Quantitative Analysis Summary Report

Accuracy

100.52

97.66

105.49

96.41

Exp Conc

25.0000

50.0000

125.0000

250.0000

Final Conc

25.1307

48.8288

131.8593

241.0263

Response

1039

2288

6704

12600Calibration

RT

1.174

1.178

1.176

1.179Benzo Cal06.d

Compound

7-amino flunitrazepam

7-amino flunitrazepam

7-amino flunitrazepam

7-amino flunitrazepam

86.35

7-amino flunitrazepamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Sample Type

Calibration

Calibration

Calibration

Accuracy

99.40

102.20

97.41

101.52

99.77

163.2034

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

189.0000

Final Conc

24.8509

51.0992

121.7594

253.8018

498.8381

2400

5192

12941

28338

60068

17646

0.982

0.982

0.982

0.984

0.983

0.982

Calibration

Calibration

Calibration

Calibration

Calibration

QC

7-amino clonazepam

7-amino clonazepam

7-amino clonazepam

7-amino clonazepam

7-amino clonazepam

7-amino clonazepam

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Benzos Mix Unit Pos APCI Segs.m

Benzos Mix Unit Pos APCI Segs.m

Benzos Mix Unit Pos APCI Segs.m

Quantitation Results7-amino clonazepamData File Compound Sample Type RT Response

Acq Method File

Benzos Mix Unit Pos APCI Segs.m

Benzos Mix Unit Pos APCI Segs.m

Benzos Mix Unit Pos APCI Segs.m

Benzos Mix Unit Pos APCI Segs.m

Benzos Mix Unit Pos APCI Segs.m

QC1

Sample Type

Calibration

Calibration

Calibration

Calibration

Calibration

Blank

Sample

QC

-1

-1

Level

L1

L2

L3

L4

L5

-1

-1

-1

-1

-1

-1

Benzo QC

Position

P1-F3

P1-F4

P1-F5

P1-F6

P1-F7

P1-F2

P1-F9

P1-F8

Benzo Cal09.d

Benzo Cal08.d

Sample Name

25 Std

50 Std

125 Std

250 Std

500 Std

Blank

123456

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal02.d

Last Calib Update 12/23/2008 8:58 PM Batch State Processed

Sequence TableData File Volume

Analysis Time 12/23/2008 8:58 PM Analyst Name mtischler

Report Time 2/26/2010 10:24 PM Reporter Name mtischler

Batch Info2008-12-23T20:58:47.6220336-08:00 2010-02-26T22:24:39.3655776-08:00 2008-12-23T20:58:47.2414864-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ESTD_Complete_B_04_00.xlsx Page 1 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Summary Report

Data File Compound Sample Type RT Response Final Conc

Accuracy

101.18

97.39

97.30

108.41

97.50

4.3147

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

Final Conc

25.2959

48.6968

121.6290

271.0307

487.5074

2.958

Response

2521

5325

14188

32945

61553

25

RT

3.518

3.513

3.509

3.517

3.518

Sample Type

Calibration

Calibration

Calibration

Calibration

Calibration

Blank

Benzo Cal07.d

Benzo Cal02.d

Compound

alpha-OH alprazolam

alpha-OH alprazolam

alpha-OH alprazolam

alpha-OH alprazolam

alpha-OH alprazolam

alpha-OH alprazolam

alpha-OH alprazolamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

0.0000

Accuracy

100.65

98.08

100.86

101.20

99.38496.8960

5.1514

4.5336

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

33023

69168

143521

204

41

Final Conc

25.1618

49.0376

126.0736

252.9898

QC

RT

3.286

3.288

3.286

3.292

3.295

3.311

3.272

flunitrazepam

flunitrazepam

flunitrazepam

Sample Type

Calibration

Calibration

Calibration

Calibration

Calibration

Blank

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal08.d

Compound

flunitrazepam

flunitrazepam

flunitrazepam

flunitrazepam

92.43

flunitrazepamData File

Benzo Cal03.d

Benzo Cal04.d

Response

5526

11932

Accuracy

98.88

104.49

95.51

102.34

99.77

3.3301

95.1997

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

103.0000

Final Conc

24.7196

52.2448

119.3880

255.8607

498.8468

3.301

3.195

Response

4519

10363

25046

56764

119448

48

19686

RT

3.194

3.192

3.188

3.196

3.200

clonazepam

Sample Type

Calibration

Calibration

Calibration

Calibration

Calibration

Blank

QC

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal08.d

Compound

clonazepam

clonazepam

clonazepam

clonazepam

clonazepam

clonazepam

clonazepamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

Accuracy

101.02

97.21

101.27

101.65

99.15

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

1687

Final Conc

25.2561

48.6047

126.5878

254.1215

495.7699

11.9202

Response

4242

8725

23794

48755

97125

Sample

RT

2.465

2.467

2.465

2.470

2.471

2.463

Sample Type

Calibration

Calibration

Calibration

Calibration

CalibrationBenzo Cal07.d

Benzo Cal09.d

Compound

zopiclone

zopiclone

zopiclone

zopiclone

zopiclone

zopiclone

zopicloneData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

100.0000

100.95

96.15

Exp Conc Accuracy

500.0000

4797

504.7471

96.1471

27273Calibration

QC

1.180

1.180

Benzo Cal07.d

Benzo Cal08.d

7-amino flunitrazepam

7-amino flunitrazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 2 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Summary Report

Exp Conc AccuracyData File Compound Sample Type RT Response Final Conc

98.23102.0000

Accuracy

101.18

97.17

100.16

103.22

98.72

2.0854

139.3762

100.1899

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

Final Conc

25.2959

48.5826

125.1943

258.0590

493.5876

4.056

Response

3517

7077

19133

41287

84446

16

21422

15140

Sample

QC

RT

4.056

4.058

4.054

4.064

4.065

3.953

4.058

alprazolam

alprazolam

alprazolam

Sample Type

Calibration

Calibration

Calibration

Calibration

Calibration

Blank

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal09.d

Benzo Cal08.d

Compound

alprazolam

alprazolam

alprazolam

alprazolam

alprazolam

alprazolamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

Accuracy

100.57

98.73

99.75

101.74

99.32

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

34

Final Conc

25.1414

49.3650

124.6842

254.3550

496.6123

0.7403

Response

3691

7397

19398

41757

89279

Blank

RT

4.035

4.031

4.018

4.025

4.024

4.012

Sample Type

Calibration

Calibration

Calibration

Calibration

CalibrationBenzo Cal07.d

Benzo Cal02.d

Compound

flurazepam

flurazepam

flurazepam

flurazepam

flurazepam

flurazepam

flurazepamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

105.0000

Accuracy

102.46

95.33

100.90

103.78

98.42

99.58

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

43

20974

Final Conc

25.6155

47.6670

126.1275

259.4508

492.0771

0.0000

104.5606

4.175

4.177

3.749

4.171

Response

5393

9590

25498

56020

119797

oxazepam

oxazepam

Sample Type

Calibration

Calibration

Calibration

Calibration

Calibration

Sample

QC

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal09.d

Benzo Cal08.d

Compound

oxazepam

oxazepam

oxazepam

oxazepam

oxazepam

96.02

oxazepamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

RT

4.169

4.170

4.165

Accuracy

98.56

105.63

95.95

100.38

100.50

25.0000

50.0000

125.0000

250.0000

500.0000

104.00004947

Final Conc

24.6404

52.8173

119.9394

250.9428

502.5176

99.8621

3.898

3.906

3.910

3.901

Response

1100

2560

5947

12184

22776

triazolam

Sample Type

Calibration

Calibration

Calibration

Calibration

Calibration

QC

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Compound

triazolam

triazolam

triazolam

triazolam

triazolam

triazolamData File

Benzo Cal03.d

Benzo Cal04.d

RT

3.902

3.905

Exp Conc

4.55373.507 53alpha-OH alprazolam SampleBenzo Cal09.d

QuantReport_ESTD_Complete_B_04_00.xlsx Page 3 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Summary Report

98.89

250.0000

500.0000

0.0000

Accuracy

102.15

95.36

102.28

102.06

16

Final Conc

25.5379

47.6801

127.8539

255.1505

494.4441

0.0000

0.0000

0.0000

5.355

5.319

Response

2372

4330

11594

23692

48302

14

20

Blank

Sample

QC

RT

5.391

5.404

5.392

5.400

5.399

5.409

chlordiazepoxide

chlordiazepoxide

chlordiazepoxide

chlordiazepoxide

Sample Type

Calibration

Calibration

Calibration

Calibration

Calibration

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal09.d

Benzo Cal08.d

Compound

chlordiazepoxide

chlordiazepoxide

chlordiazepoxide

chlordiazepoxide

96.88

chlordiazepoxideData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Exp Conc

25.0000

50.0000

125.0000

Accuracy

99.16

102.63

97.78

100.61

100.08

25.0000

50.0000

125.0000

250.0000

500.0000

107.000015199

Final Conc

24.7912

51.3168

122.2259

251.5143

500.3779

103.6595

4.650

4.662

4.660

4.655

Response

3570

7433

17999

38157

80203

temazepam

Sample Type

Calibration

Calibration

Calibration

Calibration

Calibration

QC

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Compound

temazepam

temazepam

temazepam

temazepam

temazepam

94.86

temazepamData File

Benzo Cal03.d

Benzo Cal04.d

RT

4.653

4.658

Exp Conc

Accuracy

99.65

101.38

97.75

101.85

99.58

0.9575

95.8101

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

101.0000

Final Conc

24.9125

50.6919

122.1880

254.6351

497.9057

4.614

4.541

Response

2062

4287

10592

22790

46946

17

8243

RT

4.545

4.540

4.534

4.545

4.548

desalkylflurazepam

Sample Type

Calibration

Calibration

Calibration

Calibration

Calibration

Blank

QC

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal08.d

Compound

desalkylflurazepam

desalkylflurazepam

desalkylflurazepam

desalkylflurazepam

desalkylflurazepam

desalkylflurazepam

desalkylflurazepamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

56.0000

Accuracy

100.64

98.60

98.75

103.61

98.78

95.90

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

14

8260

Final Conc

25.1594

49.2988

123.4390

259.0184

493.9033

2.9769

53.7015

4.111

4.114

4.225

4.115

Response

3595

7536

19938

43776

88618

lorazepam

lorazepam

Sample Type

Calibration

Calibration

Calibration

Calibration

Calibration

Blank

QC

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal08.d

Compound

lorazepam

lorazepam

lorazepam

lorazepam

lorazepam

lorazepamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

RT

4.106

4.110

4.106

QuantReport_ESTD_Complete_B_04_00.xlsx Page 4 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Summary Report

0.0000

Accuracy

100.61

98.45

100.44

101.12

99.47497.3567

1.8848

1.4099

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

8651

18256

38828

39

8

Final Conc

25.1532

49.2238

125.5455

252.8084

QC

RT

6.438

6.449

6.437

6.447

6.443

6.529

6.863

diazepam

diazepam

diazepam

Sample Type

Calibration

Calibration

Calibration

Calibration

Calibration

Blank

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal08.d

Compound

diazepam

diazepam

diazepam

diazepam

100.34

diazepamData File

Benzo Cal03.d

Benzo Cal04.d

Response

1605

3252

Accuracy

100.76

97.91

101.63

100.15

99.71

1.3858

54.1860

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

54.0000

Final Conc

25.1893

48.9558

127.0355

250.3807

498.5487

6.531

6.325

Response

2199

4407

11852

24202

51236

13

4897

RT

6.334

6.324

6.327

6.315

6.319

midazolam

Sample Type

Calibration

Calibration

Calibration

Calibration

Calibration

Blank

QC

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal08.d

Compound

midazolam

midazolam

midazolam

midazolam

midazolam

midazolam

midazolamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

0.0000

Accuracy

100.18

99.32

100.82

99.71

100.00

25.0000

50.0000

125.0000

250.0000

500.0000

10

Final Conc

25.0442

49.6591

126.0278

249.2801

500.0161

5.6429

5.6634

3202

7264

19918

40513

83063

7

QC

RT

5.816

5.831

5.814

5.833

5.827

5.239

5.892

Calibration

Calibration

Calibration

Calibration

Calibration

Blank

Benzo Cal08.d

Compound

nordiazepam

nordiazepam

nordiazepam

nordiazepam

nordiazepam

nordiazepam

nordiazepam

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal02.d

nordiazepamData File Sample Type Response Exp Conc

QuantReport_ESTD_Complete_B_04_00.xlsx Page 5 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Calibration Report

41.5670

45.7672

53.6296

50.4010

54.5461

47.97264797

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

100.0000

Response

1039

2288

6704

12600

27273

QC

Level

L1

L2

L3

L4

L5

QC1

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

93.3630

Target Compound 7-amino flunitrazepam

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Enabled

RF

RF

95.9836

103.8304

103.5310

113.3522

120.1350

17646

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

189.0000

Response

2400

5192

12941

28338

60068

QC1

Enabled

Level

L1

L2

L3

L4

L5

Benzo Cal08.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

QC

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Last Calib Update 12/23/2008 8:58 PM Batch State Processed

Calibration InfoTarget Compound 7-amino clonazepam

Analysis Time 12/23/2008 8:58 PM Analyst Name mtischler

Report Time 2/26/2010 10:24 PM Reporter Name mtischler

Batch Info2008-12-23T20:58:47.6220336-08:00 2010-02-26T22:24:39.3655776-08:00 2008-12-23T20:58:47.2414864-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ESTD_Complete_B_04_00.xlsx Page 6 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Calibration Report

191.1305

RF

180.7456

207.2518

200.3698

227.0552

238.8966

19686

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

103.0000

Response

4519

10363

25046

56764

119448

QC1

Enabled

Level

L1

L2

L3

L4

L5

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

QC

Target Compound clonazepam

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

RF

169.6761

174.5039

190.3556

195.0196

194.2509

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

Response

4242

8725

23794

48755

97125

Enabled

Level

L1

L2

L3

L4

L5

Benzo Cal06.d

Benzo Cal07.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

Target Compound zopiclone

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

QuantReport_ESTD_Complete_B_04_00.xlsx Page 7 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Calibration Report

RF

100.8527

106.4921

113.5063

131.7807

123.1056

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

Response

2521

5325

14188

32945

61553

L4

L5

Enabled

Benzo Cal06.d

Benzo Cal07.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

Target Compound alpha-OH alprazolam

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

221.0404

238.6467

264.1821

276.6725

287.0412

INF41

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

0.0000

Response

5526

11932

33023

69168

143521

QC

Level

L1

L2

L3

L4

L5

QC1

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

Target Compound flunitrazepam

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Enabled

RF

QuantReport_ESTD_Complete_B_04_00.xlsx Page 8 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Calibration Report

215.7070

191.7950

203.9834

224.0786

239.5933

199.747720974

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

105.0000

Response

5393

9590

25498

56020

119797

QC

Level

L1

L2

L3

L4

L5

QC1

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

47.5720

Target Compound oxazepam

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Enabled

RF

RF

43.9965

51.2044

47.5754

48.7342

45.5522

4947

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

104.0000

Response

1100

2560

5947

12184

22776

QC1

Enabled

Level

L1

L2

L3

L4

L5

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

QC

Target Compound triazolam

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

QuantReport_ESTD_Complete_B_04_00.xlsx Page 9 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Calibration Report

148.4349

RF

140.6704

141.5411

153.0635

165.1493

168.8918

15140

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

102.0000

Response

3517

7077

19133

41287

84446

QC1

Enabled

Level

L1

L2

L3

L4

L5

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

QC

Target Compound alprazolam

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

RF

147.6474

147.9411

155.1873

167.0275

178.5588

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

Response

3691

7397

19398

41757

89279

Enabled

Level

L1

L2

L3

L4

L5

Benzo Cal06.d

Benzo Cal07.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

Target Compound flurazepam

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

QuantReport_ESTD_Complete_B_04_00.xlsx Page 10 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Calibration Report

81.6184

RF

82.4857

85.7494

84.7394

91.1604

93.8915

8243

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

101.0000

Response

2062

4287

10592

22790

46946

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

QC

Target Compound desalkylflurazepam

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

143.7812

150.7213

159.5080

175.1057

177.2351

147.50108260

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

56.0000

Response

3595

7536

19938

43776

88618

QC

Level

L1

L2

L3

L4

L5

QC1

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

Target Compound lorazepam

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Enabled

RF

QuantReport_ESTD_Complete_B_04_00.xlsx Page 11 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Calibration Report

INF

RF

94.8629

86.5922

92.7539

94.7662

96.6036

16

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

0.0000

Response

2372

4330

11594

23692

48302

QC1

Enabled

Level

L1

L2

L3

L4

L5

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

QC

Target Compound chlordiazepoxide

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

142.7909

148.6645

143.9950

152.6281

160.4055

142.049415199

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

107.0000

Response

3570

7433

17999

38157

80203

QC

Level

L1

L2

L3

L4

L5

QC1

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

Target Compound temazepam

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Enabled

RF

QuantReport_ESTD_Complete_B_04_00.xlsx Page 12 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Calibration Report

90.6852

RF

87.9468

88.1469

94.8166

96.8080

102.4730

4897

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

54.0000

Response

2199

4407

11852

24202

51236

QC1

Enabled

Level

L1

L2

L3

L4

L5

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

QC

Target Compound midazolam

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

128.0815

145.2706

159.3451

162.0516

166.1253

INF10

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

0.0000

Response

3202

7264

19918

40513

83063

QC

Level

L1

L2

L3

L4

L5

QC1

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

Target Compound nordiazepam

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Enabled

RF

QuantReport_ESTD_Complete_B_04_00.xlsx Page 13 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Calibration Report

64.2167

65.0392

69.2075

73.0244

77.6564

INF8

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

0.0000

Response

1605

3252

8651

18256

38828

QC

Level

L1

L2

L3

L4

L5

QC1

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Cal Type

Calibration

Calibration

Calibration

Calibration

Calibration

Target Compound diazepam

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Enabled

RF

QuantReport_ESTD_Complete_B_04_00.xlsx Page 14 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

24.9125

24.7912

25.5379

25.0442

25.1893

25.1532

25.2959

24.6404

25.6155

25.1414

25.2959

25.1594

Final Conc

24.8509

25.1307

25.2561

24.7196

25.1618

2062

3570

2372

3202

2199

1605

2521

1100

5393

3691

3517

3595

5.391

5.816

6.334

6.438

Response

2400

1039

4242

4519

5526

4.169

4.035

4.056

4.106

4.545

4.653

midazolam

diazepam

RT

0.982

1.174

2.465

3.194

3.286

3.518

3.902

alprazolam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

clonazepam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

Sample Chromatogram

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

Position P1-F3 Inj Vol -1.00

Comment Sample Info

Sample Type Calibration Dilution 1

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 3/8/2007 10:50

Last Calib Update 12/23/2008 8:58 PM Batch State Processed

Analysis Info

Data File Benzo Cal03.d Sample Name 25 Std

Analysis Time 12/23/2008 8:58 PM Analyst Name mtischler

Report Time 2/26/2010 10:24 PM Reporter Name mtischler

Batch Info2008-12-23T20:58:47.6220336-08:00 2010-02-26T22:24:39.3655776-08:00 2008-12-23T20:58:47.2414864-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ESTD_Complete_B_04_00.xlsx Page 15 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

Compound Graphics

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

flunitrazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 16 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 17 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

desalkylflurazepam

temazepam

alprazolam

lorazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 18 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

chlordiazepoxide

nordiazepam

midazolam

diazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 19 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

QuantReport_ESTD_Complete_B_04_00.xlsx Page 20 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

50.6919

51.3168

47.6801

49.6591

48.9558

49.2238

48.6968

52.8173

47.6670

49.3650

48.5826

49.2988

Final Conc

51.0992

48.8288

48.6047

52.2448

49.0376

4287

7433

4330

7264

4407

3252

5325

2560

9590

7397

7077

7536

5.404

5.831

6.324

6.449

Response

5192

2288

8725

10363

11932

4.170

4.031

4.058

4.110

4.540

4.658

midazolam

diazepam

RT

0.982

1.178

2.467

3.192

3.288

3.513

3.905

alprazolam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

clonazepam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

Sample Chromatogram

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

Position P1-F4 Inj Vol -1.00

Comment Sample Info

Sample Type Calibration Dilution 1

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 3/8/2007 11:00

Last Calib Update 12/23/2008 8:58 PM Batch State Processed

Analysis Info

Data File Benzo Cal04.d Sample Name 50 Std

Analysis Time 12/23/2008 8:58 PM Analyst Name mtischler

Report Time 2/26/2010 10:24 PM Reporter Name mtischler

Batch Info2008-12-23T20:58:47.6220336-08:00 2010-02-26T22:24:39.3655776-08:00 2008-12-23T20:58:47.2414864-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ESTD_Complete_B_04_00.xlsx Page 21 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

Compound Graphics

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

flunitrazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 22 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 23 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

desalkylflurazepam

temazepam

alprazolam

lorazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 24 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

chlordiazepoxide

nordiazepam

midazolam

diazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 25 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

QuantReport_ESTD_Complete_B_04_00.xlsx Page 26 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

122.1880

122.2259

127.8539

126.0278

127.0355

125.5455

121.6290

119.9394

126.1275

124.6842

125.1943

123.4390

Final Conc

121.7594

131.8593

126.5878

119.3880

126.0736

10592

17999

11594

19918

11852

8651

14188

5947

25498

19398

19133

19938

5.392

5.814

6.327

6.437

Response

12941

6704

23794

25046

33023

4.165

4.018

4.054

4.106

4.534

4.650

midazolam

diazepam

RT

0.982

1.176

2.465

3.188

3.286

3.509

3.898

alprazolam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

clonazepam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

Sample Chromatogram

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

Position P1-F5 Inj Vol -1.00

Comment Sample Info

Sample Type Calibration Dilution 1

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 3/8/2007 11:11

Last Calib Update 12/23/2008 8:58 PM Batch State Processed

Analysis Info

Data File Benzo Cal05.d Sample Name 125 Std

Analysis Time 12/23/2008 8:58 PM Analyst Name mtischler

Report Time 2/26/2010 10:24 PM Reporter Name mtischler

Batch Info2008-12-23T20:58:47.6220336-08:00 2010-02-26T22:24:39.3655776-08:00 2008-12-23T20:58:47.2414864-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ESTD_Complete_B_04_00.xlsx Page 27 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

Compound Graphics

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

flunitrazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 28 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 29 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

desalkylflurazepam

temazepam

alprazolam

lorazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 30 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

chlordiazepoxide

nordiazepam

midazolam

diazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 31 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

QuantReport_ESTD_Complete_B_04_00.xlsx Page 32 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

254.6351

251.5143

255.1505

249.2801

250.3807

252.8084

271.0307

250.9428

259.4508

254.3550

258.0590

259.0184

Final Conc

253.8018

241.0263

254.1215

255.8607

252.9898

22790

38157

23692

40513

24202

18256

32945

12184

56020

41757

41287

43776

5.400

5.833

6.315

6.447

Response

28338

12600

48755

56764

69168

4.175

4.025

4.064

4.111

4.545

4.662

midazolam

diazepam

RT

0.984

1.179

2.470

3.196

3.292

3.517

3.906

alprazolam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

clonazepam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

Sample Chromatogram

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

Position P1-F6 Inj Vol -1.00

Comment Sample Info

Sample Type Calibration Dilution 1

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 3/8/2007 11:21

Last Calib Update 12/23/2008 8:58 PM Batch State Processed

Analysis Info

Data File Benzo Cal06.d Sample Name 250 Std

Analysis Time 12/23/2008 8:58 PM Analyst Name mtischler

Report Time 2/26/2010 10:24 PM Reporter Name mtischler

Batch Info2008-12-23T20:58:47.6220336-08:00 2010-02-26T22:24:39.3655776-08:00 2008-12-23T20:58:47.2414864-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ESTD_Complete_B_04_00.xlsx Page 33 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

Compound Graphics

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

flunitrazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 34 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 35 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

desalkylflurazepam

temazepam

alprazolam

lorazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 36 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

chlordiazepoxide

nordiazepam

midazolam

diazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 37 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

QuantReport_ESTD_Complete_B_04_00.xlsx Page 38 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

497.9057

500.3779

494.4441

500.0161

498.5487

497.3567

487.5074

502.5176

492.0771

496.6123

493.5876

493.9033

Final Conc

498.8381

504.7471

495.7699

498.8468

496.8960

46946

80203

48302

83063

51236

38828

61553

22776

119797

89279

84446

88618

5.399

5.827

6.319

6.443

Response

60068

27273

97125

119448

143521

4.177

4.024

4.065

4.114

4.548

4.660

midazolam

diazepam

RT

0.983

1.180

2.471

3.200

3.295

3.518

3.910

alprazolam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

clonazepam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

Sample Chromatogram

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

Position P1-F7 Inj Vol -1.00

Comment Sample Info

Sample Type Calibration Dilution 1

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 3/8/2007 11:31

Last Calib Update 12/23/2008 8:58 PM Batch State Processed

Analysis Info

Data File Benzo Cal07.d Sample Name 500 Std

Analysis Time 12/23/2008 8:58 PM Analyst Name mtischler

Report Time 2/26/2010 10:24 PM Reporter Name mtischler

Batch Info2008-12-23T20:58:47.6220336-08:00 2010-02-26T22:24:39.3655776-08:00 2008-12-23T20:58:47.2414864-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ESTD_Complete_B_04_00.xlsx Page 39 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

Compound Graphics

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

flunitrazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 40 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 41 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

desalkylflurazepam

temazepam

alprazolam

lorazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 42 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

chlordiazepoxide

nordiazepam

midazolam

diazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 43 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

QuantReport_ESTD_Complete_B_04_00.xlsx Page 44 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

2.9769

0.9575

0.0000

5.6429

1.3858

1.8848

Final Conc

3.3301

5.1514

4.3147

0.7403

2.0854

14

17

14

7

13

39

5.409

5.239

6.531

6.529

Response

48

204

25

34

16

midazolam

diazepam

RT

3.301

3.311

2.958

4.012

3.953

4.225

4.614

flurazepam

alprazolam

lorazepam

desalkylflurazepam

chlordiazepoxide

nordiazepam

Sample Chromatogram

Quantitation Results

Compound

clonazepam

flunitrazepam

alpha-OH alprazolam

Position P1-F2 Inj Vol -1.00

Comment Sample Info

Sample Type Blank Dilution 1

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 3/8/2007 10:40

Last Calib Update 12/23/2008 8:58 PM Batch State Processed

Analysis Info

Data File Benzo Cal02.d Sample Name Blank

Analysis Time 12/23/2008 8:58 PM Analyst Name mtischler

Report Time 2/26/2010 10:24 PM Reporter Name mtischler

Batch Info2008-12-23T20:58:47.6220336-08:00 2010-02-26T22:24:39.3655776-08:00 2008-12-23T20:58:47.2414864-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ESTD_Complete_B_04_00.xlsx Page 45 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

Compound Graphics

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

flunitrazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 46 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 47 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

desalkylflurazepam

temazepam

alprazolam

lorazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 48 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

chlordiazepoxide

nordiazepam

midazolam

diazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 49 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

QuantReport_ESTD_Complete_B_04_00.xlsx Page 50 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Final Conc

11.9202

4.5537

0.0000

139.3762

0.0000

Response

1687

53

43

21422

20

alprazolam

chlordiazepoxide

RT

2.463

3.507

3.749

4.058

5.355

Sample Chromatogram

Quantitation Results

Compound

zopiclone

alpha-OH alprazolam

oxazepam

Position P1-F9 Inj Vol -1.00

Comment Sample Info

Sample Type Sample Dilution 1

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 3/8/2007 12:01

Last Calib Update 12/23/2008 8:58 PM Batch State Processed

Analysis Info

Data File Benzo Cal09.d Sample Name 123456

Analysis Time 12/23/2008 8:58 PM Analyst Name mtischler

Report Time 2/26/2010 10:24 PM Reporter Name mtischler

Batch Info2008-12-23T20:58:47.6220336-08:00 2010-02-26T22:24:39.3655776-08:00 2008-12-23T20:58:47.2414864-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ESTD_Complete_B_04_00.xlsx Page 51 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

Compound Graphics

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

flunitrazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 52 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 53 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

desalkylflurazepam

temazepam

alprazolam

lorazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 54 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

chlordiazepoxide

nordiazepam

midazolam

diazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 55 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

QuantReport_ESTD_Complete_B_04_00.xlsx Page 56 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml54.1860

1.4099

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml100.1899

53.7015

95.8101

103.6595

0.0000

5.663410

4897

8

Final Conc

163.2034

96.1471

95.1997

4.5336

99.8621

104.560620974

15140

8260

8243

15199

165.319

5.892

6.325

6.863

Response

17646

4797

19686

41

49473.901

4.171

4.056

4.115

4.541

4.655temazepam

chlordiazepoxide

nordiazepam

midazolam

diazepam

RT

0.982

1.180

3.195

3.272flunitrazepam

triazolam

oxazepam

alprazolam

lorazepam

desalkylflurazepam

Sample Chromatogram

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

clonazepam

Position P1-F8 Inj Vol -1.00

Comment Sample Info

Sample Type QC Dilution 1

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 3/8/2007 11:51

Last Calib Update 12/23/2008 8:58 PM Batch State Processed

Analysis Info

Data File Benzo Cal08.d Sample Name Benzo QC

Analysis Time 12/23/2008 8:58 PM Analyst Name mtischler

Report Time 2/26/2010 10:24 PM Reporter Name mtischler

Batch Info2008-12-23T20:58:47.6220336-08:00 2010-02-26T22:24:39.3655776-08:00 2008-12-23T20:58:47.2414864-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ESTD_Complete_B_04_00.xlsx Page 57 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

flunitrazepam

Compound Graphics

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 58 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 59 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

lorazepam

desalkylflurazepam

temazepam

alprazolam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 60 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

diazepam

chlordiazepoxide

nordiazepam

midazolam

QuantReport_ESTD_Complete_B_04_00.xlsx Page 61 of 62 Printed at: 10:25 PM on: 2/26/2010

Quantitative Analysis Sample Report

QuantReport_ESTD_Complete_B_04_00.xlsx Page 62 of 62 Printed at: 10:25 PM on: 2/26/2010