene9. Ethane



Injection temp : 200 Detector : TCD (210 )Carrier gas : He, 50 mL/min Sample Volume: 0.5mL


Column temp : 40 300 Program rate 20 /minInjection temp : 300 Detector : TCD (300 )Carrier gas : He, 50 mL/minSample Volume: 0.75mL

1

25

2 3 4 5

6

7

8

9

10

11

5 10 15

30

20

1. Air2. Carbon Monoxide 3. Methane4. Carbon Dioxide5. Ethylene6. Ethane7. Propylene8. Propane9. iso-Butane

10. n-Butane11. n-Pentane

1

2

3 4

5 10 15

Column : SHINCARBON ST 50/80 mesh 6.0m x 3.0mm I.D., SUS

Column temp : 40 Injection temp : 50 Detector : TCD (50 )Carrier gas : Ar, 50 mL/minSample Volume: 1.0mL

1. Helium2. Hydrogen 3. Oxygen4. Nitrogen

1

2

3

10

1. Oxygen2. Nitrogen 3. Methane4. Carbon Monoxide

Column : Molecular Sieve 5A 60/80 mesh1.6m x 3.2mm I.D., Glass

Column temp : 50 Injection temp : 50 Detector : TCD (50 )Carrier gas : He, 40 mL/minSample Volume: 1.0mL

1Air, Methane 2Ethane, Ethylene 3Propane 4Propylene 5iso-Butane 6n-Butane 71-Butene, iso-Butene 8trans-2-Butene 9cis-2-Butene101,3-Butadiene11iso-Pentane12n-Pentane

Column6.0 33 m 3.0 mm I.D. Stainless steel Dibutyl Maleate-Oxydipropionitrile 955 35% Shinwasorb-U 40/60Column temp.40Carrier gasHe, 20 mL/minDetectorTCD

0 5 10 15 20 25 30 35 40

1

56

7

23

10 11 12

4

138 9 14

1. Air, Methane2. Ethane3. Ethylene4. Propane5. Propylene6. iso-Butane7. n-Butane

10.0 (5+5) m x 3.0 mmI.D.40TCDC1 C5 (5000ppm)

Dibutyl Maleate + Propylene Carbonate(35:65) 35% on Shinwasorb-U 40/60

Carrier gas 20ml/min HeHead Pressure 145 kPa

https://solutions.shimadzu.co.jp/glc 513

GC

07

GLC CATALOG 2017

1

2

3

45

6

7

8

9 1011

12 13

204 8 12

24

16

1

20

2

3

4

5

6

7 8

9

10

11

13

12

4 8 12

16

24 28

32

36

1

2

2

3

4

5

6

7

84 6

LP

0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30

1

56

7

23

8 9 10 11 12 14

4

13

1. Air, Methane2. Ethane3. Ethylene4. Propane5. Propylene6. iso-Butane7. n-Butane

9.0 (3+3+3) m x 3.0 mmI.D.40TCD C2 C5 (5000ppm)

Sebaconitrile 25%on Shinwasorb-U 40/60

Carrier gas 22ml/min HeHead Pressure 180 kPa

1. Air2. Methane 3. Carbon Dioxide4. Nitrous Oxide5. Ethylene6. Ethane7. Water

Column : Sunpak-A 50/80 mesh 2.1m x 3.2mm I.D., GlassColumn temp : 40 Injection temp : 200 Detector : TCD (150 )Carrier gas : He, 40 mL/minSample Volume: 1.0mL

1. Methane2. Ethylene 3. Ethane4. Propylene5. Propane6. iso-Butane7. n-Butane8. n-Pentane9. n-Hexane

10. n-Heptane11. n-Octane12. n-Nonane13. n-Decane

Column : Sunpak-A 50/80 mesh 2.1m x 3.2mm I.D., GlassColumn temp : 65 250 Program rate 10 /minInjection temp : 260 Detector : FID (260 )Carrier gas : N2, 50 mL/minSample Volume: 0.5mL

1. Methane2. Ethane, Ethylene 3. Propane4. Propylene5. iso-Butane6. Cyclopropane7. n-Butane8. 1-Butene, iso-Butene9. trans-2-Butene

10. cis-2-Butene11. iso-Pentane12. 1,3-Butadiene13. n-Pentane

Column : SM-6 6.0m(3m+3m) x 3.0mm I.D., SUSColumn temp : 30 Injection temp : 50 Detector : FID (50 )Carrier gas : N2, 20 mL/minSample Volume: 1.0mL

Column3.0 m 2.2 mm I.D. Stainless steelSilicone DC-200 20% Shinwasorb-U 40-60Column temp.50 1 min 10/min 120Injection port temp.200DetectorFID 200Carrier gasHe, 15 mL/minSample volume0.1 mL gas

1Methane 2Ethane 3Propane 4Isobutane 5n-Butane 6Isopentane 7n-Pentane 8Isohexane 93-Methylpentane10n-Hexane

Column3.0 m 2.2 mm I.D. Stainless steelTCEP 10% Shinwasorb-U 40-60Column temp.80Injection port temp.200DetectorFID 200Carrier gasHe, 20 mL/minSample volume0.1 uL

1Benzene2Toluene3Ethylbenzene4p-, m-Xylene5o-Xylene61,2,4-Trimethylbenzene

12 3

45 6

87

910

11

1213

0 10 20 30 40

1. n-C102. n-C113. n-C124. n-C135. n-C146. n-C157. n-C168. n-C179. n-C18

10. n-C1911. n-C2012. n-C2113. n-C22

Column: 2.5 m x 3.0 mm I.D. StainlessSample: Mixture of kerosene and light oil Sample volume: 1.0 LColumn temp.: 80-250 (6 /min), 250 (12 min hold) Carrier gas: 50 mL/min N2Injection port temp.: 270 Detector: FID 270

Silicone SE- 52 5% Shinwasorb -U 40/60

514 Shimadzu GLC Ltd.

GC

07

GLC CATALOG 2017

1

2

3

4

56

7

8

0 5 10 15

Column: 2.1 m x 3.2 mm I.D. GlassSample: DMFColumn temp.: 110Injection port temp.: 230

Detector: FID 230Sample volume: 1 LCarrier gas: 50 mL/min N2

1. Benzene2. Toluene3. Ethylbenzene4. Isopropylbenzene5. n-Propylbenzene6. Styrene monomer7. Cyclopentanol8. N,N-Dimethylformamide

FON 10% Shinwasorb-S 60/80*

* Original stationary phases manufactured by Shinwa Chemical Industries Ltd.

Shinchrom F51 + Bentone34 3 + 2% Shinwasorb-U 60/80*1

2

4

5

3

0 5 10 15

1. Hexane2. Ethylbenzene3. p-Xylene4. m-Xylene5. o-Xylene

Column: 2.1 m x 3.2 mm I.D. GlassSample: 100 ppm in hexaneColumn temp.: 80Injection port temp.: 240



Column 3.0 m 2.2 mm I.D. Stainless steel TCEP 10% Shinwasorb-U 40-60Column temp. 80Injection port temp. 200Detector FID 200Carrier gas He, 20 mL/minSample volume 0.1 uL

1n-Octane 2n-Nonane 3n-Decane 4n-Undecane 5Benzene 6n-Dodecane 7Toluene 8p-Xylene 9o-Xylene101,2,4-Trimethylbenzene

Column 3.1 m 3.2 mm I.D. Glass Polyethylene glycol 1500 20% Shinwasorb-S 40-60Column temp.100

1Acetone2Ethyl acetate3Methyl ethyl ketone4Methanol

Injection port temp. 200Detector FID 200Carrier gas Nitrogen, 50 mL/minSample volume 0.1 uL

52-Propanol6Toluene7n-Butyl acetate

0 10 20 30

2

3

6

5

7

8

9

10

11

12

14

13

15

16

17

18

1

4

Column: 2.1 m x 3.2 mm I.D. Glass

Sample volume: 1.0 L

Sample: 22

Column temp.: 60120 (4 /min)

Carrier gas: 40 mL/min N2

Detector: FID 200

Injection port temp.: 200

1. Methylcyclohexane2. Acetone3. Ethyl acetate4. Methyl ethyl ketone5. Methanol6. iso -Propanol7. Ethanol, n-propylacetate8. n-Propanol, iso-butyl acetate,

methyl isobutyl ketone9. Toluene

10. n-Butyl acetate11. Ethylbenzene12. m,p-Xylene13. o-Xylene , propyleneglycol

monomethyl ether14. Styrene15. Ethyl cellosolve16. Cellosolve acetate17. Cyclohexanone18. Diacetone alcohol

PEG1500 12.5% Shinwasorb-U 40/60

1

2

345

67

8

9

10

11

12 13

14

15

16

17

18

150 5 2520

10

30

1. n-Hexane2. Methanol3. Acetone4. 2-Propanol 5. Ethyl Acetate6. Methyl Ethyl Ketone7. Benzene8. Trichloroethylene9. Isobutanol

10. Isobutyl Acetate11. Toluene12. n-Butyl Acetate13. Isoamyl Alcohol14. Ethylbenzene15. m,p-Xylene16. o-Xylene17. n-Propylbenzene18. Cyclohexanone

Column : SBS-100 10% Shimalite TPA 60/80 mesh 3.1m x 3.2mm I.D., GlassColumn temp : 110 Injection temp : 200 Detector : FID (200 )Carrier gas : N2, 30 mL/minSample Volume: 1.0 mL

12

3

4

5

6

7

8 910

11 1213

14

15

1617

82 4 12

106 14

18

16 26

24

22

20

1. Diethyl Ether2. n-Hexane3. Methanol4. Methyl Acetate 5. 2-Propanol6. Ethyl Acetate7. Tetrahydrofuran8. 2-Butanol9. Isobutanol

10. Toluene11. n-Butyl Acetate12. Methyl n-Buthyl Ketone13. Isoamyl Alcohol14. Ethylbenzene15. m,p-Xylene16. o-Xylene17. Styrene

Column : SBS-120 12% SHINCARBON A 80/100 mesh 3.1m x 3.2mm I.D., GlassColumn temp : 100 Injection temp : 200 Detector : FID (200 )Carrier gas : N2, 30 mL/minSample Volume: 1.0 mL


GC

07

GLC CATALOG 2017

12

3

4

5

6

7

8

205 10

25

15

9

10

11

12

13

14

15

1716 18

Column : SBS-200 20% Shimalite W 100/120 mesh AW -DMCS, 3.1m x 3.2mm I.D., GlassColumn temp : 100 Injection temp : 240 Detector : FID (240 )Carrier gas : N 2 , 50 mL/minSample Volume: 1.0 mL

1. Acetone2. 2-Propanol3. n-Hexane4. Ethyl Acetate 5. Chloroform6. Carbon Tetrachloride7. n-Butyl Alcohol8. Methyl Isobutyl Ketone9. Isobutyl Acetate

10. Toluene11. n-Butyl Acetate12. Ethylbenzene13. m,p-Xylene14. o-Xylene15. Cyclohexanone16. Buthyl Cellosolve17. 1,1,2,2-Tetrachloroethane18. o-Dichlorobenzene

1

2

3

4

5

6

7 8

205 10

15

9

10

1112

1. Dichloromethane2. trans-1,2-Dichloroethylene3. Chloroform4. 1,2-Dichloroethane 5. 1,1,1-Trichloroethane6. Carbon Tetrachloride

7. Trichloroethylene8. Toluene9. Tetrachloroethylene

10. Chlorobenzene11. 1,1,2,2-Tetrachloroethane12. o-Dichlorobenzene

Column : SBS-300 20% Shimalite W 80/100 mesh AW-DMCS, 3.1m x 3.2mm I.D., GlassColumn temp : 100 Injection temp : 240 Detector : FID (240 )Carrier gas : N2, 30 mL/minSample Volume: 1.0 mL

1

2

3

4

5 6

2 12

78

9

10

64 8 10

Column : Thermon-1000 5% Sunpak-A 50/80 mesh2.1m x 3.2mm I.D., Glass

Column temp : 180 Injection temp : 240

Detector : FID (240 )Carrier gas : N2, 50 mL/minSample Volume: 1.0L

1. Water2. Methanol3. Acetaldehyde4. Ethanol5. 2-Propanol6. 1-Propanol7. Ethyl Acetate8. Isobutanol9. n -Butanol

10. Isoamyl Alcohol

1

2

34

5

2 4 61. Water2. Ethanol3. Acetonitrile4. 2-Propanol5. Hexane

Column : Thermon-1000 5% Sunpak-A 50/80 mesh 2.1m x 3.2mm I.D., Glass

Column temp : 180

Injection temp : 250 Detector : FID (230 )Carrier gas : N2, 50 mL/minSample Volume: 1.0L

1

2

3

4

5

6

28

204 8 12 24

16 32

1. 2-Propanol2. Methyl Cellosolve3. n -Butanol4. 1-Methoxy -2-Propanol5. Ethyl Cellosolve6. Buthyl Cellosolve

Column : Thermon-1000 5% Sunpak-A 50/80 mesh 2.1m x 3.2mm I.D., Glass

Column temp : 170 220 Program rate 6 /minInjection temp : 260 Detector : FID (260 )Carrier gas : N2, 50 mL/minSample Volume: 1.0L

1

2,34

56

78

0 1 2 3 4 5 6 7 8 9 10

PEG 20M 5% Shinwasorb-S 60/80

Column: 2.1 m x 3.2 mm I.D. GlassColumn temp.: 90Injection port temp.: 250Detector temp.: 250 FIDSample volume: 1 LCarrier gas: 50 mL/min N2

1. Acetone (solvent)2. sec-Butanol3. n-Propanol4. iso-Butanol5. Allyl alcohol6. n-Butanol7. iso-Amyl alcohol8. n-Amyl alcohol

(1,000 ppm v/v)

0 10

1

23

4

5

6

87

Column: 2.1 m x 3.2 mm I.D. GlassSample: Low Alcohol in waterCarrier gas: 50 mL/min N2Injection port temp.: 250Sample volume: 1.0 LColumn temp.: 150Detector: 250FID)

1. Methanol2. Ethanol3. 2-Propanol4. 1-Propanol5. iso-Butane6. n-Butane7. iso-Amyl alcohol8. n-Amyl alcohol

Sunpak-H 60-80


GC

07

GLC CATALOG 2017

Diol

0 1 0 2 0

1 2

3

4

5

68

7

1. Methanol2. Acetaldehyde3. Ethanol4. Acetic acid5. n-Propanol6. Ethyl acetate7. iso-Butanol8. Active amyl alcohol

iso-amyl alcohol

Column: 2.1m x 3.2 mm I.D. GlassSample: Carrier gas: 20 mL/minN2Injection port temp.: 230Sample volume: 1.0 LColumn temp.: 150Detector: 230FID)

1

23

4

5 6

7

8

9

10

2 1264 8 10

14

16

18

1. Air2. Formaldehyde3. Acetaldehyde4. Methyl Formate5. Acetone6. Methanol7. Ethanol, 2 -Propanol8. Water, 1 -Propanol9. Acetic Acid

10. Formic Acid

Column : TSG-1 15% SHINCARBON-A 60/80 mesh 3.1m x 3.2mm I.D., Glass

Column temp : 60 180 Program rate 8 /minInjection temp : 200 Detector : TCD (200 )Carrier gas : He, 40 mL/minSample Volume: 1.0L

Sunpak-H 60-80

0 10 20 30

1

2

34

5

6

87

Sunpak-H 60-80 Sunpak-H 60-801. AcetoneAcetonitrile2-Propanol2. Dichloromethane3. MetyletylketoneMEK4. TetrahydrofuranTHF5. 1,4-Dioxane6. N,N-dimethylformamide7. DimethylsulfoxideDMSO8. Cyclohexanone

Column: 2.1 m x 3.2 mm I.D. GlassSample: in waterCarrier gas: 50 mL/min N2Injection port temp.: 250

Sample volume: 1.0 LColumn temp.: 165Detector: 250FID)

1. Ethylene glycol2. 1,2-Propanediol3. 1,3-Propanediol4. 1,3-Butanediol5. 1,4-Butanediol6. Diethylene glycolGlycerol

0 5 10 15 20

12

34

5

6

Column: 2.1 m x 3.2 mm I.D. GlassSample: Diol in waterCarrier gas: 50 mL/min N2Injection port temp.: 250

Sample volume: 1.0 LColumn temp.: 190Detector: 250FID)

1

2

204 8 12

16 24

Column : Sorbitol 12% Chromosorb W 80/100 mesh NAW 1.5m x 3.0mm I.D., Stainless

Column temp : 150 Injection temp : 230 Detector : FID (230 )Carrier gas : N2, 60 mL/minSample Volume: 1.0L

1. Ethyleneglycol2. Diethyleneglycol

1 2

3

4

5

6

5

Column : FAL-M 10% Shimalite TPA 60/80 mesh, 2.1m x 3.2mm I.D., Glass


1. Acetaldehyde2. Propionaldehyde3. Isobutylaldehyde4. n-Butylaldehyde5. Isovaleraldehyde6.n-Valeraldehyde

1

2

10

3

4

5

6 1. Acetaldehyde2. Acrolein3. Crotonaldehyde4. Paraldehyde5. Furfural6. Benzaldehyde

Column : FAL-M 10% Shimalite TPA 80/100 mesh NAW 1.5m x 3.0mm I.D., SUS



GC

07

GLC CATALOG 2017

1

23

4

5

6

724204 8 12

16

Column : FFAP + H3PO4 0.3+0.3% Graphitecarbon 60/80 mesh 1.6m x 3.2mm I.D., Glass


1. Acetic Acid2. Propionic Acid3. iso -Butyric Acid4. n -Butyric Acid5. iso -Valeric Acid6. -Valeric Acid7. n -Heptanoic Acid

1

2

3 45 6

78

9

10

204 8 12 16

24

1. Acetic Acid2. Propionic Acid3. iso -Butyric Acid4. n -Butyric Acid5. iso -Valeric Acid6. n -Valeric Acid7. iso -Caproic Acid8. n -Caproic Acid9. n -Heptanoic Acid

10. Lactic Acid

Column : Thermon-3000 5% SHINCARBON-A 60/80 mesh 1.6m x 3.2mm I.D., Glass


1 2 3

4

5

6

87

9

4 8 12 16

1. Acetic Acid2. Propionic Acid3. iso -Butyric Acid4. n-Butyric Acid5. iso -Valeric Acid6. n-Valeric Acid7. iso -Caproic Acid8. n-Caproic Acid9. n-Heptanoic Acid

Column : FAL-M 10% SHINCARBON-A 80/100 mesh 2.1m x 3.2mm I.D., Glass


12

3

4

56

7 8

0 10 20

Column: 2.1 m x 3.2 mm I.D. GlassSample: Lower free fatty acid in water (2000 ppm)Carrier gas: 50 mL/min N2Injection port temp.: 250

Sample volume: 1.0 LColumn temp.: 175Detector: 250 (FID)

1. Acetic acid2. Propionic acid3. iso-butyric acid4. n-butyric acid5. iso-valeric acid6. n-valeric avid7. iso-caproic acid8. n-caproic acid

Sunpak-H 60/80 Column3.0 m 3.0 mm I.D. Glass *FON 20% Shinwasorb-U 40-60Column temp.200Injection port temp.250DetectorFID 250Carrier gasHelium, 20 mL/minSample volume1 uL

1Acetone solvent 2Acetic acid 3Propanoic acid 4Isobutyric acid 5n-Butyric acid 6Isovaleric acid 7n-Valeric acid 8Isocapric Acid 9n-Capric acid10n-Enanthic acidEach 100 ppm w/v

Column: 2.1 m x 3.2 mm I.D. GlassSample: Column temp.: 150Injection port temp.: 250


1

2

4

5

3

9

67

8

10

0 5 10 15

1. Acetone2. Acetic acid3. Propionic acid4. Isobutyric acid5. Butyric acid6. Isovaleric acid7. Valeric acid8. Isocaproic acid9. Capric acid

10. Enanthic acid

Thermon-1000 + H3PO4 2.5 + 0.25% Shinwasorb-U 60/80

*

0 5 10 15 20 25

54

6

1 32

7

8

9

1011

min

5% Shinchrom E71 Shinwasorb-U 60/80

Column: 3.1 m x 3.2 mm I.D. GlassSample: FAME (C10C24)Carrier gas: 40 mL/min N2Injection port temp.: 250

Sample volume: 1.0 LColumn temp.: 230Detector: FID 250

1. Acetone2. C103. C124. C145. C166. C187. C18=18. C209. C22

10. C22=111. C24


GC

07

GLC CATALOG 2017

-

1 2

3

4

5

67

8

9

5 10

10

Column : Advance-DS 5% Chromosorb W 80/100 mesh AW-DMCS, 2.1m x 3.2mm I.D., Glass


1. Methyl Caprate2. Methyl Laurate3. Methyl Myristate4. Methyl Palmitate5. Methyl Stearate6. Methyl Oleate7. Methyl Linoleate8. Methyl Arachidate9. Methyl Linolenate

10. Methyl Behenate

1 2 3

4

5

6 7

8

910

204 8 12

16

24

28

32

36

Column : Shinchrom E71 5% Shimalite-TPA 60/80 mesh 3.1m x 3.2mm I.D., Glass


1. Methyl Myristate2. Methyl Palmitate3. Methyl Palmitoleate4. Methyl Stearate5. Methyl Oleate6. Methyl Linoleate7. Methyl -Linolenate8. Methyl cis-5,8,11,14,17

-Eicosapentaenoate9. Methyl cis-7,10,13,16,19

-Docosapentaenoate10. Methyl cis-4,7,10,13,16,19

-Docosahexaenoate

1Trimethylamine2Dimethylamine3Methylamine4Ethanol solvent Each 100 ppm w/v

Column3.1 m 3.2 mm I.D. GlassDiglycerolTEPKOH 7.57.51%Shinwasorb-S 60-80Column temp.70

Injection port temp.200DetectorFID 200Carrier gasNitrogen, 50 mL/minSample volume1 uL

23

4

56

1. Monomethylamine (1,000 ppm)

2. Dimethylamine (500 ppm)

3. Ethylamine (500 ppm)

4. Trimethylamine (1,000 ppm)

5. Triethylamine (500 ppm)

6. Monoethanolamine (2,000 ppm)

Column: Thermon-3000 + KOH 2+2%Sunpak-N 60/100 mesh 2.1 m x 3.2 mm I.D.

Column temp.: 120 (5 min hold) 200

Program rate: 4/minCarrier gas: N2 50 mL/minInjection: 1 mL (250)Detector: FID (250)

1

2

3

4

164 8 12

5 6

1. Air, Methane2. Ethane 3. Ammonia4. Propane5. iso-Butane, Monomethylamine6. n-Butane

Column : Thermon-3000 + KOH 2+2% Sunpak-N 60/100 mesh 2.1m x 3.2mm I.D., Glass

Column temp : 80 Injection temp : 100 Detector : TCD (100 )Carrier gas : He, 50 mL/minSample Volume: 1.0L

0 10 20

12

4

3

5

67

1. Chloroform2. 1,1,1-Trichloroethane3. Trichloroethylene4. Bromodichloromethane5. Tetrachloroethylene6. Chlorodibromomethane7. Bromoform

Silicone DC-550 10% Shinwasorb-S 60/80

Column: 3.1 m x 3.2 mm I.D. GlassSample: Standard mixture of trihalomethanes Column temp.: 90Injection port temp.: 220Detector: ECD 220Sample volume: 1 LCarrier gas: 50 mL/min N2

Column: 3.1 m x 3.2 mm I.D. GlassSample: Chlorinated solvents in airColumn temp.: 100Injection port temp.: 240

Detector: FID 240Sample volume: 1 mLCarrier gas: 30 mL/min N2

*SBS-300 10% Shinwasorb-S 60/80


1. Dichloromethane2. trans-1,2-Dichloroethylene3. Chloroform4. 1,2-Dichloroethane5. 1,1,1-Trichloroethane6. Carbon tetrachloride7. Trichloroethylene8. Toluene9. Tetrachloroethylene

10. Chlorobenzene11. 1,1,2,2,-Tetrachloroethane12. o-Dichlorobenzene

1 2 3

4

65 7 8

10

911

4 20

8 12

16

Column : SHINCARBON-ST 50/80 mesh,1.0m x 3.0mm I.D., Glass

Column temp : 170 270 Program rate: 8 Injection : 280

Detector : FID (280 )Carrier gas : N2, 50 mL/minSample Volume: 0.25L

1. Methane2. Acetylene 3. Ethylene4. Ethane5. Chloromethane6. Propylene7. Propane8. Vinylchloride9. Dichloromethane

10. iso-Butane11. n-Butane


GC

07

GLC CATALOG 2017

PCB

PCBs

PCBs

Column3.1 m 3.2 mm I.D. Glass12.5 % , -Oxydipropionitrile Shinwasorb-S 60/80 STSampleEach 1.0 ppm in benzeneSample volume1.0 LCarrier gas50 mL/min N2Column temp.70Injection port temp.180DetectorFPD S 180

1Carbonyl sulfide2Hydrogen sulfide3Carbon disulfide4Methyl mercaptan5Ethyl mercaptan6Dimethyl sulfide7Dimethyl disulfide

12

4

5 6 7

3

0 5 10 15 20

Column: 3.1 m x 3.2 mm I.D. GlassSample: Each 1.0 ppm in Benzene Column temp.: 70Injection port temp.: 180Detector: FPD 180Sample volume: 1 LCarrier gas: 50 mL/min N2

1. Carbon sulfide2. Hydrogen sulfide3. Carbon disulfide4. Methyl mercaptan5. Ethyl mercaptane6. Dimethyl sulfide7. Benzene

1,2,3-TCEP 25% Shinwasorb-S 80/100 ST 1

2

3 4

2 4 6

5

8 10

12

16

14

6 8

7

Column : Sunpak-S 80/100 mesh, 2.1m x 3.2mm I.D., GlassColumn temp : 100 Injection temp : 180 Detector : FPD (180 )Carrier gas : N2, 50 mL/minSample Volume: 1.0mL

1. Methane2. Ethane 3. Hydrogen Sulfide4. Carbonyl Sulfide5. Propane, Propylene6. Iso-Butane7. Methyl Mercaptan8. n-Butane

1

2

0 1 2 3 4

Thermon-HG 5% Shinwasorb-U 60/80*

1. Methyl mercuric chloride2. Ethyl mercuric chloride

(100 ppb in n-hexane)

Column: 0.5 m x 3.0 mm I.D. GlassColumn temp.: 160Injection port temp.: 250

Detector: ECD 250Sample volume: 1 LCarrier gas: 50 mL/min N2


0

24

25

26 27

14

1516

17

18

19

20

2122

23

13

20 40 60 80

4

1

5

78

11

12

10

3

92

0

6

Silicone OV-17 2 Shinwasorb-S 60/80

Column: 2.1 m x 3.2 mm I.D. GlassSample: KC-mix each 1.0 ppm in hexaneColumn temp.: 210Injection port temp.: 260Detector: ECD 260Sample volume: 4 LCarrier gas: 50 mL/min N2

0 20 40 60

16

17

18

19

20

21

2223

2425

26

0

14

15

4

1

5 67 8

2 1112

1310

3

9

Column: 2.1 m x 3.2 mm I.D. GlassSamp le: KC-mix each 1.0 ppm in hexane Carrier gas: 50 mL/min N2Injection port temp.: 260

Samp le volume: 4.0 LColumn temp.: 195Detector: ECD 260

2 Silicone OV-1 Shinwasorb-S 60/80 N2:50ml/min Column2.1 m 3.2 mm I.D. Glass1% Silicone OV-17 Shinwasorb-U 60/80SampleOrganophosphorus compoundsSample volume1 LCarrier gas50 mL/min N2Column temp.180-250 8/min)Injection port temp.260DetectorFPD 260

1Acetone2Dichlorvos DDVP3Methyldemeton4Methyl parathion5Parathion6EPN


GC

07

GLC CATALOG 2017

1

2

3

0 5 10 15

Sunpak-A 50/80

1. Methanol2. Propyleneglycol3. 1,3-PropanediolTrimethyleneglycol)

Column: 2.1 m x 3.2 mm I.D. GlassSample: Propyleneglycol, 1,3-propanediolCarrier gas: 50 mL/min N2

Sample volume: 1.0 LColumn temp.: 180Detector: FID 230

Injection port temp.: 200

1

43

2

5

0 5 10 15

1. Acetone2. Sorbic acid3. Dehydroacetic acid4. Benzoic acid5. trans-Stilbene

Column: 3.1 m x 3.2 mm I.D. GlassSample: PreservativesColumn temp.: 200Injection port temp.: 260



*Advance-DS + H3PO4 2 + 0.25% Shinwasorb-S 60/80

FAP-S Shinwasorb-U 60/80

1. Acetone2. 2,6-Xylenol3. o-Cresol4. Phenol5. 2,4-Xylenol6. p-Cresol7. m-Cresol8. 3,5-Xylenol9. 3,4-Xylenol

Column: 3.1 m x 3.2 mm I.D. GlassColumn temp.: 160Injection port temp.: 250


1

2

45

3

67

8 9

0 10 20 30 40

*


Column2.1 m 3.2 mm I.D. Glass12.5% Flexol 8N8 Shinwasorb-U 60/80SampleEthylene oxideSample volume100 LCarrier gas40 mL/min N2Column temp.50Injection port temp.150DetectorFID 150

1Ethylene oxide2Propylene oxide

1

2 3 4 56 78

910

11

12

13

14

15

2716

18

19

202123

22

2425

2628

17

0 10 20 30 40

Thermon-3000 5% Shinwasorb-S 80/100 *

1. Hexane2. -Pinene3. -Pinene4. Limonene5. n-Octyl aldehyde6. n-Nonyl aldehyde7. Citronellal8. n-Decyl aldehyde9. Linalool

10. Linalyl acetate

11. Isobornyl acetate (citronellol)12. Menthol13. Benzyl acetate14. Perillaldehyde15. Geraniol16. -Ionone17. Benzyl alcohol18. Rose-P19. n-Dodecyl alcohol20. Anisaldehyde

21. Methyl cinnamate22. Ethyl cinnamate23. Eugenol24. Heliotropin25. Diethyl phthalate26. Vanillin27. Benzyl benzoate28. Benzyl salicylate

Column: 2.1 m x 3.2 mm I.D. GlassSample: Column temp.: 80-2606 /min)Injection port temp.: 280Detector: FID 280Sample volume: 1 LCarrier gas: 50 mL/min N2* Original stationary phases manufactured by Shinwa Chemical Industries Ltd.

2

3

41

0 5 10 15 20

1. Ethyl acetate2. di-n-butyl phthalate3. Teprenone (mono-cis isomer)4. Teprenone (all-trans isomer)The resolution between the mono-cis andall trance-isomers of teprenone: 1.69

FFAP 5% Shinwasorb-U 80/100

Column: 2.1 m x 3.2 mm I.D. GlassSample: TeprenoneColumn temp.: 235Injection port temp.: 270

Sample volume: 2.0 LCarrier gas: 47 mL/min N2Detector: FID 270

2

3

4

1

0 5 10 15 20

1. Ethyl acetate2. di-n-butyl phthalate3. Teprenone (mono-cis isomer)4. Teprenone (all-trans isomer): 1.63

FON 5% Shinwasorb-U 80/100*

Column: 2.1 m x 3.2 mm I.D. GlassSample: TeprenoneColumn temp.: 235Injection port temp.: 270Detector temp.: FID 270Sample volume: 2 LCarrier gas: 47 mL/min N2

* Original stationary phases manufactured by Shinwa Chemical Industries Ltd.* Conform to Japanese Pharmacopeia


GC

07

GLC CATALOG 2017

d- , dl-


Column: 5.1 m x 3.2 mm I.D. GlassSample: 200 ppm in hexaneColumn temp.: 120 /130Injection port temp.: 200Detector temp.: 200 FIDSample volume: 2 LCarrier gas: 40 mL/min N2

0 10 20 30

12

3

0 10 20 30

12

3

1. Limonene2. Cineole

121.81(1.5)

3. Anisole

Thermon-3000 5% Shinwasorb-S 80/100 Column temp.: 130*

Thermon-3000 5% Shinwasorb-S 80/100 Column temp.: 120*

1. Limonene2. Cineole

121.98(1.5)

3. Anisole

Apiezone L + KOH 2+1% Shinwasorb-S 80/100

Column: 2.1 m x 3.2 mm I.D. GlassSample: Column temp.: 125 (5 min hold) 150 (5 /min)

150 (10 min holdInjection port temp.: 200Detector: FID 200Sample volume: 2 LCarrier gas: 50 mL/min N2

1. Chloroform2. Ethanol3. Naphthalene4. Amantadine

1

2

3

4

0 5 10 15 20

Silicone SE-52 2.5% Shinwasorb-S 80/100

2

3

1

0 2 4 6 8 10 12

1. N,N-dimethylformamide

2. Triphenylantimony

3. Spectinomycin

5

2

Column: 0.6 m x 3.2 mm I.D. Glass

Sample volume: 1.0 LDetector: FID 220

Sample: N,N-dimethylformamide, Triphenylantimony, SpectinomycinColumn temp.: 180Injection port temp.: 215Carrier gas: 37 mL/min N (Adjust so that the retention time of spectinomycin is about 10 minutes.)

DEGS 1.5% Shinwasorb-S 60/80

1

3

2

0 5 10 15

1. Ethyl acetate2. Caf feine3. o-Toluene sulfonamide

4.4

o-2

Column: 1.0 m x 3.0 mm I.D. Glass Sample volume: 1.0 LSample: Ethyl acetate, Caffeine, o-Toluene sulfonamide Detector: FID 250Column temp.: 210Injection port temp.: 225Carrier gas: 55 mL/min N (adjust so that the retention time of caffeine is about 6 minutes.)

PEG600+PEG1500 5+5% Shinwasorb-S 100/120

1. Acetone2. 1-Propanol

1

2

0 1 2 3 4 5 6

Column: 2.1 m x 3.2 mm I.D. GlassSample: Acetone, 1-Propanol Column temp.: 100Injection port temp.: 115Detector: FID 120Sample volume: 1 LCarrier gas: 50 mL/min N2

Column: 3.1 m x 3.2 mm I.D. GlassSample: HypromellosesColumn temp.: 110Injection port temp.: 150Detector: FID 150Sample volume: 2 LCarrier gas: 30 mL/min N2

Silicone DC 200 10% Shinwasorb-S 80/100

1. Methyl iodide2. iso-Propyl iodide3. n-Octane4. o-Xylene

0 5 10 15 20

1

2

3

4

PEG20M 5% Shinwasorb-S 60/80

Column: 3.1 m x 3.2 mm I.D. GlassSample: Ethanol, d-Comphor, Methyl salicylateColumn temp.: 160Injection port temp.: 200Detector: FID 200Sample volume: 2 LCarrier gas: 45 mL/min N2

1

2

3

1. Ethanol2. d-Comphor3. Methyl salicylate

0 3 6 9 12 15 18


GC

07

GLC CATALOG 2017

Silicone OV-17 1% Shinwasorb-S 60/80

Column: 1.6 m x 3.2 mm I.D. GlassSample: /Column temp.: 210Injection port temp.: 270Detector: FID 270Sample volume: 2 LCarrier gas: 40 mL/min N2

0 1 2 3 4 5 6 7 8

1

2

1. 2.

4.3 (3)

Silicone OV-17 1% Shinwasorb-S 60/80

1

2

1. 2.

9.7(6)

0 2 4 6 8 10

Column: 1.6 m x 3.2 mm I.D. GlassSample: /Column temp.: 210Injection port temp.: 250Detector: FID 250Sample volume: 2 LCarrier gas: 45 mL/min N2

1

2

0 2 4 6 8 10

DEGA+H3PO4 2.5+0.5% Shinwasorb-S 80/100

1. n-valeric acid2. valproic acid

n-: 8.85

Column: 2.1 m x 3.2 mm I.D. GlassSample: n-valericacid, valproic acid/ formic acid, methyl acetate (1:1) Sample volume: 2.0 LColumn temp.: 145 Carrier gas: 35 mL/min N2Injection port temp.: 200 Detector: FID 200

0 5 10

1

2 1. acetone2. styrene

PEG20M 7.5% Shinwasorb-S 80/100

27641.03(8000.81.2 )

Column: 2.1 m x 3.2 mm I.D. GlassSample: acetone, styrene Sample volume: 5.0 LColumn temp.: 90 Carrier gas: 60 mL/min N2Injection port temp.: 200 Detector: FID 200

PEG6000 12.5% Shinwasorb-S 60/80

PEG6000 25% Chromosorb-W 60/80 AW-DMCS

12 3

0 1 0 2 0 3 0

1

2

3

0 1 0 2 0 3 0

1. ethanol2. n-ethyl caprylate3. L-menthol

1. ethanol2. n-ethyl caprylate3. L-menthol

12.6

5

6.5

5

Column: 2.1 m x 3.2 mm I.D. Glass Sample volume: 1.0 LSample: ethanol, n-ethyl caprylate, L-menthol Carrier gas: 33 mL/min N2 (Shinwasorb) Column temp.: 140 Carrier gas: 28 mL/min N2 (Chromosorb-W) Injection port temp.: 200 Detector: FID 200

Porapak-Q 80/100

0 5 10 15 20

12

Sunpak-A 80/100

0 5 10 15 20

1

2

8.1

2

12.0

2

1. ethanol2. 1-propanol

1. ethanol2. 1-propanol

Column: 1.6 m x 3.2 mm I.D. Glass Sample volume: 1.0 LSample: ethanol (solvent), 1-propanol Carrier gas: 30 mL/min N2 (Sunpak-A)Column temp.: 115 (Sunpak-A) / 125 (Porapak-Q) Carrier gas: 33 mL/min N2 (Porapak-Q) Injection port temp.: 200 Detector: FID 200


GC

07

GLC CATALOG 2017

12

0 10 20 30 40

DEGS 12.5% Shinwasorb-S 60/80

1. docosanoic acid methyl2. ethyl icosapentate

4.93.0

Column: 1.8 m x 4.0 mm I.D. Glass Sample volume: 3.0 LSample: docosanoicacid methyl, ethyl icosapentate Carrier gas: 47 mL/min N2 Column temp.: 210 Detector: FID 200Injection port temp.: 230

0 2 4 6 8

1

Sunpak-H 80/100

1. ethyl acetate

1445 1.04

5001.5

Column: 1.1 m x 3.2 mm I.D. Glass Sample volume: 1.0 LSample: ethyl acetate Carrier gas: 34 mL/min N2Column temp.: 130 Detector: FID 200Injection port temp.: 200

0 2 4 6 8 10

1

3

2

Sunpak-H 80/100

1. Chloroform2. Trichloroethylene3. N,N-dimethylformamide

4.2

3

Column: 1.1 m x 3.2 mm I.D. Glass Sample volume: 1.0 LSample: Chloroform, Trichloroethylene, N,N-dimethylformamideColumn temp.: 160

Detector: FID 200

Injection port temp.: 200Carrier gas: 45 mL/min N (Adjust so that the retention time of chloroform is about 2 minutes.)

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GC

07

GLC CATALOG 2017

Documents

島津GLC総合カタログ2017【GC充てん剤 パックド …. n-Buta e カラム： ステンレ 1 0 .( 5+ ) mx 3 I D 分析温度：40 検出器：TCD サンプル：C1 ～C5

島津GLC総合カタログ2017【GC充てん剤パックド …. n-Buta e カラム：ステンレ 1 0 .( 5+ ) mx 3 I D 分析温度：40 検出器：TCD サンプル：C1 ～C5