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1.
2. 2.1
2.1.1
2.1.2
2.2
2.2.1
2.2.2
2.2.2.1
2.2.2.2
2.2.2.3
2.2.2.4
2.2.2.5
2.2.2.6
2.2.3
2.3
3. KZRCAD3.1
3.1.1
3.1.2
3.2
3.3
3.3.1
3.3.2
3.3.3
3.3.3.1
3.3.3.2
3.3.4
3.3.5 X
3.4 KZRCADKZR-Sinfur
2
333455667788101011
1313131414151516161617191920
.
CAD/CAMCAD
CAD/CAM
CAD/CAM
2 3
CAD/CAM
CAD/CAM
CAD/CAM
KZRCAD
.
.
..
Zr ZrO2
2,700
1
1
2000
..
84%
4 5
.
..
7.9%
4% 1)
Y2O3
CaOMgO
(cubic zirconia, CZ)
Y2O33mol%100%Y-TZPTetragonal
Zirconia Polycrystal
..
Cubic
Tetragonal
Monoclinic
23701170
950
Cubic
Tetragonal
Monoclinic
2370 1170
950
CAD/CAM
2009
23,488
14,530
5,285
2,489
427
320
2009
8,904
2,660
760
103
436
1,003
3,943
3
2 2
2009
1262010
..
...
6 7
...
12%
...
7
4
5 3) 6)
6 3) 6)
107(6)670-6842007
...
...
Watanabe1600Y2O3 4 mol800
100200
3007
8 9
200300
Zr-O-Zr8Zr-O-Zr
9)ChevalierY-TZP
372520%10)
Tompson37191213
3.611
81 mm
9
11
201022-37
10-6/K W/mK
14.2
18.9
8.4
6.8
1010.5
317
429
21.9
32
2.5
100hours
RT 100 200 300 400 500 600 700 800 900
1600
1500
1450
50hr
ZrO2-3molY2O3
100
50
00 200 400 600 800
mol
HHH
H OO
O
Zr
Zr
O
Zr O
O
H
H
Zr
Zr
Zr
Watanabe M., Iio S., Fukuura I.Aging behavior of Y-TZP. Advanced in Ceramics, Vol. 12, Science and Technology of Zirconia II. Edited by N. Claussen and R. Rhle and A.H. Heuer, American Ceramic Society, 391-398, 1984.
Sato T., Ohtaki S., Shimada M.Transformation of Yttria Partially Stabilized Zirconia by Low Temperature Annealing in Air, J. Mater. Sci., 20(4), 1466-1470, 1985.
Sato T., Ohtaki S., Shimada M.Transformation of Yttria-Doped Tetragonal ZrO2 Polycrystals by Annealing in Water. J. Am. Ceram. Soc., 68(6), 356-359, 1985.
...
37
0.5 mm/min
10
..
JIS T 652612ISO 6872DentistryCeramic
materials13
10 11
800 MPa100g/cm2
0.510-6 K-1
.
CAD/CAM
CCD
12
CAD
13
20%
CAM
14
10-
11
12
0
10
20
30
40
50
60
MPa
Ti
Ni-Cr
Co-Cr
Au
Au-Ag-Pd
ZrO2
JIS T 6526:2012
MPa
g/cm2
a b
a b
a
b
1 50
100
100
300
300
500
800
100
100
2000
100
2000
2000
100
2
3
4
5
6
13CAD
14
JIS T 65262012
13501600
15
12 13
. KZRCAD
CAD/CAM
KZRCAD
KZRCAD
.
..
9899 mm
98.5 mm
2013
181416 mm1820 mm
KZRCAD14 mm20 mm25 mm
1862
15
16
17ABC
20 vol%
A B C
0
5
10
15
20
25
8 10 12 14 15 16 18 20 22 25 30
mm
..
19
.
Y2O3
14 15
KZRCAD
CIP
..
.
KZRCAD
1.
2.
3.
..
KZRCADCIP
20
21
20
20
21
1962
24
40
36
KZRCAD Twt%
ZrO2HfO2Y2O3
Y2O3
Al2O3
SiO2
Fe2O3
Na2O
99.00
4.955.35
0.200.30
0.020
0.010
0.040
..
KZRCAD 1000500/10001450300
/1450
KZRCAD
..
...
JIS T 0304200914
KZRCAD
cm2 (MO5) 30 mL
37
2.5 mL1 mL1 mL
151 g/mL
500 L50 mLICP
(NexION 300D[Perkin Elmer])
1.6 kW
1.20 L/min ()
18.00 L/min ()
1.09 L/min ()
16 17
89 ()
115 ()
2.5 mL3 mL25 %400 L
1 mL15
1 g/mL500 L50 mL
1.6 kW
1.20 L/min ()
18.00 L/min ()
1.09 L/min ()
90 ()
205 ()
KZRCAD
...
ISO10993-515V79
V79 (23) ()
V79
(24)
2423V79
KZRCAD
22
0
500
1000
1500
0 2 4 6 8 10 12 14 16 18 20
hr
KZRCAD
D
A
E
CB
F
60 cm2 (MO5) 10 mL3724
(100%) MO5100502512.56.25
3.3%
V795037%
10%
0.1%
MO5
100% ()
KZRCAD101.5111.9%
()ISO10993-5
(100%)
70%
KZRCAD
KZRCAD
18 19
..
KZRCAD1 m
.. X
XKZRCAD
26
26
25SEM10,000
26X
%
3.13
6.25
12.5
25
50
100
/
48.5
53.5
48.8
49.5
50.8
51.0
47.8
%
101.5
111.9
102.1
103.6
106.3
106.7
100.0
X
X
CuK/40 kV/40 mA
Ultima
20~70deg
4 deg/min
0.01 deg
2/
1m
20 30 40 50 60 70
2/
cps
tt
t t
t
tt
t
t
.KZRCADKZR-Sinfur
KZR2014
20
) 201012-20
) 201022-37
)[] 20021504
)2000108
)JA45336-3441979
)Zpex5657-612012
)Watanabe M.Iio S.Fukuura I.Aging behavior of Y-TZP. Advanced in CeramicsVol.12, Science and Technology of Zirconia IIEdited by Claussen N.Rhle R.Heuer A.H.American Ceramic Society, 391-398, 1984.
)Sato T.Ohtaki S.Shimada M.Transformation of Yttria-Doped Tetragonal ZrO2 Polycrystals by Annealing in Water. J. Am. Ceram. Soc., 68(6), 356-359, 1985.
)101989157-174
10Chevalier. J., Drouin. J. M., Cales. B.Low temperature ageing behavior of zirconia hip joint heads. Bioceramics, 10135-138, 1997
11Tompson I.Rawlings R.D.Meohanical behaviour of zirconia and zirconia-toughened alumina in a simulated body environmentBiomaterials11505-5081990
12JIS T 65262012
13ISO 68722008Dentistry-Ceramic materials
14JIS T 03042009
15ISO 10993-52009
27KZR-Sinfur
3.5
/29kg
30cm
20100
10
R&D
CAD/CAM
CAD/CAM
CAD/CAM
2014221