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Creative company with infinite potential | Inorganic analysis | Organic analysis | Material physical properties analysis | Environmental radioactivity analysis KNDT&i

KNDT&i - orbitech.co.kr · Creative company with infinite potential 케이엔디티앤아이 주식회사 / 화학사업본부 / 기술연구소 서울시 구로구 구로동 197-5

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Creative company with infinite potential 케이엔디티앤아이 주식회사 / 화학사업본부 / 기술연구소

서울시 구로구 구로동 197-5 삼성IT밸리 806, 807호

# 806 Samsung IT Valley 197-5, Guro-dong Guro-gu Seoul, Korea

Tel: 02-2028-2163~4 Fax: 02-2028-2165

www.kndt.co.kr

| Inorganic analysis | Organic analysis | Material physical properties analysis | Environmental radioactivity analysis

KNDT&i

Korea Non-Destructive Testing and internet Co., Ltd02

Creative company with infinite potential KNDT&i

창의적인 기술개발 인간존중의 조직문화

고객 중심의 가치창조

| Inorganic analysis

| Organic analysis

| Material properties analysis

| Environmental radioactivity analysis

경영이념 management philosophy

To make it beneficial for you.The most powerful company for you.

회사소개

시험의뢰방법

분석장비

무기분석 ICP-MS

ICP

FIMS

유기분석 GC-MS

GC

UV-vis

HPLC

재료물성분석 PSA

TGA

DSC

Video Microscope

환경방사능분석 LSC

Low Background α-β Counting System

Information

contents04

05

06

07

08

09

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11

12

13

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18

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www.kndt.co.kr 03

KNDT&i Information

KNDT& i04

● 대 표 자 _ 이 의 종

● 설 립 일 _ 1991년 3월

● 종 업 원 _ 약 510명

● 주 소 _ 본사) 서울시 구로구 구로동 170-5 우림e-Biz 센터 805, 806호

화학사업본부 | 기술연구소) 서울시 구로구 구로동 197-5 삼성IT밸리 806, 807호

● 주요업무 _ 물질성분 검사업, 방사선 안전관리, 비파괴검사

케이엔디티앤아이(주)는

정확하고 객관적인 시험검사 연구서비스를 통한

글로벌 전문 시험검사기관입니다.

시험의뢰방법

Process

www.kndt.co.kr 05

시험방법의

유효성확인

시험의뢰 시험접수 샘플링

시료분석 시험방법확인

성적서 발행결과보고 불만사항 접수

케이엔디티앤아이 주식회사 연구소는 1997년 설립이후 화학 및 환경 엔지니어링 분야 설계 및 시공을 전문으로 수행하고 있습니다.

이러한 연구기반을 바탕으로 하여 기술력을 선도하는 벤처기업, INNO-BIZ 기업으로 선정되는 등 기술적 우위성을

인정받고 있습니다.

KNDT& i06

Applications● Environmental : Water quality, Pollution control

● Clinical : Blood, Urine, Serum

● Petrochemistry : Heavy metal and naphtha

ingredient analysis

● Semiconductor : Impurity confirmation of solvent

and water surface analysis

● Atomic energy facility : Radionuclide analysis

(isotope analysis possibility)

● The automobile : Engine oil analysis

● Geochemical

● Agriculture and food

SpecificationsRF generator : 27.12 MHz

RF power : 600-1600 W

Mass analyzer : Quadrupole

Detection limit : ppt-sub ppb level

Mass Scan (U238, Pu238)2.058E5

c/s c/s

AMULog Manual Overlay

228.313 231 232 233 234 235 236 237 238 239 240 241 242 243 244 245 248.362

1.5E5

100000

50000

0

2.058E5

1.5E5

100000

50000

0

Autoscale Zoom

2 31

Skimmer Cone Vacuum

Shadow StopLens

Figure 5. The ICP-MS interface

Sampler ConeSkimmer Cone Vacuum

Shadow StopLens

Figure 5. The ICP-MS interface

Sampler Cone

Aerosol (fine droplets)

Liquid Sample

Figure 3. Cross-flow nebulizer

ArgonNebulizerFlow

Aerosol (fine droplets)

Liquid Sample

Figure 3. Cross-flow nebulizer

ArgonNebulizerFlow

ICP-MS

ICP-MS | ICP | FIMS

무기분석 | Inductively Coupled Plasma Mass Spectrometer

www.kndt.co.kr 07

ApplicationsEnvironmental : Water, Air, Soil, Waste

Materials : Ceramic, Metal alloy, Plastics

Biological and clinical

Agriculture and food

Geochemical and metallurgical

P206.236206.104

-2520

cps

wavelength (nm)

25k

0

Zn 206.200

Plasma

Figure 7. Simplified drawing of a basic ICP system

Spectrometer Detector

Inductively Coupled Plasma Spectrometer

ICP-MS | ICP | FIMS

ICP | 무기분석

Microwave Digestion SystemPretreatment equipment●

Plasma

Figure 7. Simplified drawing of a basic ICP system

Spectrometer Detector

KNDT& i

FIMS

ICP-MS | ICP | FIMS

무기분석 | Mercury Analysis System

08

ApplicationsEnvironmental : Water, Air, Soil, Waste

Materials : Ceramic, Metal alloy, Plastics

Biological and clinical

Agriculture and food

Geochemical and metallurgical

Figure 1. Absorbance signal of sewage sludge sample 2.

0.20

0.15

0.10

0.05

0

0 10 20 30

Time (seconds)

Figure 1. Absorbance signal of sewage sludge sample 2.

0.20

0.15

0.10

0.05

0

0 10 20 30

Time (seconds)

Hg Lamp

Quartz WindowAssembly

Cell Heating 50℃

Cell

Hg Gas

Detector

Figure 2. FIMS optical diagram

Hg Lamp

Quartz WindowAssembly

Cell Heating 50℃

Cell

Hg Gas

Detector

Figure 2. FIMS optical diagram

www.kndt.co.kr 09

Gas Chromatograph Mass Spectrometer

GC-MS | GC | UV-vis | HPLC

GC-MS | 유기분석

ApplicationsAnalysis of organic composition.

(Liquid, Solid, Gas)

Environmental samples.

(Water, Soil, Detergent)

SpecificationAccessaries : Purge & Trap, Headspace●

1

1

1 2 3

4

5

6

78

9

10

11

1213

1415

16

2 3

4

5 6

7 8

9

1011

1213

14 15

16

2

0 5 10 15 20 25 30 35 min

3

4

5

6

78

9

101112 13

14 15

16Chemical derivatization

Mixture ofVolatilederivatives

GASCHROMATOGRAPH

MASSSPECTROMETER -identity components

Mixture ofchemicalconstituents

GC

GC-MS | GC | UV-vis | HPLC

유기분석 |

KNDT& i

Gas Chromatograph

10

ApplicationsAnalysis of organic composition

(Liquid, Solid, Gas)

Environmental samples

(Water, Soil, Detergent)

SpecificationDetectors : ECD, NPD, FID, PID●

TCMX_

PCB28_

PCB52_

PCB101_

PCB118_

PCB153_

PCB158_

PCB180_

PCB198_

www.kndt.co.kr 11

UV-Visible Spectrophotometer

GC-MS | GC | UV-vis | HPLC

UV-vis | 유기분석

010100010

010100010

010100010

010100010

010100010

010100010

010100010

010100010

010100010

Inside a UV/VIS Spectrophotometer

Specifications Wavelength range : 190 to 900 nm

Spectral bandwidth : 0.2 mm

Working range : 3.5 Abs

ApplicationsQuantitative analysis of DNA, RNA, Protein and

nucleic acid

Purity(QC)

HPLC

GC-MS | GC | UV-vis | HPLC

유기분석 |

KNDT& i

High Performance Liquid Chromatograph

12

Application● Analysis of compound protein, Hexane,

Hydrocarbon, Medical supplies, Terpenoid,

Pesticide, Antibiotics, Steroid,

Metal-organic and inorganic

SpecificationsDetector : UV detector (190 ㎚ ~ 600 ㎚)

Wavelength accuracy : 1.0 ㎚

Flow accuracy : <2 %

Maximum operating pressure : 6000 psi

ChromatographicProcess

Elution through the Column

BB

B+A

A

A

0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 19.00 20.00

-47.9704

95.1397

238.2498

381.3598

524.4699

2.11

67

6.01

67

time(min)

volt

age(

mV)

Application● Analysis of compound protein, Hexane,

Hydrocarbon, Medical supplies, Terpenoid,

Pesticide, Antibiotics, Steroid,

Metal-organic and inorganic

www.kndt.co.kr 13

Particle Size Analyzer

PSA | TGA | DSC | Video Microscope

PSA | 재료물성분석

Specifications Measuring range : - 0.02 ~2000 ㎛

Resolution : Results reported in 100 size classes

Laser

Fourier Lens

Particles Scattering Intensity distribution

Laser Beam

Sample Cell Detectors

1 3 5 7 9 12 15 18 21 24 27 30 33 36 39 42 45 48 51

300

200

150

100

50

0

Data Graph - Light Scattering

Glass beads, 28 January 2003 17:07:41Background data

Detector Number

Lign

tEne

rgy

d(0.5): 42.521 um d(0.9):

Particle Size Distribution

1 10 100 1000 3000

ApplicationParticle size and particle size distribution of

emulsions, Suspensions, Dry Powders and

cosmetics

TGA

DSC | TGA | PSA | Video Microscope

재료물성분석 | Thermo Gravimetric Analyzer

14

ApplicationsSolvent | Moisture | Polymer/resin | Filler | Ash

Glass | Carbon black | Evaluation of stabilizers

Loss on drying | Proximate oil analysis

Oxidation studies

Balance

SAMPLE

High Temperature Furnace

Purge Gas (oxidizing or inert)

Styrene

Polyester

Fiberglass

CaCO3

0 100 200 300 400 500 600 700 800 900 1000

40

50

60

70

80

90

100

110

4 ℃/min to 900 ℃

SpecificationsTGA furnace: Low-mass furnace with large uniform

temperature zone

Balance capacity: up to 1500 mg

Balance sensitivity: resolution: 0.2 mm

balance accuracy: ± 3 mm | Scan rate: 0.1~100 ℃/min

Tare reproducibillty: < 3 mm | Temp: 20~1000 ℃

Cooling time: With chiller 1000 to 100 ℃ under 10 min

Atmosphere : Static or dynamic, Including nitrogen,

Argon, Helium, Carbon dioxide, Air, Oxygen or other

inert or active gases, Over temperature range

Autosampler: up to 45 samples can be run unattended,

and samples can be added anytime

KNDT& i

High Temperature Furnace

www.kndt.co.kr 15

Difference Scanning Calorimeter

PSA | TGA | DSC | Video Microscope

DSC | 재료물성분석

ApplicationsGlass transition temperature

Fictive temperature

Curing studies

Melting point and crystallinity studies

Oxidative induction test

Specific heat capacity determination

using DSC

DSC kinetics

SpecificationsSensor : Precisely-machined

disc of chromel alloy

Heating Rate : 0.1 to 100 ℃/min

Cooling Rate : 0.1 to 100 ℃/min

Dynamic Range Resolution : ±175 mW

0.0

2.0

4.0

6.0

8.0

10.0

150.0 155.0 160.0 165.0 170.0

Temperature(ºC)

Hea

t Flo

w (m

W)

Weight 17.85 mg

Water Circulator

Showing the effect of DSC scanning fate on heat flow curve of an Indium sample

Scan Rate(ºC/min)

Tm Onset(C/min)

Heat of Fusion(J/g)

20.0

10.0

4.0

1.0

0.5

0.2

156.30

156.42

156.50

156.55

156.50

156.53

28.49

28.45

28.40

28.39

28.30

28.35

Epoxy-anhydride System (Totally uncured)

40 60 80 100 120 140 160 180 200 220 240 26728.04

-9.314

-5

0

5

10

15

20

25

3032.23

Uncure epoxy

Peak = 161.548ºC

Area = -9251,368mjDelta H = -362,800J/g

Heat Flux Calorimeter

Sample Reference

Single Heat Source

Video Microscope

DSC | TGA | PSA | Video Microscope

재료물성분석 |

KNDT& i

Video Microscope

16

Applications● Semiconductor : Wafer pattern, Wire bonding,

Channel of semiconductor

● PCB : PCB hole, Soldening, Pattern of whole film

● Fiber : Pattern of fiber matrix

SpecificationsLamp : 12 V / 100 W halogen lamp

Light intensity : 0~100 W

Camera image sensor : 1/3” color CCD

Camera pixel NTSC : 768(H) 494(V)

PAL : 752(H) 582(V)

● ●

www.kndt.co.kr 17

Liquid Scintillation Counter

LSC | Low Background α-β Counting System

LSC | 환경방사능분석

Applications● The bionics field which uses form

the radioactive tracer

● The nuclear facility liquid effluence monitoring

● Radiation treatment field

● Environment radioactivity analysis

● Sr-90, CS-137 analysis in

the radioactive substance fallout

● Carbon regiment measurement

● Biosynthesis research (C-14, P-32, P-33)

SpecificationBeta backgrounds: typically 0.4 - 1.2 CPM for H-3

0.5 Bq/L H-3 (5 TU) in 500 min direct counting

Counter control

Stop NextCtime

P A C P S A

Window Spectrum

5

1 2 3 4 5 6 7 8 9 10

10

15

20

25

30

35

40

LIVE DISPLAY

Prol: 5Sample: 1Repeat: 1Cycle: 1 Unk measTime: 58.0CPM: 5296.24BETACOUNTS: 5064

Window: 1-1024Y = COUNTS * 1

Start

LSC | Low Background α-β Counting System

Low Background α-β Counting System 환경방사능분석 |

KNDT& i

Low Background α-β Counting System

18

Applications● α,β source and equipment

leakage inspection

● Environment radioactivity

measurement and watch

● Nuclear facility surface measurement and watch

SpecificationsDetector : 2.25” diameter gas-flow

sample detector

Detector window thick : 80 μg/㎠

To make it beneficial for you.

The most powerful company

for you.

| Inorganic analysis

| Organic analysis

| Material properties analysis

| Environmental radioactivity analysis

www.kndt.co.kr 19

Low Background α-β Counting System 환경방사능분석 |

KNDT&i Information

Creative company with infinite potential

레미안

케이엔디티앤아이 주식회사(본사)

케이엔디티앤아이 주식회사·화학사업본부·기술연구소

서울시 구로구 구로동 197-5번지 삼성 IT밸리 806, 807호

152-050 # 806 Samsung IT Valley 197-5, Guro-dong Guro-gu Seoul, Korea

Tel: 02-2028-2163~4 Fax: 02-2028-2165

www.kndt.co.kr

Creative company with infinite potential 케이엔디티앤아이 주식회사 / 화학사업본부 / 기술연구소

서울시 구로구 구로동 197-5 삼성IT밸리 806, 807호

# 806 Samsung IT Valley 197-5, Guro-dong Guro-gu Seoul, Korea

Tel: 02-2028-2163~4 Fax: 02-2028-2165

www.kndt.co.kr

| Inorganic analysis | Organic analysis | Material physical properties analysis | Environmental radioactivity analysis

KNDT&i