PQ_IV Protocol - RGD Bigger Lot Size V8

7/23/2019 PQ_IV Protocol - RGD Bigger Lot Size V8

http://slidepdf.com/reader/full/pqiv-protocol-rgd-bigger-lot-size-v8 1/13

(TS#U015/14 RG Drumming Bigger Lot Size) Document No.: !G""$%4

Re&i'ion: 5

FPG OLEOCHEMICALS SDN BHD

PERFORMANCE QUALIFICATION & INITIAL VERIFICATION PROTOCOL

!roect Nme: RG Drumming Bigger Lot Size

** Num+er: ,014/0-,

Dte: $ rc ,015

. B23*T3

To ro&i6e 6ocumente6 e&i6ence tt RG Drumming Bigger Lot Size roect 7i88 +e +8e to meet

+e8o7 o+ecti&e'.

1) 88 te Re9ine6 G8cerin ro6uce t RG Drumming ; 1?;B) 7i88 +e +8e to trn'9er to 1?*) ten to RG 6rumming 7itout n @u8it n6'9et inci6ent.

%) To &8i6te te 9re@uenc o9 9i8ter +g cnge t <B 9rom % mont once to mont8.

4) To &8i6te te 9re@uenc o9 9i8ter +g cnge n6 o8i' 9i8ter cnge t RG Drumming to 15

6' o9 oertion 'ince ro6uct 8re6 go troug ) To &8i6te te cnge o9 Lot. No in te T3S ''tem.

?) To generte 6t to 'uort ro6uct omogeneit in 1?B;*) rior 'en6 it to RG Drumming or <B.

t RG Drumming te Re9ine6 G8cerin 7i88 +e 9i88e6 in to 6rum or B* n6 'ie6 out to cu'tomer

&i continer.

t 1?;B to 1?*. rom n8'i' Tn= S1>1?* te Re9ine6 G8cerin 7i88 +e um to RG

Drumming 9or c=ing. (Re9er to Section 2 ttcment 1 n6 , 9or roce'' 98o7)

t RG !8nt

Te Re9ine6 G8cerin 7i88 +e 'en6 into n8'i' Tn= S"1>1?;B. en te n8'i' Tn= i' 9u88 it

7i88 +e i'o8te6 n6 'm8e 7i88 +e t=en 9or n8'i'. 9ter te n8'i' i' com8ete6 n6 meet te

re8e'e criteri te Re9ine6 G8cerin 7i88 +e 'en6 to <B.

!ge 1 o9 1%

FPG18eoc/emic)8'




Re&i'ion: 5

t 1? ;B. Te Re9ine6 G8cerin coming 9rom n8'i' Tn= 7i88 continue unti8 te 1?* t

RG !8nt. Te 8o6ing to 'otiner 8'o 7i88 +e 9rom te ointe6 <B tn=. During te trn'9er

te Re9ine6 G8cerin 7i88 '' troug 9i8ter +g t <B. Te cnge 9re@uenc 9or te 9i8ter +g

cnge 8'o 7i88 +e &8i6te6 6uring &8i6tion. Te 9re@uenc o9 cnging te 9i8ter +g i' mont8.

t RG !8nt

n8'i' Tn= S1>1?* 7i88 recei&e te Re9ine6 G8cerin coming 9rom 1?* 7i88 'er&e ' 'urge tn= rior 'en6ing te Re9ine6 G8cerin to RG Drumming.

t RG Drumming

1) RG Drumming 7i88 recei&e te Re9ine6 G8cerin 9rom n8'i' Tn= S1>1?*. Te Re9ine6

G8cerin 7i88 '' troug 9i8ter +g n6 o8i' 9i8ter +e9ore +eing 9i88e6 into 6rum or B*.

Te como'ite 'm8e (;L) 7i88 +e t=en 9rom te 6rum or B* 9or n8'i'. 9ter 9i88ing te

6rum or B* 7i88 +e 'tore t te 7reou'e 7iting 9or re8e'e n6 'iment. 9ter te como'ite'm8e i' n8'i' n6 re8e'e it cn +e 'ie6 out to cu'tomer.

,) Te 9re@uenc o9 cnging te 9i8ter +g n6 o8i' 9i8ter 7i88 +e &8i6te6 6uring &8i6tion. Te

9re@uenc o9 cnging te 9i8ter 7i88 +e e&er 15 6' o9 ro6uction.

%) Te ne7 8ot rinte6 on te 6rum n6 B* 7i88 8'o +e &8i6te6 6uring ti' &8i6tion.

3Cm8e *urrent o9 Lot No. !roo'e Lot. No. t RG Drumming

*urrent: G 0$*T,014 " 6te o9 RG

n8'i' Tn= i' i'o8te6

LT 4,-,0%--"G* 7ere

4"Eer (,014),-,"running 6 in er te n8'i' tn=

i' i'o8te6 ($ ct)

0%--"!G co6e (9iC no)

G*"n8'i' Tn= S"1>1?*

!roo'e: G 012N,015 " 6te o9 <B

Tn=/n8'i' Tn= i' i'o8te6 (1 2n ,015)

<B Tn= n8'i' Tn=

Lot No 50010%--",0",

5" Eer

001"running 6 in

er 9or <B tn=

i'o8tion 6te (1 2n

,015)

0%--"!G co6e (9iC no)

,0"G8cerin <B Tn=

#,0,"'econ6 running 6te

9or RGD c=ing

'e@uence (% 2n ,015

7ere te 9ir't 6te i' on, 2n ,015)

Lot No 50010%--"G"1

5" Eer

001"running 6 in

er 9or n8'i' tn=

i'o8tion 6te (1 2n

,015)

0%--"!G co6e (9iC no)

G" n8'i' Tn=

S1>1?1"RG Drumming

!c=ing (Ti' 7i88 +e

9iC num+er)

!ge , o9 1%




Re&i'ion: 5

FRe9er to !ro6uct 6enti9iction n6 Trce+i8it " !G""00? re& 15 (6r9t) in Section 2

ttcment 1 9or 6eti8.

*. !RDU*T D3S*R!TN ; !RDU*T D3SGN

Ti' &8i6tion 7i88 co&er te Re9ine6 G8cerin ro6uce t RG !8nt ten 'torge t RG n8'i'

Tn= S1>1?;B 1?* n6 RG Drumming.

D. !R*3SS D3S*R!TN ; B*<GRUND

1. De'crition o9 te !roce''

88 te Re9ine6 G8cerin ro6uce t te RG !8nt 7i88 +e trn'9er 9rom n8'i' Tn= S1>1?;B

to <B Tn= ,0;,1. 9ter com8ete 'en6ing one n8'i' tn= te ertion 7i88 +8o7 te 8ine

to <B tn= u'ing nitrogen. Ti' roce'' 7i88 continue unti8 te 1?*. 9ter

com8ete6 trn'9erring 9rom 1?* 1?*. rom n8'i' Tn= S1>1?* te Re9ine6 G8cerin 7i88 +e um to RGDrumming 9or c=ing. 9ter com8ete6 te 7o8e 8ot te RG Drumming ertion 7i88 +8o7 +c= te ro6uct to n8'i' Tn= S1>1?/B.

,. 8o7 Digrm

Re9er to te Section 2 ttcment , n6 %.

%. !re&iou' 3Ceriment8 or= ; Re8te6 Document'

niti8 !8nt 'trt"u reort U00,/05

HH RG Bigger Lot Size U015/14

!G St+i8it , er reort R;D reort + Rut ger' ,01,

4. !roce'' *ontro8 Strteg

Loction S! Tit8e S! No.

Re9er to Section 2

n8tic8 1) Re9ine6 G8cerin Re8e'e

!roce6ure

,) !ro6uct 6enti9iction n6

Trce+i8it

1) !G""0?1 re&4

(6r9t) ttcment 4

,) !G""00? re&14

(6r9t) ttcment 1

RG !8nt 1) !roce'' *ontro8 Strteg "

Re9ine6 G8cerin

,) S'tem 1>00 G8cerinn8'i' Tn=

%) RG !urging Log'eet

1) !G""04, re&1,

ttcment 5

,) !G""?0> re&5(6r9t) ttcment >

%) ttcment ?

 1 'em,ttcment $

%) ttcment 10

!ge % o9 1%




Re&i'ion: 5

Loction S! Tit8e S! No.

Re9er to Section 2

4) Senggr i8ter RG

5) !G* G8o+8 !ro6uct

ngement !roce''

T+8e

4) <B"HS"1"11

ttcment 11

5) G*S#$$$,0,,$.00$

ttcment 1,

RG Drumming 1) !roce'' *ontro8 Strteg Re9ine6 G8cerin

,) Re9ine6 G8cerin

reou'e ngement

%) S'tem 1?00 Re9ine6

G8cerin Drumming

ertion !roce6ure

4) S'tem 1?00 i8ter

Re8cement !roce6ure

i8ter Bg n6 !o8i'

i8ter

5) Lot co6ing cec=8i't ; ,D

&eri9iction>) T3S *ec=8i't

?) Siment *ec=8i't

1) !G""04> re&10ttcment 1%

,) !G""$1> re&1,

ttcment 14

%) !G""->0 re& 1,

(6r9t) ttcment 15

4) !G""$0> re& -

(6r9t) ttcment 1>

5) ttcment 1?

>) ttcment 1-

?) ttcment 1$

Su8 *in 1) 'otiner 8eCitn=

Siment !roce6ure

,) T3S cec=8i't 9or 8ot no.

cnge

1) !G""$04 re&>

(6r9t) ttcment ,0

,) ttcment ,1

5. <e 3@uiment Li't ; *ontro8 S'tem'

Loction De'crition 3@uiment Li't

RG !8nt

n8'i' Tn=S"1>1? ;B

n8'i' Tn= Le&e8

n8'i' Tn= TemertureRe9ine6 G8cerin Trn'9er !um

L!41% ; L!415

T!4,$ ; T!4%0!"1>1?

1? *

n8'i' Tn= Le&e8

n8'i' Tn= Temerture

Re9ine6 G8cerin Drumming

!um

L!4,4

T!4,?

!"1>1-

RG Drumming Temerture ; 8o7 meter

G8cerin i8ter

G8cerin !o8i' i8ter

H05,

1?0,

1>01B

>. <e Tecnic8 eto6 Li't

Loction De'crition

n8tic8 88 n8'i' meto6 +'e6 on current * n6 !S

!ge 4 o9 1%




Re&i'ion: 5

?. Strting teri8' ; Su8ier' N/

-. *ritic8 Su+"S'tem'

Loction De'critionRG !8nt Nitrogen 'u8 ot 7ter 'u8

1? ; B +e9ore 'en6ing it to 1?* +e9ore trn'9er to RG Drumming.

N/

RG Drumming Store t RG Drumming reou'e 9ter

9i88ing.

Siment ' er S

FRe9er to Re9ine6 G8cerin Re8e'e !roce6ure !G""0?1 re& 4 (6r9t) in Section 2 ttcment 4

9or 6eti8.

3. *L3NNG ; SNTITN N/

. SUR*3S RTN

<e Source o9 rition rition or Rnge !H Ao7 66re''e6 in !H or

8o7 rte J J

Temerture Be8o7 5,K* J J

!ge 5 o9 1%




Re&i'ion: 5

G. PERFORMANCE QUALIFICATION PLAN:

1. NUB3R n6 DURTN o9 RUNS

1) Te !H 7i88 co&er 6urtion 'trting 9rom te 9ir't n8'i' Tn= /B 7ic 'en6 to <BTn= ,0/,1. 9ter te <B Tn= i' i'o8te6 it 7i88 +e 'en6 +c= to n8'i' Tn= * ten to

RG Drumming. Te !H 7i88 en6 7en te RG Drumming 9ini' 6rumming 88 te ro6uct

9rom one 1? /B)

Sm8ing oint

nce

'o8te6.

%C500 m8

(, 9or n8'i'

; 1 9or retin)

u88 n8'i' o9

Suero8 <

G8cerin

US!/**

.

' er 8imit in

* G*S

$5-$?$%5.00$

C500 m8

(% 9or n8'i'; % 9or retin)

u88 n8'i' o9

Suero8 <

G8cerinUS!/** n6

*in oo6

.

' er 8imit in

* G*S/!S

$5-$?$%5.00$n6

$>5>>0%>.00>

*omo'ite

Sm8e t RG

Drumming

nce er 8ot

>J500 m8

(% 9or n8'i'

n6 % 9or

retin)

u88 n8'i' o9

Suero8 <

G8cerin

US!/** n6

er 'eci9ic

cu'tomer re@ue't

.

' er 8imit in

* G*S/!S

$5-$?$%5.00$

n6 re8te6 *

n6 !S

00>51%4

,)Seci9ic

Gr&it G*S#

.1) USL: 0.%m8 o9

0.5N NA

USL : 1m8 o9

0.5N NA

To mi668e n6

Bottom 'm8e

!ge > o9 1%




Re&i'ion: 5

(cn +e ro8e

o&er to

'e)

Bottom

%J500m8>401,$?0

7itin rnge o9

0.044

See Be8o7 Note

,)USL: 1.,>1%

,5K*/,5K*

F9 te To i668e n6 Bottom 'm8e 9i8e6 9or te 9ir't time (1 our 9ter i'o8tion) t=e noter

'et o9 'm8e unti8 te 88 te 'm8e i' 7itin rnge o9 % 'igm 7ic i' 0.044

FSt+i8it 'm8e 7i88 +e co88ecte6 to +e ut t S* 9or te on"going 't+i8it 'tu6. Sm8e 9rom

6rum 9i88er B* 9i88er n6 <B tn= 7i88 +e co88ecte6. Te mount o9 'm8e n6 6urtion 7i88 +e

+'e6 on te on"going 't+i8it rotoco8. Re9er to ttcment ,, in Section 2.

F* Reorting 7i88 +e +'e6 on te 1?;B) 7i88 +e +8e to trn'9er to 1?*) ten to RG 6rumming 7itout n @u8it n6

'9et inci6ent.

%) No in6i&i6u8 'm8e o9 como'ite ( n6 L) 9i8e6 ernce te't.4) RG Drumming 8ot co6ing rinter +8e to rint te ne7 8ot no.

5) T3S S'tem +8e 'cn te ne7 8ot. no.>) 100M reconci8ition 9or te 8ot.

?) To i668e n6 Bottom Sm8e '' te 8imit ' er 'm8ing 8n +o&e.

*ritic8 !roce'' !rmeter Re@uirement'

1) Temerture o9 te <B Tn= i' =ee +e8o7 5,K* t 88 time. Trget i' 51K*. Te mCimum

6' o9 eting u in te <B Tn= i' 10 6' 'trting 9rom on8ine to emt out te <B tn=.

(B'e6 on 5 6' to 9i88 u te <B tn= n6 5 6' to emt out te <B tn=).

,) 9 tere i' no i'otiner 8o6ing or trn'9er +c= to !G 9or more tn t7o 6 te temerture o9

te ro6uct in te 1?* i' 5,K*.

4. R3S!NSBLT3S

T'= Re'on'i+i8it

!H !rotoco8 !8nt !D

!H !rotoco8 Brie9ing 88

n9ormtion to <B Su8 *in

Tn= !8nning Su8 *in

!ge ? o9 1%




Re&i'ion: 5

3Cecution o9 !H RG ertion ; RG Drumming

nterim Reort !8nt !D

!H Reort !8nt !D

5. !RDU*T DS!STN ; R3L3S3 *RT3R

Loction Re8e'e *riteri Remr='

RG !8nt

n8'i' Tn=

S1>1? ; B

eet 88 te criteri er

'm8ing 8n in Section ,

+o&e

<B

Tn= ,0 ; ,1

eet 88 te criteri er

'm8ing 8n in Section ,

+o&e

RG Drumming

Drum ; B*

' er 'm8ing 8n in

Section , +o&e

1) nterim reort to re8e'e te 9ir't %

8ot tt +een ro6uce i9 nee6e6 9or

'iment. To +e ro&e6 + Site

H n6 R;D.

FRe9er to Re9ine6 G8cerin Re8e'e !roce6ure !G""0?1 re& 4 (6r9t) in Section 2 ttcment 4

9or 6eti8.

H. INITIAL VERIFICATION PLAN:

1. NUB3R o9 RUNS

Te 6urtion 7i88 +e 9or one mont. Te 7i88 co&er te +e8o7 item.

1) Te 7i88 co&er 6urtion 'trting 9rom te n8'i' Tn= /B 7ic 'en6 to <B Tn=

,0/,1. 9ter te <B Tn= i' 9u88 it 7i88 +e 'en6 +c= to n8'i' Tn= * ten to RG

Drumming.

,) Te 9re@uenc o9 9i8ter cnge 9or <B i' mont8.%) Te 9re@uenc o9 9i8ter cnge 9or RG Drumming 7i88 +e e&er 15 6' o9 oertion.

4) T3S S'tem +8e to 'cn te ne7 8ot no.5) Te 8ot co6ing rinter +8e to rint te ne7 8ot no.

,. S!LNG n6 NLESS !LN

Sampling L!a"in F#$%$n!'Sampl$

Si($Anal')i) *+ Limi")

n8'i' Tn=

(S"1>1? /B)

Sm8ing oint

nce 'o8te6.

%C500 m8

(, 9or

n8'i' ;

1 9or

retin)

u88 n8'i' o9

Suero8 <

G8cerin

US!/**

.

' er 8imit in

* G*S

$5-$?$%5.00$

!ge - o9 1%




Re&i'ion: 5

C500 m8

(% 9or

n8'i' ;

% 9or

retin)

u88 n8'i' o9

Suero8 <

G8cerin

US!/** n6

*in oo6

.

' er 8imit in

* G*S/!S

$5-$?$%5.00$

n6

$>5>>0%>.00>

*omo'ite Sm8e t

RG Drummingnce er 8ot

>J500 m8

(% 9or

n8'i'

n6 % 9or

retin)

u88 n8'i' o9

Suero8 <

G8cerin

US!/** n6

er 'eci9ic

cu'tomer re@ue't

.

' er 8imit in

* G*S/!S

$5-$?$%5.00$n6 re8te6 *

n6 !S

F* Reorting 7i88 +e +'e6 on te 1?;B) 7i88 +e +8e to trn'9er to 1?*) ten to RG 6rumming 7itout n @u8it n6

'9et inci6ent.

%) No in6i&i6u8 'm8e o9 como'ite ( n6 L) 9i8e6 ernce te't.

4) RG Drumming 8ot co6ing rinter +8e to rint te ne7 8ot no.

5) T3S S'tem +8e 'cn te ne7 8ot. no.

>) 100M reconci8ition 9or 88 te 8ot.

!roce'' *ontro8 Strteg com8ince 'ucce'' criteri:

88 te 6ocument ttcment 7i88 +e u6te i9 nee6e6 7en te &8i6tion i' com8ete6.

4. R3S!NSBLT3S

T'= Re'on'i+i8it

!H !rotoco8 !8nt !D

!H !rotoco8 Brie9ing 88

n9ormtion to <B Su8 *in

Tn= !8nning Su8 *in

3Cecution o9 !H RG ertion ; RG Drumming

nterim Reort !8nt !D

!H Reort !8nt !D

!ge $ o9 1%




Re&i'ion: 5

. SGNTUR3S

Su+mitte6 +: ong Sei ei 9or te !D Tem

B 'igning +e8o7 7e in6icte tt 7e &e re&ie7e6 te rotoco8 n6 &e 9oun6 it to +e 'u99icient to

6emon'trte te c+i8it o9 te roce'' gin't rorite ccetnce criteri.

Mohd Faudzi AbdulRahman

(C)Operation Manager

Date Lee Chee San(C)Site QA

Manager

Date

Fairuz Sulong

(C)Engineering Manager

Date Saurabh Mathur

(C)PC R!D

Date

"an Shah

#ania$hra%ah

"an&u$in

(C) S'O Leader

Date

elaha brahim

(A)Site *alidation

O+ner

Date Anh Lenuhoang

(A)PC QA

Date

Peng &e

(A)PC PS

Date Ra$oul Madadi

(A)Euroa$ia R!D

Date

!ge 10 o9 1%




Re&i'ion: 5

and MPD Manager

2. TT*A3NT

No. De'crition ttcment

1 !ro6uct 6enti9iction n6 Trce+i8it

!G""00? re& 15 (6r9t)FP, ,--. RE*

/01R bigger lot1re2

, !roce'' 8o7 6igrm

Pro5e$$ Flo+Diagram46l$6

% !roce'' 8o7 Digrm

RG Trn'9er 9rom n8'i' Tn= S1>1?;B to1?* ten to RG Drumming

Pro5e$$ Flo+ Chart,R Produ5t 7ran$8er1

4 Re9ine6 G8cerin Re8e'e !roce6ure

!G""0?1 re& 4 (6r9t)FP,,-./ Re2

31R bigger lot4do56M#PR -9 -:46l$6

5 !roce'' *ontro8 Strteg " Re9ine6 G8cerin

!G""04, re& 1,FP,,-39 Re2

/9;/<4pd8

> S'tem 1>00 n8'i' Tn=

!G""?0> re& 5 (6r9t)FP,,.-= Re2

0,l>5erine Anal>$i$

? RG !urging Log'eet

R PurgingLog$heet46l$6

- engntr Semu8 !ro6u= <e6 !e8nggn

B"L3"HS"!<"04 re&%P@,-3 , MenghantarSemula Produ? @epad

$ Lorn !ro6u= Trn'9er =e !G

 1@O#,OP=,/(Sem49)46l$

10 <B !urging Log'eet

@O#,OP=,/(Sem49)46l$

!ge 11 o9 1%




Re&i'ion: 5


11 Senggrn i8ter RG

<B"HS""11@O#,QMS,",// ,

Senggaraan Filter R

1, !G* G8o+8 !ro6uct ngement !roce''

T+8eG*S#$$$,0,,$.00$ PROD,PROS19-9

91--;/<4pd8

1% !roce'' *ontro8 Strteg " Re9ine6 G8cerin

!G""04> re& 10FP,,-3= Re2

/-;/<4pd8

14 Re9ine6 G8cerin reou'e ngement

!G""$1> re&1,FP,,/= Re2

/9;/<4pd8

15 S'tem 1?00 Re9ine6 G8cerin Drumming

ertion !roce6ure!G""->0 re& 1, (6r9t) FP,,B=- Re2 /9 ,

R #igger lot $ize4do

1> S'tem 1?00 i8ter Re8cement !roce6ure

i8ter Bg n6 !o8i' i8ter

!G""$0> re& - (6r9t) FP, ,-= Re2 dra8t4do56

1? B!R RG Drumming

Lot *o6ing *ec=8i't n6 ,D *o6e eri9iction

*ec=8i't re&1 M#PR R DrummingProdu5tion Che5?li$t

1- T3S *ec=8i't

RG Drumming 7ESA R Drumming

Che5?li$t4do56

1$ u88 Siment *ec=8i't

R Drum$ ShipmentFull1Che5?li$t1Re2=4

,0 'otiner 8eCitn= Siment !roce6ure

!G""$04 re& > (6r9t)FP,,-3re2= ,

R bigger Lot $ize4do

,1 T3S *ec=8i't

Su8 *in 7ESA Suppl> Chain

Che5?li$t4do56

,, n"going St+i8it !rotoco8

FP R Stabilit> ,Proto5ol 2/494do5

!ge 1, o9 1%




Re&i'ion: 5


,% Signi9icnt *nge

SC , R #igger LotSize4do5

,4 6e ''e''ment

dea A$$e$$ment,RD / #at5h Strateg

!ge 1% o9 1%

Documents

PQ_IV Protocol - RGD Bigger Lot Size V8