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    AN EXPERIMENTAL EVALUATION OF VISCOSITY GRADING

    FOR CONTROLLING FINGERING IN MISCIBLE

    DISPLACEMENTS

    H.K. SARMA B.B. MAINI

    this article begins on the next page FF

    ic -P 7,73 ENHANCED OIL RECOVERY An experimental evaluation of viscosity grading for controlling fingering in miscible displacements HEMANTA K. SARMA and BRIJ B. MAINI Petroleum Recovery Institute ABSTRACT Displacement of oil by miscibleflooding processes is adversely affected by the hydrodynamic instability at the flood front whenever the viscosity ratio is unfavourable. Instabilities cause viscousfingers to grow and make the displacement process in- efficient and uneconomical. Therefore, it is necessary to devel- op ways of reducing or eliminating the detrimental effects of viscous

    instabilities to make miscible flooding processes economically viable under adverse viscosity ratio conditions. Grading the viscosity of the displacing j7uids appears to be an effective technique for controlling viscous instabilities. This paper presents an experimental evaluation of the effi- cacy of graded-viscosity solvent banks for improving the per- formance ofsolventflooding under very adverse viscosity ratios. A scaled physical model with transparent top surface was devel- opedfor visual examination of viscousfingers during solvent floods. Base case displacement experim ents carried out to quantify the effects of viscosity ratio andflood velocity on the development of viscousfingers and the resulting displacement efficiency. The displa cement experiments were then repeated with graded-viscosity solvent slugs to determine the effective- ness of such viscosity grading. Tw o different methods of design- ing graded-viscosity banks (the Claridge and the Cos- kuner-Bentsen methods) were examined. Results show that the extent of viscousfingering present and the resulting displacement efficiency, in the base case displace- ments, varied significantly with viscratio andflood veloc- ity. The use of graded-viscosity banks always reduced, and often, totally eliminated the viscous fingering. In this study, the viscous target oil was used as an additive for increasing the solvent viscosity. Forf ield application of the graded-viscosity bank process, less expensive additives for increasing the viscosity of the solvent will be needed. Until such additives become available or the procedure can be improved upon, the use of graded-viscosity banks in miscible solventflood appears to be uneconomical Introduction Miscible flooding has received

    considerable attention in recent years because of its inherent potential to achieve a higher recov- ery efficiency. A 1989 survey by Thomas et al.(') suggests that miscible flooding was the most popular method with operators in the United States during 1980-1981. However, because of the high material and operational costs the process has become less attractive at the current uncertain oil prices. Paper reviewed and accepted for publication by the Editorial 36 Although the miscible displacement process is not consider- ed an obvious choice for heavy oils, it may have some poten- tthin heavy-oil reservoirs where thermal methods are not suitable because of excessive heat losses to the underlying and _ overlying strata. However, in the case of miscible floods, high viscosity ratios between the oil and solvent often result in vis- cous instabilities at the front, and lead to a lower recovery effi- ciency. Therefor e, it is important to minimize the extent and effects of viscous instabilities. Fingers in a miscible flood tend to generate a transition zone at the interface due to mass transfer. The transition zone, whose composition exhibits continu ous gradation

    viscosity due to blending, arrests finger ing of displacing fluid to an extent(3). However, in the field it is unlikely that such zone will dev elop at the initial stages of the solvent injection, and as a conse - quence, severe viscous fingering may occur. In such situations, a graded-viscosity bank ca n be used to minimize viscous finger- ing. Lake(l) suggests that the concept of graded viscos ity can become economic only when the mobility ratio is very hig h and/or the formation is very heterogeneous. Liter ature Review Literature on viscous instabili ties in immiscible and miscible dis-placements is quite extensive. Homsy(4) has presented a com- prehensive state-of-the-art review of the important papers on this subject. However , the literature on the use of graded-vis- cosity bank is limited partly because its use has remained con- fined primarily in polymer floods. So far there have been only a few field-scale pilot projects using graded-viscosity banks(i-1) . The first experimental study of the concept of graded- viscosity bank is credited to Weinaug and Ling(l) in 1959 who performed Hele-Shaw type experiments using a quarter of five- spot type model. Later,Slobod and Lestz('o) reported that graded-viscosity banks could be used to minimize viscous fingering, and suggested the use of a continuous blended zone rather than step-wise viscosity gradation to completely elimi- nate viscous fingering. Perrine (11,12) proposed a stability theory to optimize the sol- vent recovery of oil by defining the limiting conditions required for a stable miscible displacement and estimated the minimum size of the solvent slug required. Later, Kyle and Perrine(13) conducted an experimental study to validate Perrine's theory and concluded that the

    concentration-gradient criterion pro- posed in Perrine's theory was an order of magnitude higher than what was observed in experiments. Board of 'Fhe Iournal of Canadian Petroleum Technology. The Journal of Canadian Petroleum Technology

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    -1cP793 o/

    ENHANCED

    OIL

    RECOVERY

    An

    exp,erimental evaluation

    of

    viscosity

    grading

    for

    controHing fingering

    miscible displacements

    lUll

    HEMANTA K SARMA

    and BRIJ

    B MAINI

    Petroleum Recovery

    Institute

    BSTR CT

    Displacement

    o

    oil

    by

    miscible

    flooding

    processes is adversely

    afJe(,ted by the hydrodynamic instability at the

    flood from

    whenever the viscosity ratio ;s unfavourable. Instabilities cause

    ~ i s c o u s fingers to grow and make the displacement process in

    efficient

    and

    uneconomical. Therefore, it is necessary to devel

    op ways

    o f

    reducing or eliminating the detrimental effects

    of

    viSCD IS instabilities

    to make

    miscible

    flooding

    pro esses

    economically viable under adverse viscosifJ ratio conditions.

    Grading the

    ~ I i s c o s i t y

    o he displacing fluids appears fO be an

    effective technique jor controlling viscous instabilities.

    This paper presents an experimental evaluation

    o

    Ihe effi

    cacy o graded-viscosity solvent banks for improving the per

    ormance ojsolvent flooding under very adverse viscosity ratios.

    A scaled physical model with transparent top surface was devel

    oped Jor

    visual examination o viscous fingers during solvent

    loods. Base case displacement experiments were carried out to

    quantify the effects

    o j

    \ iscosity ratio and flood velocity on the

    development o viscous fingers

    and

    the resulting displacement

    efficiency. The displacement experiments were then repeated

    with graded-viscosity solvent slugs to determine the effective

    ness 0/ uch viscosity grading. Two different melhods

    o

    design

    ing graded-l- ;scosity banks (the Claridge

    and

    the Cos

    kuner-Bentsen methods) were examined.

    Results show that the extem

    o

    viscousjingering present and

    the resulting displacement efficiency, in the base case displace

    ments, varied significantly with \ iscosity ratio andf/ood veloc

    ily. The use

    o

    graded-viscosity banks always reduced. and

    often, totally eliminated the viscous fingering.

    In this study, the viscous target oil was used as an additive

    or

    increasing thesolvellt viscosity. For field application oj he

    graded-viscosity bank process, less expensive additives

    for

    increasing the viscostty o he solvent wilJ be needed. Until such

    additives become available or the procedure can be improved

    upon, the

    lise of

    graded-viscosity banks in miscible solvent

    flood

    appears to be uneconomical.

    Introduction

    Miscible flooding has received considerable atten tion in recem

    years because of its inherent pOlential to achieve a higher recov

    Although the miscible displacement process

    is

    not co

    ed an obvious choice for heavy oils, it may have some

    tial in thin heavy-oil reservoirs where thermal methods

    suitable because

    of

    excessive heat losses to the underly

    overlying strata. However, in the case

    of

    miscible nood

    viscosity ratios between the oil and soh em orten re .ul

    cous instabilities

    at

    the front, and lead to a lower recove

    ciency. Therefore, it is

    important

    to minimize the ext

    effects of viscous instabilities.

    Fingers in a miscible flood tend to generate a transiti

    at the interface due

    to

    mass transfer. The transition zone

    composition exhibits continuous

    gradation

    in viscosity

    blending, arrest'S" fingering

    of

    displacing fluid to an e

    However. in the field it is unlikely that such zone will

    at

    the initial stages

    of

    the solvent injection, and as a

    quence, severe viscous Fingering may occur. In such situ

    a graded-viscosity bank can be used to miOimize viscous

    ing. Lake(J) suggests that the concept

    of

    graded viscos

    become economic only when the mobility ratio i ;;

    Vc

    and/or the formation is very heterogeneous.

    Literature lReview

    Literature on viscous instabilities in immiscible and misc

    placements is quite extensive. HomsyH) has prescnted

    prehensive state-of-the-art review of the important pa

    this subject. However, the literature

    on

    the lise of grad

    cosity

    bank

    is

    limited

    panly

    because its use has remain

    fined primarily

    in

    polymer floods. So far there have be

    a fel,.\ field-scale pilot projects using graded-viscosity ban

    The first experimental study of the concept of

    viscosity

    bank

    is

    credited to Weinaug and Ling(9) in

    19

    performed Hele-Shaw type experiments using a quarter

    spot

    type model. Later, Slobod

    and Les[z(lO)

    reporte

    graded-viscosity banks could be used

    [

    minimize

    fingering, and suggested the use of a continuous blende

    rather than

    step-wise viscosity gradation to completely

    nate viscous fingering.

    Perrine(l),12) proposed a smbility theory [Q optimize

    vent recovery

    of

    oil by defining the limiting conditions r

    for a stable miscible displacement

    and

    estimated the mi

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    In 1963, Koval(l4) proposed the K-factor method for pre

    dicting the performance

    of

    unstable immiscible displacements

    in heterogeneous media by combining the effects

    of

    a

    number

    of

    factors, such as: viscosity ratio, channelling and longitudi

    nal dispersion_ The K-faclor

    is

    essentially the

    product

    of two

    other factors: the heterogeneity factor (H) and effective viscos

    ity ratio (E)-

    A heterogeneous system as defined by Koval is the one in

    whrch the recovery

    at

    one pore volume solvent injected in a

    matched viscosity flood is less

    than

    991lJo _According to Koval,

    the heterogeneity factor is a function

    of

    dispersion, channel

    ling and the length

    of

    the system_ Empirically. he observed that

    the shorter the length

    of the

    core, the higher is the heteroge

    neity factor_In a recent study , Menzie(l5) a bserved

    that

    the H

    factor was higher for rocks with higher dispersivity_

    When the transition or mixing zone develops at the inter

    face, the viscosity of the oil changes significantly, and in most

    cases, the viscosity decreases. Thus, in effect, the oil is displaced

    by a mixture

    of

    the solvent

    and

    oil with a viscosity intermediate

    between

    that of

    the pure solvent and

    pure

    oiL Koval's effective

    viscosity ratio takes this into account when calculating the vis

    cosity ratio between the displaced oil and the displacing oil

    solvent mixture_

    For

    systems with minimum effects

    of

    disper

    sion and channelling, the empirrcal relationship between E and

    V is given by:

    o

    -I-

    E (0_78

    + 0.22

    V )

    . . . . . ._. __

    ._ .. _.

    __

    ._.

    __

    ._._._._ .. _ . _._ . . . . _ . _

    ...

    (I)

    The

    solvent mixture compositions

    of 781170

    oil and 221lJo solvent

    were chosen arbitrarily as such compositions gave the best fit

    of

    experimental data_

    Using Koval's K-factor metho d repeatedly for each viscos

    ity zone, Claridge('6) proposed a method for designing graded

    viscosity banks to minimize viscous fingering in linear systems

    and suggested a criterion

    for

    the minimum size

    of

    a continuously

    graded bank:

    TABLE 1. Typical scaling parameters

    for

    Tellus320

    oil

    Paramelers

    Prolotype Model

    L,

    (m)

    150.0 0.50

    L,

    (m)

    60.0 0.20

    h

    (m) 3.0

    0.Q1

    ( ,I ,)

    1406.3 1406.3

    k ( m')

    3.0 159.0

    v (m/day)

    0.1

    3.6

    K, (m /s)

    1.63E6 1.96E7

    K,

    (m /s)

    5.14E-8

    6.17E9

    Objectives

    The objectives

    of

    this paper were to study

    how

    viscous instabil

    i[ies affected cumulative oil recoveries in miscible displacements

    of

    viscous oils, and to detennine the efficacy of viscosity graded

    slugs in suppressing the detrimental effects of viscous instabil

    ities_

    To meet these objectives, the following tasks were

    undertaken_

    1_

    Derive a set

    of

    scaling criteria and use these criteria to design

    a scaled physical model to carry out flow-visualization studies

    of

    the displacement process_

    2_ Conduct

    displacement experiments using three different

    methods: (a) pure solvent flood. (b) Claridge method and

    (c) Coskuner-Bentsen method_

    3_

    Compare

    and evaluate experimental findings from the three

    methods.

    Scaling Criteria

    In order to make this study more relevant to field situations,

    scaled laboratory experiments were designed with following

    scaling criteria. These criteria were derived

    on

    the basis

    of

    the

    dimensional and inspectional analyses_

    ~ ~ P = (1

    -

    IIMD-44)

    --.--------.,----.------------------.------------ (2)

    Geometric Similarity

    For a very large M, the size

    of

    the continuously graded

    bank

    is nearly equal [ 0 one pore volume_

    According to Claridge, if 0,

    I,

    2, ... were the successive slugs

    of

    the displacing fluid with descending viscosities away from

    the oil, the size

    of

    a panicular slug can be estimated by using

    the following equation:

    [Mo

    M

    o

    - I]

    s1ug

    = -'------ ------'''----_''----

    _________

    .

    ________

    . .

    ____ (3)

    [ Mn

    l\:l

    n

    _

    1

    ___

    M2, lvl

    l

    Mo] 2

    Coskuner and Bentsen(17) proposed a stability theory for

    miscible displacement processes. Using

    Chuoke's

    unpublished

    work reported by

    Gardner

    and Ypma(lB) to account for the

    boundary conditions at side walls

    of

    the porous medium, they

    demonstrated that this theory could be used to predict the initial

    length and the upper and lower bounds

    of

    the transition region

    between the solvent and oiL

    Upper bound:

    .4k [ ~ d . ~ g ]

    h

    2

    L2

    JlZ = _ . . . : : . k _ . : : d ~ c _ ~ d ~ c - - - -

    ---:-:---- :-:-___________

    . .

    (4)

    p rp

    7r1 KI l +

    Lower bound:

    .k ~ ~ _ d ~ g ]

    k de de

    .;.z

    hl L2

    ,

    .. _ . _ .... (5)

    h

    2

    + L2

    ,

    Although Coskuner and Bentsen validated their theory by using

    data from the literature, they did

    not

    report

    any

    experimental

    validation of their own_

    January 1993, Volume 32, No_ 1

    L,

    [ L ] Model

    ,

    = [ ~ ] ProLOlype

    ---.--. ,--.--------. . ----.----

    (6)

    ,

    Viscous Ratio

    [ ]

    Model =

    [ ~ ]

    Pr010L}'pe -----------------------.------

    (7)

    lis

    Ratio of Viscous to Gravity Forces

    Lx II 11

    [ k

    g

    h

    lip

    -------':........:...::_ _ ._._

    ..

    _

    .

    _ (8)

    ] [

    Lxvpo ]

    Model

    k

    g

    h o lt.p Prololype

    Longitudinal Dispersion Effects

    K,

    [ ]

    Model

    L,

    V

    K,

    [

    L

    V ] ProlOlypc ------------------------

    (9)

    Transverse Dispersion Effects

    [

    K, L,

    v Ll

    ] Model

    [

    K,

    L,

    v

    Ll

    ] ProtOlype ----------------------

    (10)

    For

    the sake of ilIus[ration, a set of typical scaling paramete rs

    for Tellus-320 oil are presented in Table

    1.

    37

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