REPORT NUMBER : TURA120090308 · R E S U L T S Page 2 of 6 REPORT : TURA120090308 02 August, 2012 Code Test Method Result Requirements Intertek Test Hizmetleri A.S . Merkez Mahallesi

TEST REPORT Page 1 of 6

Füsun Karaoğlu Neslihan Sözer Coordinator Chemical Laboratory Manager

Intertek Test Hizmetleri A.S .

Merkez Mahallesi Sanayi Cad. No: 23 Altında ğ Plaza Yenibosna 34197 - ISTANBUL / TURKEY Phone : +90.212. 496 46 46 Fax : +90.212. 452 80 55

e-mail : [email protected] www.intertek-labtest-tur.com

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REPORT NUMBER : TURA120090308

APPLICANT NAME Keskin Color Kartpostalcılık A. Ş.

Bağlar Mah. Çeşmealtı Sk.No:23 Istanbul FAX NO : 0212 550 12 66

ADDRESS Attention : Muhiddin Keskin ([email protected])

SAMPLE DESCRIPTION : 16.5*22.5 cm Funky Designed 100 Page Notebook

BUYER : TÜKİD

DATE IN : 26 July, 2012 (13:59)

DATE OUT : 02 August, 2012

ARTICLE NO : 418011-99

PHOTO OF PRODUCT TESTED :

Part No Tested Part 1 BEIGE COVER WITH PRINT 2 YELLOW STRIPED PAGE 3 METAL WIRE

R E S U L T S Page 2 of 6 REPORT : TURA120090308 02 August, 2012

Code Test Method Result Requirements


Merkez Mahallesi Sanayi Cad. No. 23 Altında ğ Plaza Yenibosna 34197 - ISTANBUL / TURKEY Phone : +90.212. 496 46 46 Fax : +90.212. 452 80 55


RESULTS :

Analysis Parameter

Reference Analysis Method

PASS FAIL Norm Limit Standard for Norm Limit

Tested Part

Azo Dyes 64 LFBG B 82.02.2 P - 30 ppm 2004/21/EC Part 1-2

Toxic Element Analysis

BS EN 71-3:1995 P -

Sb: 60 ppm As: 25 ppm Ba: 1000 ppm Cd: 75 ppm Cr: 60 ppm Pb: 90 ppm Hg: 60 ppm Se: 500 ppm

EN 71-3 Part 1-3

Phthalate EN 14372 by GC MS P -

DBP/DEHP/BBP : 1000 ppm DINP/DNOP/ DIDP :1000 ppm

(27893) Notification On Market Supervision And Controls Regarding Hazardous Chemical Contents Of Some End-User Products

Part 1-2

P = MEETS BUYER' S REQUIREMENT / F = DOES NOT MEET BUYER' S REQUIREMENT / NR = NO REQUIREMENT / SC=STILL CONTINUES / X=NOT PERFORMED The test results relate only to the items tested. The report shall not be reproduced except in full, without the written approval of the laboratory. The reported uncertainity is based on a standard uncertainity multiplied by a coverage factor k=2, providing a level of confidence of approximately 95%. The uncertainity evaluation has been carried out in accordance with ISO/IEC 17025 and UKAS accreditation requirements. Unless otherwise is specified, all Pass or Fail results are given without uncertainity considered. When uncertainity is taken into account, the result may be borderline. Borderline results need to be re-tested to determine their disposition up to customer’s decision. Opinions and interpretations expressed herein are outside the scope of UKAS accreditation. Tests marked (*) in this test report are not included in the UKAS accreditation schedule for this laboratory.






Azo Dyestuff 64 LFGB 82.02.2:2004 Determination of Certain aromatic Amines derived from azo colorants followed by GC- MS Analysis

Part 1&2 Composite sample of Beige cover with red print,yellow striped page PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN

THE OFFICIAL COMPILATION OF TEST METHODS TEXTILE ACCORDING TO § 64 LFGB 82.02-2, LEATHER ACCORDİNG TO § § 64 LFGB 82.02-3, PES ACCORDING TO § 64 LFGB 82.02-4, EXTRACTED BY CITRATE BUFFERED SOLUTION pH 6 AT 70 °C AND DETECTED BY GC/MS AND CONTROLLED BY HPLC/DAD AND THIN LAYER CHROMATOGRAPHIC ANALYSIS.

FORBIDDEN AMINE CAS NO 4-AMINOBIPHENYL 92-67-1 BENZIDINE 92-87-5 CHLORO-O-4-CHLOR-O-TOLUIDINE 95-69-2 2-NAPHTHYLAMINE 91-59-8 *O-AMINOAZOTOLUENE 97-56-3 *2-AMINO-4-NITROTOLUENE 99-55-8 P-CHLOROANILINE 106-47-8 2,4-DIAMINOANISOLE 615-05-4 4,4’-DIAMINOBIPHENYLMETHANE 101-77-9 3,3’-DICHLOROBENZIDINE 91-94-1 3,3’-DIMETHOXYBENZIDINE 119-90-4 3,3’-DIMETHYLBENZIDINE 119-93-7 3,3’-DİMETHYL-4,4’ DIAMINOBIPHENYLMETHANE 838-88-0 P-CRESIDINE 120-71-8 4,4’-METHYLENE-BIS-(2 CHLOROANILINE) 101-14-4 4,4’-OXYDIANILINE 101-80-4 4,4’-THIODIANILINE 139-65-1 O-TOLUIDINE 95-53-4 2,4-TOLUYLENDIAMINE 95-80-7 2,4,5-TRIMETHYLANILINE 137-17-7 O-ANISIDINE 90-04-0 **P-AMINOAZOBENZENE 60-09-3

NOTE:* The amines o-amino-azotoluene and 2-amino-4-nitrotoluene are detected by its splitted product o-toluidine and 2,4- toluylenediamine. **Azo colorants that are able to form 4-aminoazobenzene, generate under the condition of this method aniline and 1,4- phenylendiamine . The presence of these colorants can not be reliably ascertained without additional information, e.g. chemical structure of the colorant used.

Remark < = Less Than ppm(Part per million)= mg/ kg Detection Limit = 5 ppm Total Uncertainity = ±10%






Toxic Elements Analysis BS EN 71-3:1995 : Acid extraction method was used and toxic elements content were determined by Inductively Coupled Plasma-ICP_OES.

RESULT IN ppm PASS/FAIL Requirement (ppm)

Part 1 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 2 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 3 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 ppm (Part per million) =mg / kg < =Less Than (Total uncertainty=Results quoted have been corrected for uncertainty. -)






TOTAL PHTHALATE CONTENT EN 14372 : 2004 Method By Gas Chromotographic-Mass Spectrometric (GC-MS) Analysis : Part 1 RESULT (%, w/w) DIBUTYL PHTHALATE (DBP) Not Detected DIETHYL HEXYL PHTHALATE (DEHP) Not Detected BENZYL BUTYL PHTHALATE (BBP) Not Detected

SUM OF THREE PHTHALATES Not Detected

LIMIT (MAX.) 1000 ppm (0.1% (w/w)) RESULT (%, w/w) DI-ISO-NONYL PHTHALATE (DINP) Not Detected DI-N-OCTYL PHTHALATE (DNOP) Not Detected DI-ISO-DECYL PHTHALATE (DIDP) Not Detected

SUM OF THREE PHTHALATES Not Detected LIMIT (MAX.) 1000 ppm (0.1% (w/w))

REMARK =The Above Limit Was Quoted According To The EEC Directive 2005/84/EC On 14 December 2005. ppm (part per million) =mg / kg Detection Limit =10 ppm < =Less Than * =EXCEEDED LIMIT (Total Uncertainty=±5 %)











## END OF TEST REPORT ##






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SAMPLE DESCRIPTION : A4 Free checked Notebook 60 Page

BUYER : TÜKİD

DATE IN : 26 July, 2012 (13:59)




Part No Tested Part 1 YELLOW PP COVER 2 WHITE/BLACK CHECKED PAPER 3 TRANSPARENT PLASTIC WIRE






RESULTS :

Analysis Parameter



Tested Part



BS EN 71-3:1995 P -


EN 71-3 Part 1-3




Part 1-3








Part 1&2&3 1)Composite sample of Yellow PP cover,white/black checked paper PASS 30 ppm 2)Transparent plastic wire PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN

















































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SAMPLE DESCRIPTION : Şirinler designed drawing book

BUYER : TÜKİD

DATE IN : 26 July, 2012 (13:59)




Part No Tested Part 1 MULTICOLOR DESIGNED COVER 2 WHITE PAPER 3 WHITE METAL WIRE






RESULTS :

Analysis Parameter



Tested Part



BS EN 71-3:1995 P -


EN 71-3 Part 1-3




Part 1-2








Part 1&2 1)Multicolor designed cover PASS 30 ppm 2)White paper PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN



































PP

Aşkın GÜNERİ





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SAMPLE DESCRIPTION : Pepee Designed Weekly Course Schedule

BUYER : TÜKİD

DATE IN : 26 July, 2012 (13:59)

DATE OUT : 30 July, 2012



Part No Tested Part 1 MULTICOLOR DESIGNED PAPER

R E S U L T S Page 2 of 5 REPORT : TURA120090312 30 July, 2012





RESULTS :

Analysis Parameter



Tested Part

Azo Dyes 64 LFBG B 82.02.2 P - 30 ppm 2004/21/EC Part 1


BS EN 71-3:1995 P -


EN 71-3 Part 1




Part 1








Part 1 Multicolor designed paper PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN












Part 1 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 ppm (Part per million) =mg / kg < =Less Than (Total uncertainty=Results quoted have been corrected for uncertainty. -)

















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SAMPLE DESCRIPTION : Pepee Construction paper

BUYER : TÜKİD

DATE IN : 26 July, 2012 (13:59)

DATE OUT : 30 July, 2012



Part No Tested Part 1 RED PAPER 2 GREEN PAPER 3 BLUE PAPER 4 BROWN PAPER 5 PINK PAPER 6 ORANGE PAPER 7 BLACK PAPER 8 NAVY PAPER 9 YELLOW PAPER 10 GREY PAPER 11 MULTICOLOR PEPEE DESIGNED COVER






RESULTS :

Analysis Parameter



Tested Part



BS EN 71-3:1995 P -


EN 71-3 Part 1-11




Part 1-11








Part 1&2&3&4&5&6&7&8&9&10&11 1)Composite sample of Red,Green,Blue paper PASS 30 ppm 2)Composite sample of Brown,Pink,Orange paper PASS 30 ppm 3)Composite sample of Black,navy,yellow paper PASS 30 ppm 4)Grey paper PASS 30 ppm 5)Multicolor pepee designed cover PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN












Part 1 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 2 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 3 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 4 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 ppm (Part per million) =mg / kg < =Less Than (Total uncertainty=Results quoted have been corrected for uncertainty. -)





































































































































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SAMPLE DESCRIPTION : Spiderman A5 Metallize Checked Designed Notebook 80 Page

BUYER : TÜKİD

DATE IN : 26 July, 2012 (13:59)




Part No Tested Part 1 SPIDERMAN DESIGNED MULTICOLOR COVER 2 MULTICOLOR CHECKED PAPER 3 METAL WIRE






RESULTS :

Analysis Parameter



Tested Part



BS EN 71-3:1995 P -


EN 71-3 Part 1-3




Part 1-2








Part 1&2 1)Spiderman designed multicolor cover PASS 30 ppm 2)Multicolor checked paper PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN


































TEST REPOR Page 1 of 8

Zeynep Akın Neslihan Sözer Assistant Chemical Laboratory Manager Chemical Laboratory Manager




****110077364110077364110077364110077364**** 110077364

tugcekomurcu



Bağlar Mah. Çeşmealtı Sk. No:23 34209 Güneşli Đstanbul TÜRKĐYE FAX NO :0212 550 12 66

ADDRESS Attention :Muhiddin Keskin (mkeskin@keskinc olor.com)

SAMPLE DESCRIPTION : Ten samples of Ground color carton

BUYER : TÜKĐD

DATE IN : 04 August, 2011 (13:59)



Part No Tested Part Part No Tested Part 1 RED CARDBOARD 6 GREY CARDBOARD 2 YELLOW CARDBOARD 7 PINK CARDBOARD 3 BLACK CARDBOARD 8 ORANGE CARTBOARD 4 BLUE CARDBOARD 9 GREEN CARDBOARD 5 WHITE CARDBOARD 10 BROWN CARDBOARD






RESULTS :

Analysis Parameter



Tested Part

Azo Dyes 64 LFBG B 82.02.2 P - 30 ppm 2004/21/EC Part 1-10 Determination of perfluorooctane sulfonates (PFOS) & perfluorooctanoic acıd (PFOA)

INTERTEK IHTM AL-2-123 by LC/MS/MS P - 1 µg/m² 2006/122/EC Part 1-10

Formaldehyde JIS LAW 112 (Textile) 35 LFBG 82.02.1 (Leather)

P - 20 ppm 2002/371/EC Part 1-10

Toxic Element Analysis BS EN 71-3:1995 P -


EN 71-3 Part 1-10








Part 1&2&3&4&5&6&7&8&9&10 1) Composite sample of Red, Yellow, Black cardboard PASS 30 ppm 2) Composite sample of Blue, White, Grey cardboard PASS 30 ppm 3) Composite sample of Pink, Orange, Green cardboard PASS 30 ppm 4) Brown cardboard PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN

THE OFFICIAL COMPILATION OF TEST METHODS TEXTILE ACCORDING TO § 64 LFGB 82.02-2, LEATHER ACCORDĐNG TO § § 64 LFGB 82.02-3, PES ACCORDING TO § 64 LFGB 82.02-4, EXTRACTED BY CITRATE BUFFERED SOLUTION pH 6 AT 70 °C AND DETECTED BY GC/MS AND CONTROLLED BY HPLC/DAD AND THIN LAYER CHROMATOGRAPHIC ANALYSIS.

FORBIDDEN AMINE CAS NO 4-AMINOBIPHENYL 92-67-1 BENZIDINE 92-87-5 CHLORO-O-4-CHLOR-O-TOLUIDINE 95-69-2 2-NAPHTHYLAMINE 91-59-8 *O-AMINOAZOTOLUENE 97-56-3 *2-AMINO-4-NITROTOLUENE 99-55-8 P-CHLOROANILINE 106-47-8 2,4-DIAMINOANISOLE 615-05-4 4,4’-DIAMINOBIPHENYLMETHANE 101-77-9 3,3’-DICHLOROBENZIDINE 91-94-1 3,3’-DIMETHOXYBENZIDINE 119-90-4 3,3’-DIMETHYLBENZIDINE 119-93-7 3,3’-DĐMETHYL-4,4’ DIAMINOBIPHENYLMETHANE 838-88-0 P-CRESIDINE 120-71-8 4,4’-METHYLENE-BIS-(2 CHLOROANILINE) 101-14-4 4,4’-OXYDIANILINE 101-80-4 4,4’-THIODIANILINE 139-65-1 O-TOLUIDINE 95-53-4 2,4-TOLUYLENDIAMINE 95-80-7 2,4,5-TRIMETHYLANILINE 137-17-7 O-ANISIDINE 90-04-0 **P-AMINOAZOBENZENE 60-09-3


Remark < = Less Than ppm(part per million)= mg/ kg Detection Limit = 5 ppm Total Uncertainity = ±10%






Determination of Perfluorooctane sulfonates (PFOS) & Perfluorooctanoic Acid (PFOA) INTERTEK IHTM AL-2-123 : Solvent Extraction Followed By Liquid Chromotographic- Mass Spectrometric(LS-MS-MS) Analysis

Part 1 Result

PFOS (Perfluorooctane sulfonates) Not detected PFOA (Perfluorooctanoic Acid) Not detected

Part 2 Result


Part 3 Result


Part 4 Result


Part 5 Result


Part 6 Result


Part 7 Result


Part 8 Result


Part 9 Result


Part 10 Result

PFOS (Perfluorooctane sulfonates) Not detected PFOA (Perfluorooctanoic Acid) Not detected Detection Limit =0.25 ppb /0.5 µg/m² ND Not Detected (<0,25 ppb / <0.5 µg/m²)

Requirement 1µg/m² according to 2006/122/EC

(Total Uncertainty=±4 %)






Free Formaldehyde JIS LAW 112 Determination of Free Formaldehyde Content by UV-VIS Spectrophotometer : 2000 (for Textile)

35 LFBG 82.021 Determination of Free Formaldehyde Content by UV-VIS Spectrophotometer : 2000 (for Leather)

Part 1 <10 ppm 20 ppm Part 2 <10 ppm 20 ppm Part 3 <10 ppm 20 ppm Part 4 <10 ppm 20 ppm Part 5 <10 ppm 20 ppm Part 6 <10 ppm 20 ppm Part 7 <10 ppm 20 ppm Part 8 <10 ppm 20 ppm Part 9 <10 ppm 20 ppm Part 10 <10 ppm 20 ppm

ppm (part per million) =mg / kg Detection Limit =10 ppm < Less Than

(Total uncertainty=±6 %)








Part 1 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 2 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 3 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 4 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 ppm (part per million) =mg / kg < =Less Than (Total uncertainty=Results quoted have been corrected for uncertainty. -)
















Part 9 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 10 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 ppm (part per million) =mg / kg < =Less Than (Total uncertainty=Results quoted have been corrected for uncertainty. -)







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SAMPLE DESCRIPTION : One sample of Drawing Book with Spiral 17*25 cm

BUYER : TÜKĐD

DATE IN : 04 August, 2011 (13:59)



Part No Tested Part 1 MULTICOLOR COVER 2 WHITE PAPER 3 METAL WIRE






RESULTS :

Analysis Parameter



Tested Part

Azo Dyes 64 LFBG B 82.02.2 P - 30 ppm 2004/21/EC Part 1 Determination of perfluorooctane sulfonates (PFOS) & perfluorooctanoic acıd (PFOA)



P - 20 ppm 2002/371/EC Part 1-2



EN 71-3 Part 1-3








Part 1 Multicolor cover PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN










Determination of Perfluorooctane sulfonates (PFOS) & Perfluorooctanoic Acid (PFOA) INTERTEK IHTM AL-2-123 :

Solvent Extraction Followed By Liquid Chromotographic- Mass Spectrometric(LS-MS-MS) Analysis

Part 1 Result

PFOS (Perfluorooctane sulfonates) Not detected PFOA (Perfluorooctanoic Acid) Not detected Part 2 Result






Part 1 <10 ppm 20 ppm Part 2 <10 ppm 20 ppm










Part 1 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 2 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 Part 3 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 ppm (part per million) =mg / kg < =Less Than (Total uncertainty=Results quoted have been corrected for uncertainty. -)







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tugcekomurcu



Bağlar Mah. Çeşmealtı Sk. No:23 Güneşli Đstanbul TÜRKĐYE FAX NO :0212 550 12 66


SAMPLE DESCRIPTION : One sample of A4 Caligraphy notebook

BUYER : TÜKĐD

DATE IN : 04 August, 2011 (13:59)



Part No Tested Part 1 MULTICOLOR COVER 2 PAPER






RESULTS :

Analysis Parameter



Tested Part


INTERTEK IHTM AL-2-123 by LC/MS/MS

P - 1 µg/m² 2006/122/EC Part 1-2

Formaldehyde JIS LAW 112 P - 20 ppm 2002/371/EC Part 1-2



EN 71-3 Part 1-2








Part 1&2 1) Multicolor cover PASS 30 ppm 2) Composite sample of Pink, Blue, White paper PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN












Part 1 Result





Free Formaldehyde JIS LAW 112 Determination of Free Formaldehyde Content by UV-VIS Spectrophotometer : 2000

Part 1 <10 ppm 20 ppm


















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SAMPLE DESCRIPTION : One sample of A4 Notebook with plastic paper

BUYER : TÜKĐD

DATE IN : 04 August, 2011 (13:59)



Part No Tested Part 1 MULTICOLOR COVER 2 TRANSPARENT COVER 3 WHITE STRIPED PAPER 4 METAL WIRE






RESULTS :

Analysis Parameter



Tested Part





BS EN 71-3:1995 P -


EN 71-3 Part 1-4




Part 1-2

PAH ZEK 01-08 Method P - Total PAH <10 ppm BaP <1 ppm 2005/69/EC Part 1-2








Part 1&2&3 1) Composite sample of Multicolor cover PASS 30 ppm 2) Composite sample of Transparent cover, White striped paper INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN










Determination of Perfluorooctane sulfonates (PFOS) & Perfluorooctanoic Acid (PFOA) INTERTEK IHTM AL-2-123 : 2010


Part 1 Result













































Polycyclic Aromatic Hydrocarbons (PAHs) Analysis IHTM AL.2.032 ZEK 01-08 :

Harmonisierte Methode zur Bestimmung von polycyclischen aromatischen Kohlenwasserstoffen (PAK) in Kunststoffproben ZEK 01-08 AS SOLVENT EXTRACTION AND FOLLOWED BY GAS CHROMATOGRAPHY MASS SPECTROMETRIC (GC/MS) ANALYSIS

Part 1 RESULT (ppm) REQUIREMENT

NAPHTHALENE Not Detected Category 2 ACENAPHTHYLENE Not Detected Total 16 PAH : 10 mg/kg ACENAPHTHEN Not Detected Benzo(a)pyrene : 1 mg/kg FLUORENE Not Detected PHENANTHRENE Not Detected ANTHRACENE Not Detected FLUORANTHENE Not Detected PYRENE Not Detected BENZO (a) ANTHRACENE Not Detected CHRYSENE Not Detected BENZO (b) FLUORANTHENE Not Detected BENZO (k) FLUORANTHENE Not Detected BENZO (a) PYRENE Not Detected INDENO (1,2,3-cd) PYRENE Not Detected DIBENZO (a,h) ANTHRACENE Not Detected BENZO (ghi) PERYLENE Not Detected ---- SUM (16 PAH): Not Detected ppm (part per million) =mg / kg Detection Limit = 0.1 ppm n.d. = Not Detected

(Total Uncertainty= ± 3 %)

















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SAMPLE DESCRIPTION : One sample of Multicolour sticker with schedule

BUYER : TÜKĐD

DATE IN : 04 August, 2011 (13:59)



Sample No Tested Sample 1 MULTICOLOR STICKER WITH SCHEDULE






RESULTS :

Analysis Parameter



Tested Sample

Azo Dyes 64 LFBG B 82.02.2 P - 30 ppm 2004/21/EC Sample 1 Determination of perfluorooctane sulfonates (PFOS) & perfluorooctanoic acıd (PFOA)


P - 1 µg/m² 2006/122/EC Sample 1

Formaldehyde JIS LAW 112 P - 20 ppm 2002/371/EC Sample 1



EN 71-3 Sample 1








Sample 1 Multicolor sticker PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN




Remark < = Less Than ppm(Sample per million)= mg/ kg Detection Limit = 5 ppm Total Uncertainity = ±10%








Sample 1 Result





Sample 1 <10 ppm 20 ppm

ppm (Sample per million)

=mg / kg

Detection Limit =10 ppm < Less Than









Sample 1 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 ppm (Sample per million)

=mg / kg

< =Less Than (Total uncertainty=Results quoted have been corrected for uncertainty. -)







****110077374110077374110077374110077374**** 110077374

tugcekomurcu





SAMPLE DESCRIPTION : One sample of UV-LAK packing paper 50*70 cm

BUYER : TÜKĐD

DATE IN : 04 August, 2011 (13:59)



Part No Tested Part 1 MULTICOLOR PAPER






RESULTS :

Analysis Parameter



Tested Part

Azo Dyes 64 LFBG B 82.02.2 P - 30 ppm 2004/21/EC Part 1 Determination of perfluorooctane sulfonates (PFOS) & perfluorooctanoic acıd (PFOA)

INTERTEK IHTM AL-2-123 by LC/MS/MS P - 1 µg/m² 2006/122/EC Part 1

Formaldehyde JIS LAW 112 P - 20 ppm 2002/371/EC Part 1


BS EN 71-3:1995 P -


EN 71-3 Part 1








Part 1 Multicolor paper PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN












Part 1 Result















Part 1 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 ppm (part per million) =mg / kg < =Less Than (Total uncertainty=Results quoted have been corrected for uncertainty. -)







****110077373110077373110077373110077373**** 110077373

tugcekomurcu





SAMPLE DESCRIPTION : One sample of Bag with handle

BUYER : TÜKĐD

DATE IN : 05 August, 2011 (17:06)



Part No Tested Part 1 MULTICOLOR FILE 2 BLACK PLASTIC 3 RED PLASTIC






RESULTS :

Analysis Parameter



Tested Part





Part 1-3



EN 71-3 Part 1-3

PAH ZEK 01-08 Method P - Total PAH 10 ppm BaP 1 ppm 2005/69/EC Part 1-3








Part 1&2&3 1) Composite sample of Multicolor file PASS 30 ppm 2) Composite sample of red, black plastic PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN















































































****110077371110077371110077371110077371**** 110077371

tugcekomurcu





SAMPLE DESCRIPTION : Ten samples of Hand made paper

BUYER : TÜKĐD

DATE IN : 04 August, 2011 (13:59)



Part No Tested Part Part No Tested Part 1 YELLOW PAPER 6 GREEN PAPER 2 BLUE APER 7 PURPLE PAPER 3 BROWN PAPER 8 NAVY PAPER 4 ORANGE PAPER 9 BLUE PAPER 5 BLACK PAPER 10 RED PAPER






RESULTS :

Analysis Parameter



Tested Part





BS EN 71-3:1995 P -


EN 71-3 Part 1-10








Part 1&2&3&4&5&6&7&8&9&10 1) Composite sample of Yellow, Brown, Blue paper PASS 30 ppm 2) Composite sample of Orange, Black, Green paper PASS 30 ppm 3) Composite sample of Purple, Navy , Blue paper PASS 30 ppm 4) Red paper PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN










Determination of Perfluorooctane sulfonates (PFOS) & Perfluorooctanoic Acid (PFOA) INTERTEK IHTM AL-2-123 : Solvent Extraction Followed By Liquid Chromotographic- Mass Spectrometric(LS-MS-MS) Analysis

Part 1 Result


Part 2 Result


Part 3 Result


Part 4 Result


Part 5 Result


Part 6 Result


Part 7 Result


Part 8 Result


Part 9 Result


Part 10 Result










Part 1 <10 ppm 20 ppm Part 2 <10 ppm 20 ppm Part 3 <10 ppm 20 ppm Part 4 <10 ppm 20 ppm Part 5 <10 ppm 20 ppm Part 6 <10 ppm 20 ppm Part 7 <10 ppm 20 ppm Part 8 <10 ppm 20 ppm Part 9 <10 ppm 20 ppm Part 10 <10 ppm 20 ppm





























PP

Neslihan Sözer





****110077366110077366110077366110077366**** 110077366

tugcekomurcu





SAMPLE DESCRIPTION : One sample of A5 Notebook with glitter designed cover

BUYER : TÜKĐD

DATE IN : 04 August, 2011 (13:59)



Part No Tested Part 1 MULTICOLOR COVER 2 WHITE STRIPED PAPER 3 METAL WIRE






RESULTS :

Analysis Parameter



Tested Part





BS EN 71-3:1995 P -


EN 71-3 Part 1-3








Part 1&2 1)Multicolor cover PASS 30 ppm 2)White striped paper PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN












Part 1 Result






Part 1 <10 ppm 20 ppm Part 2 13 ppm 20 ppm

















****110077370110077370110077370110077370**** 110077370

tugcekomurcu





SAMPLE DESCRIPTION : One sample of A4 Tweety Notebook

BUYER : TÜKĐD

DATE IN : 04 August, 2011 (13:59)



Part No Tested Part 1 MULTICOLOR COVER 2 SILVER STRIPED WHITE PAPER 3 METAL WIRE






RESULTS :

Analysis Parameter



Tested Part




P - 20 ppm 2002/371/EC Part 1-2



EN 71-3 Part 1-3








Part 1&2 1) Multicolor cover PASS 30 ppm 2) Silver striped White paper PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN












Part 1 Result







Part 1 <10 ppm <20 ppm Part 2 <10 ppm <20 ppm













PP

Zübeyde Altürk





****120002660120002660120002660120002660**** 120002660

tugcekomurcu



Bağlar Mah. Çeşmealtı Sok. No: 23 34209 Güneşli Bağcılar Đstanbul FAX NO : 09 212 550 12 66

ADDRESS Attention : Muhiddin Keskin (mkeskin@keskinco lor.com.tr)

SAMPLE DESCRIPTION : One sample of Yellow/Pink/Blue/Orange/Green coated paper

BUYER : TÜKĐD

DATE IN : 09 January, 2012

DATE OUT : 23 January, 2012



Part No Tested Part 1 YELLOW PAPER 2 PINK PAPER 3 BLUE PAPER 4 ORANGE PAPER 5 GREEN PAPER

R E S U L T S Page 2 of 7 REPORT : TURA120002660 23 January, 2012





RESULTS :

Analysis Parameter



Tested Part



P - 1 µg/m² 2006/122/EC Part 1-5




EN 71-3 Part 1-5








Part 1&2&3&4&5 1) Composite sample of Yellow, Pink, Blue paper PASS 30 ppm 2) Composite sample of Orange, Green paper PASS 30 ppm INTERPRETATION OF AZO-DYES TEST RESULTS: AS PER GERMAN TEST PROCEDURE FOR DETECTION OF CARCINOGENIC AMINES IN DYED MATERIALS PUBLISHED IN












Part 1 Result






Detection Limit =0.25 ppb /0.5 µg/m² ND Not Detected (<0,25 ppb / <0.5 µg/m²)









Part 1 16 ppm 20 ppm Part 2 15 ppm 20 ppm Part 3 14 ppm 20 ppm Part 4 15 ppm 20 ppm Part 5 15 ppm 20 ppm

ppm (Part per million) =mg / kg Detection Limit =10 ppm < Less Than

















Part 5 Antimony (Sb) <2 ppm PASS 60 Arsenic (As) <2 ppm PASS 25 Barium (Ba) <2 ppm PASS 1000 Cadmium (Cd) <2 ppm PASS 75 Chromium (Cr) <5 ppm PASS 60 Lead (Pb) <5 ppm PASS 90 Mercury (Hg) <2 ppm PASS 60 Selenium (Se) <2 ppm PASS 500 ppm (Part per million) =mg / kg < =Less Than (Total uncertainty=Results quoted have been corrected for uncertainty. -)


Documents

REPORT NUMBER : TURA120090308 · R E S U L T S Page 2 of 6 REPORT : TURA120090308 02 August, 2012 Code Test Method Result Requirements Intertek Test Hizmetleri A.S . Merkez Mahallesi