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  • 1.

    2. 2.1

    2.1.1

    2.1.2

    2.2

    2.2.1

    2.2.2

    2.2.2.1

    2.2.2.2

    2.2.2.3

    2.2.2.4

    2.2.2.5

    2.2.2.6

    2.2.3

    2.3

    3. KZRCAD3.1

    3.1.1

    3.1.2

    3.2

    3.3

    3.3.1

    3.3.2

    3.3.3

    3.3.3.1

    3.3.3.2

    3.3.4

    3.3.5 X

    3.4 KZRCADKZR-Sinfur

    2

    333455667788101011

    1313131414151516161617191920

  • .

    CAD/CAMCAD

    CAD/CAM

    CAD/CAM

    2 3

    CAD/CAM

    CAD/CAM

    CAD/CAM

    KZRCAD

    .

    .

    ..

    Zr ZrO2

    2,700

    1

  • 1

    2000

    ..

    84%

    4 5

    .

    ..

    7.9%

    4% 1)

    Y2O3

    CaOMgO

    (cubic zirconia, CZ)

    Y2O33mol%100%Y-TZPTetragonal

    Zirconia Polycrystal

    ..

    Cubic

    Tetragonal

    Monoclinic

    23701170

    950

    Cubic

    Tetragonal

    Monoclinic

    2370 1170

    950

    CAD/CAM

    2009

    23,488

    14,530

    5,285

    2,489

    427

    320

    2009

    8,904

    2,660

    760

    103

    436

    1,003

    3,943

    3

    2 2

    2009

    1262010

  • ..

    ...

    6 7

    ...

    12%

    ...

    7

    4

    5 3) 6)

    6 3) 6)

    107(6)670-6842007

  • ...

    ...

    Watanabe1600Y2O3 4 mol800

    100200

    3007

    8 9

    200300

    Zr-O-Zr8Zr-O-Zr

    9)ChevalierY-TZP

    372520%10)

    Tompson37191213

    3.611

    81 mm

    9

    11

    201022-37

    10-6/K W/mK

    14.2

    18.9

    8.4

    6.8

    1010.5

    317

    429

    21.9

    32

    2.5

    100hours

    RT 100 200 300 400 500 600 700 800 900

    1600

    1500

    1450

    50hr

    ZrO2-3molY2O3

    100

    50

    00 200 400 600 800

    mol

    HHH

    H OO

    O

    Zr

    Zr

    O

    Zr O

    O

    H

    H

    Zr

    Zr

    Zr

    Watanabe M., Iio S., Fukuura I.Aging behavior of Y-TZP. Advanced in Ceramics, Vol. 12, Science and Technology of Zirconia II. Edited by N. Claussen and R. Rhle and A.H. Heuer, American Ceramic Society, 391-398, 1984.

    Sato T., Ohtaki S., Shimada M.Transformation of Yttria Partially Stabilized Zirconia by Low Temperature Annealing in Air, J. Mater. Sci., 20(4), 1466-1470, 1985.

    Sato T., Ohtaki S., Shimada M.Transformation of Yttria-Doped Tetragonal ZrO2 Polycrystals by Annealing in Water. J. Am. Ceram. Soc., 68(6), 356-359, 1985.

  • ...

    37

    0.5 mm/min

    10

    ..

    JIS T 652612ISO 6872DentistryCeramic

    materials13

    10 11

    800 MPa100g/cm2

    0.510-6 K-1

    .

    CAD/CAM

    CCD

    12

    CAD

    13

    20%

    CAM

    14

    10-

    11

    12

    0

    10

    20

    30

    40

    50

    60

    MPa

    Ti

    Ni-Cr

    Co-Cr

    Au

    Au-Ag-Pd

    ZrO2

    JIS T 6526:2012

    MPa

    g/cm2

    a b

    a b

    a

    b

    1 50

    100

    100

    300

    300

    500

    800

    100

    100

    2000

    100

    2000

    2000

    100

    2

    3

    4

    5

    6

    13CAD

    14

    JIS T 65262012

  • 13501600

    15

    12 13

    . KZRCAD

    CAD/CAM

    KZRCAD

    KZRCAD

    .

    ..

    9899 mm

    98.5 mm

    2013

    181416 mm1820 mm

    KZRCAD14 mm20 mm25 mm

    1862

    15

    16

    17ABC

    20 vol%

    A B C

    0

    5

    10

    15

    20

    25

    8 10 12 14 15 16 18 20 22 25 30

    mm

  • ..

    19

    .

    Y2O3

    14 15

    KZRCAD

    CIP

    ..

    .

    KZRCAD

    1.

    2.

    3.

    ..

    KZRCADCIP

    20

    21

    20

    20

    21

    1962

    24

    40

    36

    KZRCAD Twt%

    ZrO2HfO2Y2O3

    Y2O3

    Al2O3

    SiO2

    Fe2O3

    Na2O

    99.00

    4.955.35

    0.200.30

    0.020

    0.010

    0.040

  • ..

    KZRCAD 1000500/10001450300

    /1450

    KZRCAD

    ..

    ...

    JIS T 0304200914

    KZRCAD

    cm2 (MO5) 30 mL

    37

    2.5 mL1 mL1 mL

    151 g/mL

    500 L50 mLICP

    (NexION 300D[Perkin Elmer])

    1.6 kW

    1.20 L/min ()

    18.00 L/min ()

    1.09 L/min ()

    16 17

    89 ()

    115 ()

    2.5 mL3 mL25 %400 L

    1 mL15

    1 g/mL500 L50 mL

    1.6 kW

    1.20 L/min ()

    18.00 L/min ()

    1.09 L/min ()

    90 ()

    205 ()

    KZRCAD

    ...

    ISO10993-515V79

    V79 (23) ()

    V79

    (24)

    2423V79

    KZRCAD

    22

    0

    500

    1000

    1500

    0 2 4 6 8 10 12 14 16 18 20

    hr

    KZRCAD

    D

    A

    E

    CB

    F

  • 60 cm2 (MO5) 10 mL3724

    (100%) MO5100502512.56.25

    3.3%

    V795037%

    10%

    0.1%

    MO5

    100% ()

    KZRCAD101.5111.9%

    ()ISO10993-5

    (100%)

    70%

    KZRCAD

    KZRCAD

    18 19

    ..

    KZRCAD1 m

    .. X

    XKZRCAD

    26

    26

    25SEM10,000

    26X

    %

    3.13

    6.25

    12.5

    25

    50

    100

    /

    48.5

    53.5

    48.8

    49.5

    50.8

    51.0

    47.8

    %

    101.5

    111.9

    102.1

    103.6

    106.3

    106.7

    100.0

    X

    X

    CuK/40 kV/40 mA

    Ultima

    20~70deg

    4 deg/min

    0.01 deg

    2/

    1m

    20 30 40 50 60 70

    2/

    cps

    tt

    t t

    t

    tt

    t

    t

  • .KZRCADKZR-Sinfur

    KZR2014

    20

    ) 201012-20

    ) 201022-37

    )[] 20021504

    )2000108

    )JA45336-3441979

    )Zpex5657-612012

    )Watanabe M.Iio S.Fukuura I.Aging behavior of Y-TZP. Advanced in CeramicsVol.12, Science and Technology of Zirconia IIEdited by Claussen N.Rhle R.Heuer A.H.American Ceramic Society, 391-398, 1984.

    )Sato T.Ohtaki S.Shimada M.Transformation of Yttria-Doped Tetragonal ZrO2 Polycrystals by Annealing in Water. J. Am. Ceram. Soc., 68(6), 356-359, 1985.

    )101989157-174

    10Chevalier. J., Drouin. J. M., Cales. B.Low temperature ageing behavior of zirconia hip joint heads. Bioceramics, 10135-138, 1997

    11Tompson I.Rawlings R.D.Meohanical behaviour of zirconia and zirconia-toughened alumina in a simulated body environmentBiomaterials11505-5081990

    12JIS T 65262012

    13ISO 68722008Dentistry-Ceramic materials

    14JIS T 03042009

    15ISO 10993-52009

    27KZR-Sinfur

    3.5

    /29kg

    30cm

    20100

    10

  • R&D

    CAD/CAM

    CAD/CAM

    CAD/CAM

  • 2014221