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BHARATHIDASAN INSTITUTE OF TECHNOLOGY DEPARTMENT OF PETROCHEMICAL TECHNOLOGY
BHARATHIDASAN UNIVERSITY, TIRUCHIRAPPALLI-24
CHOICE BASED CREDIT SYSTEM (CBCS) FOR B.E / B.Tech (Petrochemical)
FULL – TIME PROGRAMME
Part 1: Regulations under Choice Based Credit Systems: Page - 2 Part 2: Curriculum for B.Tech (Petrochemical) Programme: Page -11 Part 3: Syllabi for Third & Fourth Semesters (Petrochemical): Page - 21
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BHARATHIDASAN INSTITUTE OF TECHNOLOGY (Formerly School of Engineering and Technology)
BHARATHIDASAN UNIVERSITY TIRUCHIRAPPALLI – 620 024.
CHOICE BASED CREDIT SYSTEM (CBCS) - REGULATIONS
(For the candidates admitted from the academic year 2005-2006 onwards)
BACHELOR OF TECHNOLOGY/ENGINEERING PROGRAMMES
S.No. Regulation
No. Content Page No.
1. 1. Eligibility for admission to B.Tech/B.E degree 3 2. 2. Age limit for admission to B.Tech/B.E degree 3 3. 3. Duration of Programme:
8 Semesters (4 academic years), 6 semesters (3 academic years) for lateral entry students
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4. 4. Eligibility for award of degree 4 5. 5. Branches of study 4 6. 6. Subjects of study 4 7. 7. Theory & Practical Examinations continuous assessment 4 8. 8. Distribution of theory subject Marks(30:70) & University
Practical Examination Marks 4
9. 9. Eligibility for appearance for semester examinations -Attendance criteria, - condonation fee, - Break System
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10. 10. Procedure for Completing the course -14 Consecutive semesters maximum( for I year admitted) -12 Consecutive semesters maximum( Diploma students)
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11. 11. Passing minimum and classification of successful candidates
- Passing Minimum - Award of Letter Grade - Grade Sheet Details
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12. 12. Procedure for applying Revaluation and Transparency - Maximum Period of Study - First Class with Distinction - First Class - Second Class
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13. 13. Provision for Withdrawal 8 14. 14. Discontinuation of the Course 9 15. 15. Revision of Regulations and Curriculum 9
CHOICE BASED CREDIT SYSTEM (CBCS) Regulations
(For the candidates admitted from the academic year 2005-2006 onwards)
DEGREE OF BACHELOR OF ENGINEERING/TECHNOLOGY
1. Eligibility criteria for Admission
1.1 Candidates for admission to the first semester of the eight semesters B.Tech/B.E Degree Programme should have passed the Higher Secondary Examination of the (10+2) curriculum (Academic Stream) prescribed by the Government of Tamil Nadu or any other examination equivalent thereto with minimum percentage of marks prescribed by Bharathidasan University (a mere pass for SC/ST candidates) in aggregate of subjects Mathematics, Physics and Chemistry.
OR
An examination of any University or authority recognized by the syndicate of Bharathidasan University as equivalent thereto.
1.2 Lateral Entry for Diploma passed candidates, for admission to third semester of the eight semester B.Tech/B.E Programme they should have passed three year diploma or four year sandwich diploma course in engineering/technology with a minimum of 60% marks in aggregate in the subjects covered in 3rd to 6th semester (a mere pass for SC/ST candidates). A list of diploma programmes approved for admission for each of the degree programme is given in Annexure - A.
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2. Age Limit and Medium of Instruction Candidates should not have completed 21 years of age as on 1StJuly of the academic year under consideration. For Lateral Entry admission to second year of degree programme candidates should not have completed 24 years as on Ist July of the academic year under consideration. For SC/ST candidates, the age limit is relaxable by 3 years for both the cases. The medium of instruction for the B.Tech/B.E Degree Programmes is English.
3. Duration of Programme
The Bachelor of Technology/ Engineering degree programme shall extend over a period of eight consecutive semesters (six semesters for Lateral Entry candidates) spread over four academic years (three academic years for Lateral Entry candidates) - two semesters constituting one academic year. The duration of each semester shall normally be 15 weeks excluding examination.
4. Eligibility for the Award of Degree
No candidate shall be eligible for the award of the degree of Bachelor of Technology/Engineering, unless he/she has undergone the course for a period of eight semesters (four academic years) / six semesters (three academic years for Lateral Entry candidates) and has passed the prescribed examinations in all the semesters.
5. Branches of Study
B.Tech. Degree Programmes B.Tech. Automobile Technology B.Tech. Biotechnology B.Tech. Petrochemical Technology B.Tech. Information Technology B.Tech Pharmaceutical Engineering and Technology
B.E Degree Programmes B.E. Computer Science and Engineering
B.E. Electronics and Communication Engineering B.E. Electrical and Electronics Engineering
Or any other branches of study as and when offered. The branch allocation shall ordinarily be done at the time of admission of the candidate to the first semester.
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6. Subjects of Study
The subjects of study shall include theory and practical as given in the scheme of examination and shall be in accordance with the prescribed syllabus. The subjects of study for the first two semesters shall be common for all branches of study.
7. Examinations
7.1 The theory and practical examinations shall comprise continuous internal assessment throughout the semesters in all subjects as well as end semester examinations conducted by Bharathidasan University under Autonomous status at the end of the semester (November/ December or April/ May).
8. Procedure for Awarding of Internal Marks
8.1 For Theory papers of 100 marks, Continuous Internal Assessment (C.I.A) marks will be 30. The Continuous Internal Assessment marks 30 has to be distributed as
12.5 marks each for two unit tests and 5 marks for class attendance in the particular subject.
The distribution of marks for attendance is as follows:
5 marks for 95% and above, 4 marks for 90% and above but below 95%, 3 marks for 85% and above but below 90%, 2 marks for 80% and above but below 85% and 1 mark for 75% and above but below 80%.
If a candidate is not able to attend any of the internal tests for valid reasons there will be make up test covering the entire syllabus.
8.2 Practical for which there is a university practical examination of 50 marks
The continuous internal assessment marks of 50 for laboratory subjects has to be distributed as
25 marks for the periodic practical works and records submitted thereof, 15 marks for an internal practical examination, 10 marks for an internal viva voce.
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9. Requirement for Appearing for End Semester Examination
A candidate shall be permitted to appear for end semester examinations at the end of any semester only if:
(i) He / She secures not less than 75% overall attendance arrived at by taking into account the total number of periods in all
subjects put together for the semester under consideration.
(Candidates who secure overall attendance of more than 60% and less than 75% have to apply for condonation along with condonation fee as prescribed by University and with a medical certificate obtained from medical officer not below the rank of Asst. Director. Students who have attendance below 60% are not eligible to appear for the examination.)
(ii) He/She earns a progress certificate from the Head of the Department having satisfactorily completed the course of study in all
the subjects pertaining to that semester. (iii) He/She should have paid the examination fees for the semester.
(iv) His/Her conduct is found to be satisfactory as certified by the Head of the Department. (v) In addition, the candidate shall satisfy the following conditions:
(a) To register for courses in 5th semester, the candidate should have earned a minimum of 40 credits for the I & II semesters put together.
(b) To register for the courses in 7th semester, the candidate should have completed all credit requirements in the I and II semesters and 40 credits in the 3rd and 4th semesters put together.
10. Procedure for completing the course
A candidate can join the course of study of any semester only at the time of its normal commencement and only if he/she has satisfied the course requirements for the previous semester and further has registered for the end semester examinations of the previous semester in all the subjects and as well as for all the arrear subjects if any.
There will be supplementary examinations within six weeks after the declaration of the even semester results. The supplementary examinations shall include the subjects covered during the odd and even semester of that year only. The entire course should be completed within fourteen consecutive semesters (seven years). The students admitted under lateral entry shall be allowed to complete the course within twelve consecutive semesters (six years).
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When the content of the curriculum or that of a subject in the curriculum is revised, a candidate will be permitted a maximum of three attempts to clear the subject(s) as per the old curriculum/syllabus. Thereafter the candidate has to appear entirely as per the revised curriculum. The revised curriculum shall contain a list of equivalent subjects (if any) to that in the old curriculum.
11. Passing Minimum and Classification of Successful Candidates
11.1A candidate shall be declared to have passed the examination in a subject of study only if he/she secures not less than 50% of the total marks (Continuous Internal Assessment(C.I.A) plus end semester examination marks) and not less than 40% marks in end semester examination.
11.2 Award of Letter Grades
The assessments of a course will be done on absolute marks basis. However, for the purpose of reporting the performance of a candidate, letter grades, each carrying certain points, will be awarded as per the range of total marks (out of 100) obtained by the candidate, as detailed below:
Range of Total
Marks Letter Grade Grade Point
91 to 100 S 10 81 to 90 A 9 71 to 80 B 8 61 to 70 C 7 55 to 60 D 6 50 to 54 E 5 0 to 49 F 0 ABSENT FA
F - Denotes failure in the course.
11.3 The internal assessment marks obtained by the candidate shall be considered only in the first attempt for theory subjects
alone. For the subsequent attempts, if the candidate obtains the minimum required percentage of marks in the end semester examination the Internal Assessment marks may be suitably adjusted to make the candidate pass. Further the Semester examination marks obtained in the latest attempt shall alone remain valid in total suppression of the Semester examination marks obtained by the candidate in earlier attempts. In the case of Arrear subjects, the candidates are required to obtain 50% of marks in the end semester exam for a pass.
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11.4 After the results are declared, Grade Sheets will be issued to the students. The grade sheet will contain the following details:
(a) The name of the institution (BIT) along with the name of Bharathidasan University. (b) The list of courses enrolled in each semester and the grades scored. (c) The Grade Point Average (GPA) for the semester and the Cumulative Grade Point Average (CGP A) of all the enrolled subjects from third semester onwards. (d) GPA is the ratio of sum of the product of the number of credits of courses registered and the corresponding grade points scored in those courses, taken for all the courses to the sum of the number of credits of all the courses.
[ ]⎥⎦⎤
⎢⎣⎡ ×=
C of
SumGPCofSumGPA
CGPA will be calculated in a similar manner, considering all the courses enrolled from third semester. However, 'F' and FA grades are to be excluded for calculating GPA and CGPA.
12. PROCEDURE FOR APPLYING FOR REVALUATION AND TRANSPARENCY 12.1 A candidate who has been declared "Failed" in a particular subject may reappear for that subject during the subsequent
semesters and secure a pass. However, there is a provision for revaluation in the failed or passed subjects provided he/she fulfills the following norms for revaluation.
(a) Applications for revaluation should be submitted within 15 days from the date of declaration of the result, through the Director.
(b) The candidate should have attended all the internal tests as well as end semester examination.
(c) If a candidate has failed in more than two papers in the current end semester examination, his/her representation for revaluation will not be considered.
(d) The request for revaluation must be made in the format prescribed and duly recommended by the Head of the Department along with the revaluation fee prescribed by the University. (e) The revaluation may be permitted as a special case, provided that the candidate gets the transparency of answer scripts and on the specific recommendation of the Head of the Department and Director for revaluation on the basis of the transparency. (f) The candidate who has sought for revaluation need not wait for the outcome of revaluation result. The candidate may
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register for the concerned paper(s) in the subsequent examinations. Late application for subsequent examinations on the ground that the candidate is waiting for the results of the revaluation will not be entertained at any cost. (g). The request for revaluation is not permitted for the supplementary examination mentioned in Para 2 of 10.
12.2 A candidate who satisfies the course requirements for all semesters and who passes all the examinations prescribed for all the
eight semesters within a MAXIMUM PERIOD OF 7 YEARS reckoned from the commencement of the first semester to which the candidate was admitted shall be declared to have qualified for the award of the degree. This period will be 6 YEARS for candidates admitted at the third semester level under lateral entry scheme.
12.3 A candidate who qualifies for the award of the degree passing in all subjects pertaining to semesters 3 to 8 in his/her first
appearance within 6 consecutive semesters (3 academic years) and in addition secures a CGPA of 8.50 and above for the semesters 3 to 8 shall be declared to have passed the examination in FIRST CLASS with DISTINCTION.
12.4 A candidate who qualifies for the award of the degree by passing in all subjects relating to semesters 3 to 8 within a
maximum period of 8 semesters after his/her commencement of study in the third semester and in addition secures CGPA not less than 6.5 shall be declared to have passed the examination in FIRST CLASS.
12.5 All other candidates who qualify for the award of the degree shall be declared to have passed the examination in SECOND
CLASS. 13. Provision for Withdrawal
A candidate may, for valid reasons, and on the recommendations of the Head of the Department be granted permission by the Director to withdraw from writing the entire end semester examination as one unit. The withdrawal application shall be valid only if it is made earlier than the commencement of the last theory examination pertaining to that end semester. Withdrawal shall be permitted only once during the entire course. Other conditions being satisfactory, candidates who withdraw are also eligible for the award of DISTINCTION whereas they are not eligible for the award of rank.
14. Discontinuation of Course
If a candidate wishes to temporarily discontinue the course for valid reasons, he/she shall apply through the Head of the Department in advance and obtain a written order from the Director permitting discontinuance. A candidate after temporary discontinuance may rejoin the course only at the commencement of the semester at which he/she discontinued, provided he/she pays the prescribed fees to the University. The total period of completion of the course reckoned from the commencement of the first semester to which the candidate was admitted shall not in any case exceed 7 years including of the period of discontinuance, when joining the course he will have to do the course as the curriculum and syllabi in force at the time of rejoining.
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15. Revision of Regulations and Curriculum
The Institute may from time to time revise, amend or change the regulations, curriculum and syllabus as and when found necessary.
ANNEXURE-A
B.Tech courses in which admission is sought
Diploma courses eligible for admission
Automobile Technology Automobile Engineering Mechanical Engineering Production Engineering Manufacturing Engineering Electrical & Electronics engineering Electronics & Communication Engineering Computer science Engineering Information Technology Electronics & Instrumentation Engineering Instrumentation & control engineering
Biotechnology Chemical Engineering Chemical Technology Petrochemical Technology Paper and Pulp Technology Polymer Technology Plastic Engineering Sugar Engineering Ceramic Technology Petroleum Engineering Plastic Engineering (Sandwich) Polymer Technology (Sandwich) Chemical Technology (Sandwich)
Petrochemical Technology Chemical Engineering Chemical Technology Petrochemical Technology
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Paper and Pulp Technology Polymer Technology Plastic Engineering Sugar Engineering Ceramic Technology Petroleum Engineering Plastic Engineering (Sandwich) Polymer Technology (Sandwich) Chemical Technology (Sandwich)
Information Technology Computer Science and Engineering Electronics and Communication Engineering And Electrical and Electronics Engineering
Information Technology Computer science & Engineering Computer Technology Electrical & Electronics Engineering Electronics & Communication Engineering Electronics & Instrumentation Engineering Electronics Engineering (Instrumentation) Electrical Engineering (Sandwich) Electrical Engineering (Instrumentation & Control) Instrument Technology Electrical Engineering electronics (WSI) Instrumentation & Control Engineering Instrumentation Engineering
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Pharmaceutical Engineering and Technology Chemical Engineering Chemical Technology Petrochemical Technology Paper and Pulp Technology Polymer Technology Plastic Engineering Sugar Engineering Ceramic Technology Petroleum Engineering Plastic Engineering (Sandwich) Polymer Technology (Sandwich) Chemical Technology (Sandwich) D.Pharm with Physics, Chemistry, Mathematics and Biology in H.Sc
DEGREE : B.TECH DEPT: CHEMICAL TECHNOLOGY
CURRICULUM FOR PETROCHEMICAL TECHNOLOGY
SEMESTER WORK LOAD , HOURS/WEEK CREDITS THEORY TUTORIAL PRACTICAL OTHERS TOTAL I 19 5 6 5 35 24 II 19 2 9 5 35 24 III 20 5 9 1 35 24 IV 20 4 9 2 35 25 V 20 6 9 1 35 27 VI 20 5 9 1 35 27 VII 20 4 9 2 35 27 VIII 16 5 12 2 35 22 TOTAL 154 36 72 19 280 200
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I SEMESTER: Curriculum and Syllabi common to B. Tech (Automobile, Bio Tech,
Petrochemical, Information Tech and Pharma) S.No. CODE SUBJECT L T P Cr IA UE TM
THEORY 1 EN0011 English 3 1 - 3 30 70 100
2 MA0011 Mathematics – I 3 2 - 4 30 70 100 3 PH0011 Physics 3 - - 3 30 70 100 4 CH0011 Chemistry 3 - - 3 30 70 100 5 AT0011 Basic Engineering
- I 4 - - 3 30 70 100
PRACTICALS 1 AT0021 Engineering
Drawing 3 2 - 4 50 50 100
2 PH0021 Physics Laboratory
- 3 2 50 50 100
3 AT0031 Workshop Laboratory
- - 3 2 50 50 100
Total 19 5 6 24 300 500 800 Counseling - 2 Library - 2 NSS / Hobby project - 1
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II SEMESTER: Curriculum and Syllabi common to B. Tech (Automobile, Bio Tech, Petrochemical, Information Tech and Pharma)
S.No. CODE SUBJECT L T P Cr IA UE TM THEORY 1 MA0022 Mathematics – II 3 2 - 4 30 70 100 2 AT0042 Basic Engineering -II 4 - - 3 30 70 100 3 PH0032 Material Science 3 - - 3 30 70 100 4 CH0022 Environmental Science 3 - - 3 30 70 100 5 IT0012 Introduction to
Information Tech 3 - - 3 30 70 100
PRACTICALS 1 CH0032 Chemistry Laboratory - - 3 2 50 50 100 2 IT0022 Introduction to
Information Tech Laboratory
- - 3 2 50 50 100
3 AT0052 Auto CAD Lab 3 - 3 4 50 50 100 Total 19 2 9 24 300 500 800 Counseling - 2 Library - 2 NSS / Hobby project - 1
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III SEMESTER:
S.No. CODE SUBJECT L T P Cr IA UE TM THEORY 1 MA0033 Mathematics III 4 1 - 3 30 70 100 2 CH0043 Organic Chemistry 4 - - 3 30 70 100 3 CT0013 Process Calculations 4 1 - 4 30 70 100 4 CT0023 Fluid Flow Operations 4 1 - 4 30 70 100 5 IT0063 Data Structures using C 4 - - 3 30 70 100 6 EN0023 General Proficiency-I - 2 - 1 50 - 50 PRACTICALS 1 CTP013 Fluid Flow Operations
Laboratory - - 3 2 50 50 100
2 ITP023 Computer Programming Laboratory
- - 3 2 50 50 100
3 CHP033 Organic Chemistry Laboratory
- - 3 2 50 50 100
Total 20 5 9 24 350 500 850 Extra Mural Lecture / Seminar - 1
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IV SEMESTER:
S.No.
CODE SUBJECT L T P Cr IA UE TM
THEORY 1 MA0044 Numerical Methods
and Statistics 4 1 - 3 30 70 100
2 CH0054 Physical Chemistry 4 - - 4 30 70 100 3 CT0034 Energy Technology 4 1 - 3 30 70 100 4 CT0044 Mechanical Operations 4 - - 4 30 70 100 5 CT0054 General Chemical
Technology 4 - - 4 30 70 100
6 EN0034 General Proficiency-II - 2 - 1 50 - 50 PRACTICALS 1 CTP024 Technical analysis
Laboratory - - 3 2 50 50 100
2 CHP044 Physical Chemistry Laboratory
- - 3 2 50 50 100
3 CTP034 Mechanical Operations Laboratory
- - 3 2 50 50 100
Total 20 4 9 25 350 500 850 Extra Mural Lecture / Seminar/Library - 2
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V SEMESTER
S.No. CODE SUBJECT L T P Cr IA UE TM THEORY 1 CT0065 Equilibrium
Thermodynamics 4 - - 4 30 70 100
2 CT0075 Process Heat Transfer 4 1 - 4 30 70 100 3 CT0085 Mass Transfer-I 4 1 - 4 30 70 100 4 CT0095 Process Equipment
Design 4 2 - 4 30 70 100
5 CTS115 Petroleum Refining Technology
4 - - 4 30 70 100
6 EN0045 General Proficiency-III - 2 - 1 50 - 50 PRACTICALS 1 CTP115 Petroleum Product Testing
lab-I - - 3 2 50 50 100
2 CTP145 Mass Transfer Lab-I - - 3 2 50 50 100 3 CTP155 Heat Transfer Lab - - 3 2 50 50 100 Total 20 6 9 27 350 500 850 Extra Mural Lecture / Seminar/Library - 1
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VI SEMESTER
S.No. CODE SUBJECT L T P Cr IA UE TM THEORY 1 CT0106 Transport Phenomena 4 1 - 4 30 70 100 2 CT0116 Mass Transfer-II 4 1 - 4 30 70 100 3 CT0126 Chemical Reaction
Engineering –I 4 1 - 4 30 70 100
4 CTS126 Natural Gas Engineering
4 - - 4 30 70 100
5 CTS136 Petrochemical Technology – I
4 - - 4 30 70 100
6 EN0056 General Proficiency-IV - 2 - 1 50 - 50 PRACTICALS 1 CTP166 Chemical Reaction
Engineering Lab - - 3 2 50 50 100
2 CTP176 Mass Transfer Lab-II - - 3 2 50 50 100 3 CTP126 Petroleum Product
Testing lab-II - - 3 2 50 50 100
Total 20 5 9 27 350 500 850 Library - 1
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VII SEMESTER S.No. CODE SUBJECT L T P Cr IA UE TM THEORY 1 CT0137 Process Dynamics &
Control 4 1 - 4 30 70 100
2 CT0147 Computer Aided Process Design
4 2 - 4 30 70 100
3 CT0157 Chemical Reaction Engineering-II
4 1 - 4 30 70 100
4 CTS147 Petrochemical Technology – II
4 - - 4 30 70 100
5 CTE1X7 Elective -I 4 - - 4 30 70 100 PRACTICALS 1 CTP137 Petrochemical Analysis
Lab - - 3 2 50 50 100
2 CTP187 Process Dynamics & Control Lab
- - 3 2 50 50 100
3 CTP127 a) Mini Project b) Seminar & Training Report
- -
- -
3 -
2 1
50 50
- -
50 50
Total 20 4 9 27 350 450 800
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Extra Mural Lecture / Seminar/Library - 2
VIII SEMESTER S.No. CODE SUBJECT L T P Cr IA UE TM THEORY 1 CT0168 Safety and
Environmental Engineering
4 - - 4 30 70 100
2 CT0178 Industrial Management 4 2 - 4 30 70 100 3 CT0188 Plant Utilities &
Operations 4 2 - 4 30 70 100
4 CTE2X8 Elective-II 4 1 - 4 30 70 100 PRACTICALS 1 CTP138 Project Work - - 12 6 50 100 150 Total 16 5 12 22 170 380 700 Personality Development/Library - 2
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ELECTIVE – I (VII Semester)
CTE117 PROCESS MODELING AND SIMULATION
CTE127 ENVIRONMENTAL IMPACT ASSESSMENT
CTE137 MULTICOMPONENT DISTILLATION
CTE147 POLYMER TECHNOLOGY
CTE157 PILOT PLANT AND SCALE UP PRACTISE
CTE167 PETROLEUM EXPLORATION AND EXPLOITATION TECHNIQUES
ELECTIVE – II (VIII Semester)
CTE218 ENERGY CONSERVATION IN CHEMICAL INDUSTRIES
CTE228 CHEMICAL PROCESS OPTIMISATION
CTE238 PINCH TECHNOLOGY
CTE248 NOVEL SEPARATION PROCESSES
CTE258 PETROLEUM PROCESS EQUIPMENT AUXILLRIES
CTE268 PLANT UTILITIES AND OPERATIONS
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III SEMESTER
MA0033 MATHEMATICS III
L: 4 T:1 Cr:3 TM:100
UNIT-I MULTIPLE INTEGRALS AND APPLICATIONS
Introduction - Double integral - Double integral in polar co-ordinates – Change the order of integration - Surface integral - Triple integral- Area as a double integral-volume integral.
UNIT-II
FOURIER SERIES Dirichlet's conditions - General Fourier series - Odd and even functions - Half range sine series - Half range cosine series - Complex form of Fourier series – Parseval’s identity - Harmonic Analysis.
UNIT-IV
BOUNDARY VALUE PROBLEMS Classification of second order quasi linear partial differential equations Solutions of one dimensional heat equation - One dimensional heat equation – Steady state solution of two -dimensional heat equation (Insulated edges excluded) Fourier series solutions in Cartesian co -ordinates. .
UNIT-IV
FOURIER TRANSFORM Fourier integral theorem (without proof) - Fourier transform pair - Sine and Cosine transforms - Properties - Transforms of simple functions - convolution theorem Parseval's identity.
UNIT-V
Z- TRANSFORMS AND DIFFERENCE EQUATIONS Z- Transform - elementary properties - Inverse Z- transform - Convolution theorem - Formation of difference equations - Solution of difference equations using Z-transform.
TEXT BOOKS
1. Kandasamy.P., Thilagavathy.K, and Gunavathy.K, " Engineering 2. Mathematics volume Ill", S.Chand & Company Ltd., New Delhi, 1996. 3. A.Singaravelu , “Engineering Mathematics-III.” Meenakshi Agencies Chennai-302.
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REFERENCE BOOKS
1. Narayanan.S., Manicavachagom PillayT.K and Ramaniah.G., “Advance Mathematics For Engineering Studies”, Vol.I, II and III S.Viswanathan pvt. Ltd.,Chennai,2002.
2. Grewal,B. S., " Higher Engineering Mathematics", Thirty sixth edition, Khanna Publishers, Delhi, 2001 .
3. Wylie C.Ray and Barrett Lousi, C., "Advanced Engineering Mathematics" Sixth edition, Mc Graw- Hill, Inc., New York, 1995.
CH0043 ORGANIC CHEMISTRY
L: 4 Cr: 3 TM: 100
OBJECTIVE
This paper serves the students to learn synthetic routes to many types of important organic Compounds preparations and their properties.
UNIT-I
ALKANES General methods of preparation, physical and chemical properties, ALKENES General methods of preparation, physical and chemical properties, Markovnikov rule, peroxide effect, Bayer’s test. ALKYNES General methods of preparation and properties monohydric alcohols: General methods of preparation, general properties, Saytzeff rule, methods of distinguishing the three classes of alcohols-Lucas test, dichromate test.
UNIT-II
ALDEHYDES AND KETONES General methods of preparation, physical and chemical properties, Aldol condensation, Clemmensesn reduction, Wolf-Kishner reduction. Haloform reaction, Cannizzaro reaction, Reformatsky reaction, Wittig reaction, Saturated rnonocarbozylic acids: Preparation, physical and chemical properties, Hell-Volhard-Zelinsky reaction. AMINO ACIDS Methods of preparation. Physical and chemical properties.
UNIT-III
BENZENE Aromaticity-Huckel rule, general methods of preparation of benzene, electrophilic substitution reactions of benzene, directive effects of substituents. AROMATIC AMINO COMPOUNDS General methods of preparation. Properties, carbylamines reaction.
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ARYLDIAZONIUM SALTS Preparation and synthetic applications
UNIT-IV
CARBOHYDRATES Classification, Monosaccharides-reactions of glucose and fructose, open chain and cyclic tructures of glucose and fructose, muta rotation, epimerization, Killiani-Fisher synthesis, Ruff degradation, conversion of aldoses to ketoses and ketoses to aldoses, Disaccharides- properties and structure of sucrose. Polysaccharides -properties and structure of starch and cellulose.
UNIT-V
HETEROCYCLIC COMPOUNDS AND ORGANOMETALLIC COMPOUNDS Preparation and properties of furan, thiophene, pyrrole, pyridine, quinoline and indole. Grignard reagents — preparation and synthetic applications.
TEXT BOOKS
1. Arun Bhal and B.S. Bhal, “Organic Chemistry”, S.Chand & Co., 16th edition, New Delhi, 2003
2. K.S. Tewari, S.N.Mehrotra and Vishnoi, “A Textbook of Organic Chemistry”, Vikash Publishing house Pvt. Ltd., New Delhi, 2003.
REFERENCE BOOKS
1. R.T.Morrison and Boyd, “Organic chemistry”, Prentice Hall of India ltd, 2003. 2. I.L. Finar, “Organic chemistry” (Vol-1), 6th Edition, Pearson Education, New Delhi, 2002. 3. Arun Bhal and B.S. Bhal, “Advansed Organic chemistry”, Sulthan chand and Sons, 2003.
CT0013 PROCESS CALCULATIONS
L: 4 T: 1 Cr: 4 TM: 100
OBJECTIVE
To study about Stoichiometry, Ideal gases, vapour pressure, humidity & solubility to make the process flow sheet with mass and energy balances.
UNIT – I
STOICHIOMETRY Introduction- Units and Dimensions - Stoichiometric principles-composition relations, density and specific gravity.
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UNIT – II
IDEAL GASES AND VAPOR PRESSURE Behavior of Ideal gases - application of ideal gas law- gaseous mixtures - volume changes with change in composition. Vapor pressure- effect of Temperature on vapor pressure-vapor pressure plots - vapor pressure of immiscible liquids-solutions.
UNIT – III
HUMIDITY AND SOLUBILITY Humidity - saturation - vaporization - condensation - wet and dry bulb thermometry -Solubility and Crystallization-Dissolution - solubility of gases.
UNIT – IV
MATERIAL BALANCE Material Balance- Processes involving chemical reaction-Combustion of coal, fuel gases and Sulphur - Recycling operations - Bypassing streams - Degree of conversion -excess reactant – limiting reactant
UNIT – V
ENERGY BALANCE Thermo chemistry - Calculation of Heat of reaction at other temperatures - Hess’s law of summation - heat of formation, reaction, mixing, combustion - mean specific heat -Theoretical flame Temperature.
TEXT BOOKS
1. B. I. Bhatt and S. M. Vora, " Stoichiometry", Ed. 4, Tata McGraw Hill Publishers Ltd.. New Delhi. 2004.
2. V.Venkataramani, N.Anantharaman “Process calculation”, Prentice Hall of India limited, New Delhi, 2003.
REFERENCE BOOKS
1. O.A.Hougen, K.M. Watson and R.A. Ragatz, "Chemical Process Principles", Vol-I, CBSPublishers and Distributors, New Delhi, 1995.
2. D. Himmelblau, "Basic Principles and Calculations in Chemical Engineering",6th Edn., Prentice Hall of India Ltd, New Delhi, 2000.
3. “Process Calculations for Chemical Engineering”, 2nd Revised edn. Chemical Engineering Education Development Centre, I.I.T, Madras, 1981.
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CT0023 FLUID FLOW OPERATIONS
L: 4 T: 1 Cr: 4 TM: 100 OBJECTIVE
This paper deals with the Concepts of fluid flow, Measurements and Transportation
UNIT – I
PROPERTIES OF FLUIDS AND CONCEPT OF PRESSURE Introduction - Nature of fluids - physical properties of fluids -types of fluids. Fluid statics: Pressure - density - height relationships-Pressure Measurement. Units & Dimensions. Dimensional analysis. Similarity - forces arising out of physical similarity - dimensionless numbers.
UNIT – II
MOMEMTUM BALANCE AND ITS APPLICATIONS Kinematics of fluid flow; Stream line-stream tube-velocity potential. Newtonian and non-Newtonian fluids - Time dependent fluids - Reynolds number - experiment and significance -Momentum balance - Forces acting on stream tubes - Potential flow - Bernoulli's equation - Correction for fluid friction - Correction for pump work.
UNIT – III
FLOW OF INCOMPRESSIBLE FLUIDS THROUGH DUCTS Flow of incompressible fluids in pipes- laminar and turbulent flow through closed conduits –velocity profile & friction factor for smooth and rough pipes-Head loss due to friction in pipes, fitting etc. Introduction to compressible flow-Isentropic flow through convergent and divergent nozzles and sonic velocity.
UNIT – IV
FLOW OF FLUIDS THROUGH SOLIDS Form drag-skin drag - Drag co-efficient -Flow around solids and packed beds- Friction factor for packed beds - Ergun's Equation - Motion of particles through fluids-Motion under gravitational and centrifugal fields - Terminal settling velocity. Fluidization - Mechanism, types- general properties - applications.
UNIT – V
TRANSPORTATION AND METERING Measurement of fluid flow Orifice meter, venturi meter, Pitot tube, rotameter, weirs and notches Wet gas meter and dry gas meter-Hot wire anemometers-Transportation of fluids-Fluid moving machinery performance-Selection and specification-Air lift and diaphragm pumps-Positive displacement pumps-Rotary & Reciprocating pumps-Centrifugal pumps-performance and characteristics.
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TEXT BOOKS
1. R.K. Bansal, “Fluid Mechanics and Hydraulic machines”, Laxmi Publications (P) Ltd., New Delhi. 1995
2. W.L. McCabe, J.C. Smith and P.Harriott, "Unit operations of Chemical Engineering", 6th Edn. McGraw Hill, International Edn.., 2001.
REFERENCE BOOKS
1. J.M. Coulson and J. F.Richardson, "Chemical Engineering", Vol I 3rd Edn.,Butterworth – Heinemann Publishers,2004
2. Noel.D. Nevers, "Fluid Mechanics for Chemical Engineers", McGraw Hill, International Edition. 1990.
3. Liggett de Nevers “Fluid Mechanics for Chemical Engineers”., McGraw Hill International Edn.., 1994.
IT0063 DATA STRUCTURES USING C
L: 4 Cr: 3 TM: 100
UNIT I
INTRODUCTION TO C Review of C – Constants, Variables and Data Types – Operators and Expression – Managing Input and Output Operators – Decision Making and Branching – Decision Making and Looping- Arrays – Handling of Character Strings.
UNIT II
FUNCTIONS AND POINTERS User-Defined Functions- Structures and Unions Pointers – The Preprocessor – Files.
UNIT III
ARRAYS, LISTS, STACKS AND QUEUES Arrays – Sparse matrices- Singly linked lists, The storage pool, Polynomial additions, more on linked lists, doubly linked lists and dynamic storage management, Generalised Lists. Garbage collection and compactions - The Stack ADT – The Queue ADT
UNIT IV
TREES AND GRAPHS Trees: Basic terminology, binary trees, binary tree representations, binary tree traversals, binary representations of trees, applications of trees. Graphs: Terminology and representations, Traversals, connected components and spanning trees. Shortest paths and transitive closure.
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UNIT V
SEARCHING AND SORTING Algorithm Analysis – Algorithm Strategies- Liner Search – Binary search- - Hashing – General Idea – Hash Function – Separate Chaining – Open Addressing – Linear Probing - Insertion Sort – Shellsort – Heapsort – Mergesort – Quicksort – External Sorting-
TEXT BOOKS
1. E.Balagurusamy, “Programming in ANSI C”, Tata Mc Grawhill , New Delhi, 2002. 2. Ellis Horowitz, Sartaj sahni “Fundamentals of Data structures” Galgotia Book source, New
Delhi. 2003
REFERENCE BOOKS
1. Aho, J. E. Hopcroft and J. D. Ullman, “Data Structures and Algorithms” 1983 2. Addison-Wesley Publishing Company, Ellis Horowitz, Sartaz Sahni, Sanguthevar
Rajasekaran, “Fundamentals of Computer Algorithms”, Galgotia Publications, 1983. 3. M. A. Weiss, “Data Structures and Algorithm Analysis in C”, 2nd edn, Pearson Education Asia,
2002.
N0023 GENERAL PROFICIENCY-I L: 0 T: 2 Cr: 1 TM: 50
OBJECTIVE
This paper helps the students learn the basics of communication, English through reading, speaking skills and to train for aptitude tests.
UNIT- I
BASICS OF COMMUNICATION Essential communication skills - elements of communication - basic models of communication - frames of reference - purposive communication - channels of communication - developing good communication style.
UNIT-II
LANGUAGE DEVELOPMENT THROUGH READING TOEFL-based reading comprehension - current affairs - vocabulary building- idioms and phrases - basic phonetics.
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UNIT- III
SPEAKING PRACTICE Dialogue/Conversation - types of conversations - listening skills - telephone etiquette - public speaking - debate.
UNIT –IV
QUANTITATIVE ANALYSIS Aptitude Tests
REFERENCE BOOKS
1. Bovee, Courtland Land John V Thill. “Business Communication Today”, Pearson Education, 2003.
2. Nicholls, Anne, “Mastering Public Speaking”, Jaico Publishing House, 2003. 3. Stanton Nicky, “Mastering Communication”, 4thedn., Palgrove Series, Macmillan,2004. 4. Rymniak, Marilyn J and Janet A Shanks, “TOEFL CBT EXAM”, Simon and Schuster, 2002. 5. Lewis, Norman, “Word Power Made Easy”, Bloomsbury, 2003. 6. Aggarwal, R.S. “Quantitative Aptitude”, S. Chand & Co., 2004.
CTP013 FLUID FLOW OPERATIONS LABORATORY
L: 0 P: 3 Cr: 2 TM: 100
LIST OF EXPERIMENTS
1. To verify Hagen-Poisulle Equation. 2. To relate Reynolds Number and Friction factor. 3. To study the effect of coil diameter on Friction factor. 4. Experiment on Orificemeter. 5. Experiment on Venturimeter. 6. Calibration of Rotameter. 7. To evaluate the performance of Weirs and Notches. 8. To evaluate the performance of Centrifugal pump. 9. Draining time of open tank. 10. To verify Ergun’s equation. 11. To characterize the behavior of Fluidized bed. 12. Performance of a packed bed. (Gas-Liquid)
30
ITP023 COMPUTER PROGRAMMING LABORATORY
L: 0 P: 3 Cr: 2 TM: 100 Implementation of the following using “C” language in Turbo “C”
1. Functions 2. Arrays 3. Structures 4. Unions 5. Pointers 6. File Processing 7. Searching 8. Sorting 9. Linked List 10. Stacks 11. Queues 12. Trees
CHP033 ORGANIC CHEMISTRY LABORATORY
L: 0 P: 3 Cr: 2 TM: 100
I. Organic Preparations:
Preparation of compounds involving the following reactions a. Acetylation b. Oxidation c. Reduction d. Halogenation e. Hydrolysis f. Diazotisation
II. Organic Qualitative Analysis :
The following groups of compounds are to be analysed Acids, Alcohols, Aldehydes, Amides, Amines, Esters, Ethers, Hydrocarbons, Ketones, Phenols and Sugars.
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III. Organic Quantitative Analysis
The following estimations are to be carried out a. Estimation of Esters b. Estimation of Amines c. Estimation of Carbonyl group d. Estimation of Hydroxyl group e. Estimation of Carboxyl group f. Estimation of Sugars
IV SEMESTER
MA0054 NUMERICAL METHODS AND STATISTICS
L: 4 T: 1 Cr: 3 TM: 100 UNIT-I
NUMERICAL SOLUTION OF ALGEBRAIC AND TRANSCENDENTAL QUATION Bisection method, False position, Newton-Raphson method, Iteration method and order of convergence.
UNIT-II
SOLUTION OF UNSTEADY STATE TRANSFER EQUATIONS Classification of PDE of the second order- Difference methods for solving boundary value problems involving elliptic, parabolic and hyperbolic equations- one dimensional wave equation and two dimensional Laplace and Poisson equations.
UNIT-III
SIMULATANEOUS LINEAR ALGEBRAIC EQUATION AND NUMERICAL DIFFERENTIATION AND NUMERICAL INTEGRATION Gauss elimination method, Jacobi’s method and Gauss –Seidal iterative method. Newton’s method to compute derivatives, Trapezoidal rule, Simpson’s rules.
UNIT-IV
RANDOM VARIABLES Random variables – Discrete and continuous random variable – Probability density functions- Distribution functions- Marginal and conditional probability distribution functions.
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UNIT-V
CORRELATION AND REGRESSION Mathematical expectations – Variants – Moment generating functions – Correlation coefficients – Regression.
TEXT BOOKS
1. Kandasamy.P, Thilakavathy.K and Gunavathy.K, “Numerical methods”, S.Chand and Co. New Delhi, 1999. 2. Guptha S.C., and Kapoor V.K.,- “Mathematical Statistics”, Sulthan chand and
sons,11th Edition, 2003. REFERENCE BOOKS
1. M.K.Venkatraman, “Numerical methods”, National Publishing company,1991. 2. A.Singaravelu, “Numerical methods” , Meenakshi Publication, Chennai.2000.
CH0054 PHYSICAL CHEMISTRY
L: 4 T: 0 Cr: 3 TM: 100
OBJECTIVE
This makes the students to learn the nature of chemical reactions taking place in solid, liquid and gaseous phases, Phases equilibria, Electrical conductance and Electrode Potential.
UNIT – I
GASEOUS STATE Vander Waal's equation, Law of equi partition principle, Translational, Rotational and vibrational energies of molecules, Joule-Thompson effect, liquefaction of gases. Critical constants.
UNIT – II
REACTION KINETICS Law of Mass action, Rate order and molecularity of chemical reactions. Methods for their evaluation. Calculation of rate constants. Chain reactions. Energy of activation - Theories on reaction rates. Heterogeneous reactions - Catalysis - Theory and applications - Inhibitors - Promoters - enzyme catalysis
UNIT – III
PHASE EQUILIBRIA AND SOLUTIONS Phase rule: Application - to one component system (water, sulphur and carbon dioxide). Two component systems (Eutectic, Intermediate compound formation and solid solutions) simple
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three component systems.Ideal and non-ideal solutions, solubility of gases in liquids, Henry’s law. Completely miscible liquids - Raoult's law - vapor pressure and boiling point diagrams. Partially miscible liquids - critical solution temperature, Completely immiscible liquids - Nernst distribution law – Dilute solution and their colligative properties. Molecular weight determination using these properties – Colloids – Colloidal electrolytes, electro-kinetic phenomena, gold number – separation of colloids.
UNIT – IV
ELECTRICAL CONDUCTANCE Electrolytes - strong electrolytes and weak electrolytes - Arrhenius theory of electrolytic dissociation. Debye - Huckell Onsager theory; Oswald’s dilution law - solubility of electrolytes and solubility product - common ion action - acids, bases - definitions based on proton transference, dissociation constant, amphoteric electrolyte - pH -Buffer solutions. Salts - water of crystallization, double salts, complex ions and salts.
UNIT – V
ELECTRODE POTENTIAL Electrode potential - Hydrogen electrode, reference electrodes, electrochemical series, Faraday's laws of electrolysis. Decomposition potential, over voltage, definitions of current density, current concentration, current efficiency, energy consumption; electrical conductance, oxidation – reduction redox couple; e.m.f. and energy relations. Conductometry. Potentiometry. their applications.
TEXT BOOKS
1. B. R. Puri and L. R. Sharma, M.S. Pathania, "Principles of Physical Chemistry", Shoban Lal Nagin Chand & Co., Jalandhar,1998.
2. P.L. Soni, "Text Book of Physical Chemistry ", S. Chand & Co., New Delhi,1970. REFERENCE BOOKS
1. K.J.Laidler and Meiser “Physical Chemistry” Harper and Row publishers/CBS publishers & Distributors, New Delhi,1995.
2. Gordon M.Barrow, “Physical chemistry” 6th edn., McGraw Hill,1996. 3. Barrow Gordon.M, “Physical chemistry” Boston WCB,1996.
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CT0034 ENERGY TECHNOLOGY
L: 4 T: 1 Cr: 4 TM: 100
OBJECTIVE
This paper deals with the Energy resources, their properties and utilization UNIT – I
COAL Coal – Properties and classification – Other solid fuels - Coal derived fuels; Characteristics, production methods and uses. Coal Combustion Technology, Waste heat recovery.
UNIT – II
OIL AND GASES Fuels from oil and gases - Characteristics, production methods and uses. Technology for combustion of fuels derived from oil and gas Liquid Fuels from sources other than petroleum – Types of gaseous fuels – Natural gas – Manufactured gas – Properties and Testing of gases.
UNIT – III SOLAR ENERGY
Solar energy utilization, Thermal application and photovoltaic applications; wind, geothermal and hydro energy utilization.
UNIT - IV
BIO ENERGY Biomass conversion for fuels; production methods based on thermo chemical and bioconversion. Characteristics and uses; Design of digesters.
UNIT – V NUCLEAR ENERGY
Nuclear Energy; Nuclear fission fuels processing, Nuclear reactions and nuclear reactors, Nuclear Engineering.
TEXT BOOKS
1. G. D. Rai, “Non Conventional Energy Sources”, Khanna Publishers, New Delhi,2004. 2. Samir Sarkar, “Fuels and Combustion”, 2nd Edn, Orient Longman Publications, 1988.
REFERENCE BOOKS
1. D.K.Singhal. “Fundamentals of Nuclear power Engineering” Khanna Publishers, New Delhi,2001.
35
2. Rao and Parulekar “Energy Technology- Non Conventional Renewable Resources” Khanna publishers. New Delhi,1999.
3. Sukhatme,SP “Solar Energy: Principle of Thermal Collection and Storage” New York MCG,1994.
CT0044 MECHANICAL OPERATIONS
L: 4 T: 0 Cr: 4 TM: 100
OBJECTIVE
This subject concerns with the properties, modification and separation of particulate solids in addition it gives a knowledge of designing processes and equipment in industrial handling solids.
UNIT – I CHARACTERISTICS OF PARTICULATE SOLIDS, SIZE REDUCTION AND
SCREENING Properties and characterization of particulate solids, analysis and technical methods for size and surface area distribution of powder; Introduction to size reduction equipment, determination of energy and power requirement in milling operations, computer simulation techniques for mill performance - Mechanical classifiers: Screening equipment, capacity and effectiveness.
UNIT – II FILTRATION
Filtration equipment, filtration media and filter aids, principles of filtration and clarification, Estimation of filtration parameters for compressible and incompressible cakes and calculations, centrifugal filtration equipment and principles of operation.
UNIT – III SETTLING AND SEDIMENTATION
Separation based on the motion of particles through fluids, gravity settling processes, Sedimentation, Kynch theory of sedimentation, equipment for sedimentation thickness, rate of sedimentation and sedimentation zones in continuous thickeners, design of thickeners and clarifiers, principles of centrifugal sedimentation.
UNIT – IV AGITATION AND MIXING
Introduction to agitation and mixing of liquids, agitation equipment, Axial and radial flow impellers and flow patterns in agitated vessels .prevention of swirling, Power consumption in agitated vessels. Blending and mixing, dispersion operations, mixing of solids and pastes and types of mixers.
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UNIT – V STORAGE AND CONVEYING OF SOLIDS
Introduction to storage and conveying of solids, bins, hoppers and silos, flow out of bins, design consideration of bins, loading and unloading of solids, Bucket elevators, apron conveyors, Belt conveyors: types of belt conveyors, selection considerations.
TEXT BOOKS:
1. Mc Cabe and J.C.Smith, Harriot "Unit Operation of Chemical Engineering", 6th Edn., McGraw Hill., New York, 2001
2. Badger and Banchero, "Introduction to Chemical Engineering", 1954 Tata McGraw Hill, New
3. Delhi,1954.
REFERENCE BOOKS:
1. Bhattacharaya, “Mechanial Operation”, Khanna publishers, New Delhi, 2001. 2. Raymond A. Kulweic, "Materials Handling Handbook", 3rd Edn, Wiley-Interscience
Publications, 1985. 3. M. Coulson and J.F.Richardson, "Chemical Engineering", Vol. II, 4th Edn., Butterworth –
Heineman, 2004.
CT0054 GENERAL CHEMICAL TECHNOLOGY
L: 4 T:0 Cr: 4 TM: 100
OBJECTIVE This paper deals with the manufacturing process of various inorganic chemicals in the
Chemical industries. UNIT-I
ALKALIES Chloro –alkali industries: Manufacture of Soda ash, Caustic Soda and Chlorine
UNIT-II
ACIDS Manufacture of Sulphuric acid, Hydrochloric acid and Phosphoric acid.
UNIT-III
GLASSES Manufacture of glasses and special glasses, Ceramics and Refractories,Paints and Pigments.
37
UNIT-IV
INDUSTRIAL GASES: Carbon dioxide, Nitrogen, Hydrogen, Oxygen and acetylene. Water treatment: Industrial and municipal water treatment.
UNIT-V
FERTILIZERS: Nitrogen fertilizers: Synthetic ammonia, urea, ammonium chloride, CAN, Ammonium sulphate. Phosphorous fertilizers: phosphate rock, Super phosphate, Triple Super Phosphate, MAP and DAP. Potassium fertilizers: Potassium chloride and Potassium sulphate.
TEXT BOOKS
1. Austin’s “Shreve’s chemical process industries”7th Edition McGraw Hill. NY, 1997 2. R.Gopal Rao and M.Sittig, “Drydens Outlines of Chemical Technology”, 2 nd Edition
Affiliated east-West press, New Delhi-1965 REFERENCE BOOKS
1. S.D.Shukla and G.N.Pandey, ”Text book of chemical technology” Vol-1, vikas publishing Co., 1977.
2. Sharma B.K, “Industrial chemistry”, Khanna Publishers,2001 3. Pandey.G.N, “Text Book of Chemical Technology” Vikas publishing house
Pvt Ltd., New Delhi, 1992.
EN0034 GENERAL PROFICIENCY-II
L: 0 T: 2 Cr: 1 TM: 50
OBJECTIVE
This paper teaches the importance of communication, personality development and verbal Communication.
UNIT-I
IMPORTANCE OF COMMUNICATION Introduction - verbal and non-verbal codes of communication - barriers to communication - self-assessment - SWOT analysis - identifying strengths and weaknesses.
38
UNIT-II
PERSONALITY DEVELOPMENT Body language - non-verbal skills - leadership qualities - emotional quotient - effective time management - surviving stress - overcoming failure - professional ethics.
UNIT-III
VERBAL COMMUNICATION Social exchanges - planned speech – extempore - basics of attending and organizing meetings - informal discussions.
UNIT-IV
QUANTITATIVE ANALYSIS Aptitude Tests.
REFERENCE BOOKS
1. Mohan, Krishna and Meera Banerji. “Developing Communication Skills”. Macmillan, 2002. 2. Minchinton, Jerry, “Maximizing Self-confidence”. Jaico Publishing House,2003. 3. Nicky Stanton, “Mastering Communications”. Palgrave Series, Macmillan,4th edn., 2004 4. Leigh, Andrew and Michael Maynard. “The Perfect Leader”. Random House Business Books,
1999. 5. “Perfect Communications”. Random House Business Books, 1999. 6. Thorpe, Edgar, “Course in Mental Ability and Quantitative Aptitude”. Tata McGraw-Hill,
2003.
CTP024 TECHNICAL ANALYSIS LABORATORY
L: 0 P: 3 Cr: 2 TM: 100
LIST OF EXPERIMENTS
1. Silica Content in Cement 2. Analysis of Oils and Fats 3. Analysis of Copper 4. Analysis of Bleaching Powder 5. Estimation of CaO in Lime 6. Analysis of Fertilizer 7. Analysis of Fatty Acid Content and Alkali Content in soaps 8. Pigment Analysis 9. Water Analysis 10. Flame Photometer 11. Colorimetry
39
CHP044 PHYSICAL CHEMISTRY LABORATORY
L: 0 P: 3 Cr: 2 TM: 100 LIST OF EXPERIMENTS
1. Molecular weight determination a) Rast’s Method b) Molecular weight determination of polymer by using viscosity
2. Partition Coefficient Studies
a) For Benzene – Water system
3. Phase rule Studies a) Simple Eutectic system
4. Conductivity Studies
a) Acid – Base Titration b) Precipitation Titration c) Mixtures of acid – Strong Base Titration
5. EMF Studies
a) Estimation of Cr3+ by potentiometric Titration
6. Kinetic Studies a) Kinetic studies of Persulphate – Iodide reaction b) Kinetic studies of Iodination of Acetone. c) Determination of Rate constant of Acid catalyst hydrolysis of an Ester.
7. Polarimetry Studies
a) Kinetic study of Inversion of Cane sugar.
8. Adsorption Studies a) Freundlich Adsorption Isotherm
CTP034 MECHANICAL OPERATIONS LABORATORY
L: 0 P: 3 Cr: 2 TM: 100
LIST OF EXPERIMENTS
1. Screen Effectiveness 2. Jaw Crusher 3. Ball Mill 4. Drop weight Crusher 5. Beaker Decantation 6. Air Elutriation 7. Vacuum Leaf Filter
40
8. Plate and Frame Filter press 9. Grind ability Index 10. Batch Sedimentation 11. Cyclone Separator 12. Terminal settling velocity - Stokes law Verification. 13. Mixing Index
V SEMESTER
CT0065 EQUILIBRIUM THERMODYNAMICS
L: 4 Cr: 4 TM: 100 OBJECTIVE
To educate the students in the area of Thermodynamics as applied to various Chemical Engineering processes
UNIT-I FUNDAMENTALS OF THERMODYNAMICS
Laws of thermodynamics as applied to open and closed system- reversible and irreversible processes- Thermodynamics properties, Concepts of Internal energy, Enthalpy and Entropy- State and Point function – Absolute Entropy. Principles of Heat engine and refrigeration- Thermodynamic property changes for ideal gas.
UNIT-II
PVT RELATIONS PVT relations for gases and liquids-equations of state, cubic equation of state-thermodynamic properties from equation of state, compressibility factor, generalized properties of fluids- law of corresponding state, acentric factor, gas mixtures
UNIT-III
THERMODYNAMIC RELATIONS Thermodynamic relation-Maxwell’s relation-estimation of thermodynamic properties-thermodynamic properties of homogeneous mixtures- partial molar properties, fugacity and fugacity coefficients- Lewis and Randall rule – property changes of mixing, Activity- Excess properties, Activity Coefficients.
UNIT-IV PHASE EQUILIBRIA
Phase equilibria- pure component and mixtures – Van Laar, Margules equation, Group Contribution method- Gibb’s Duhem equation – Consistency tests – Partially Miscible and Immiscible systems- Azeotropes. Retrograde Condensation – Thermodynamic diagrams.
41
UNIT-V CHEMICAL REACTION EQUILIBRIA
Chemical equilibria – Heat effects, Industrial reactions – Free energy calculations – Homogeneous reactions – Industrial reactions like NH3 synthesis, SO3 production etc.
TEXT BOOKS
1. J.M.Smith and Van Ness, “Introduction to Chemical Engineering Thermodynamics”, Ed.5, McGraw Hill, New York, 1996.
2. S.Sundaram, “Chemical Engineering Thermodynamics”, Ahuja Publishers, New Delhi, 1998.
REFERENCE BOOKS
1. Hougen and Watson. “Chwemical process Principles” Vol. II, CBS Publishers, New Delhi, 2002.
2. Ryle, “Chemical process Thermodynamics”, Ed. 2. Prentice Hall of India, New Delhi, 2000. 3. K.V.Narayanan, “A Text Book of Chemical Engineering Thermodynamics”, Prentice Hall of
India, New Delhi, 2002.
CT0075 HEAT TRANSFER
L: 4 T: 1 Cr: 4 TM: 100
OBJECTIVE
To improve the fundamental knowledge of various modes of heat transfer and to understand the basic concepts of heat transfer equipment design, which has more application in process industries.
UNIT –I CONDUCTION Modes of Heat Transfer- Concept of heat conduction – Fourier’s law of heat conduction–
one dimensional steady state heat conduction equation for flat plate, hollow cylinder, hollow sphere- Analogy between flow of heat and flow of electricity –Thermal conductivity measurement; effect of temperature on thermal conductivity, Individual and overall heat transfer coefficients and the relationship between them – Conduction with heat source. Heat Transfer in extended surfaces. Transient heat conduction-Lumped parameter Model, Unsteady state equation with boundary condition (Solution not included)
UNIT –II CONVECTION Concept of heat transfer by convection – Natural and forced convection – Application of
dimensional analysis for convection – Equations for forced convection under laminar, transient and turbulent conditions – Equations for natural convection- – Influence of boundary layer on heat transfer- Heat transfer through packed and fluidized beds.
42
UNIT –III
HEAT TRANSFER WITH PHASE CHANGE Heat transfer from condensing vapors, drop wise, film wise condensation, Nusselt’s
equation for vertical and horizontal tubes, Condensation of superheated vapors, effect of non-condensables on rate of condensation. Heat transfer to boiling liquids- mechanism of boiling, nucleate boiling and film boiling
UNIT – IV RADIATION Concept of thermal radiations – Black body concept – Stefan Boltzman’s law-Emissive
power-Black body radiation, Emissivity, Plank’s Law – radiation between surfaces - View factor for infinitely parallel grey planes. Radiation Shields.
UNIT – V HEAT EXCHANGERS Parallel and counter flow heat exchangers- Log mean temperature difference – single pass and
multi pass heat exchangers; use of correction factor charts; heat exchangers effectiveness; number of transfer unit – Chart for different configurations –Dirt Factor– Condensers.
EVAPORATORS Single effect and multiple effect evaporation –, boiling point rise, capacity and economy of
multiple effect evaporators, evaporation equipments. TEXT BOOKS
1. D.S. Kumar, “Heat and Mass Transfer” S.K. Kataria & Sons, Edition 5, 1997. 2. W. L. McCabe and J. C. Smith, “Unit Operations In Chemical Engineering", 5th Edn. McGraw
Hill Publishing Co., 2001. 3. F. Kreith,”Principles of Heat Transfer”, 4th Edition, Harper & Row, 1976.
REFERENCE BOOKS
1. D. Q. Kern, “Process Heat Transfer", Tata McGraw Hill Publishing Co., New Delhi, 1990. 2. Hollman. "Heat Transfer". McGraw Hill, 8th Edn, 1997. 3. Binay k. Dutta, ‘‘Heat Transfer’’, PrenticeHall Publications.
43
CT0085 MASS TRANSFER-I
L: 4 T: 1 Cr: 4 TM: 100
OBJECTIVE
This subject deals with fundamentals of mass transfer and some of its mass transfer operations like diffusion, absorption, humidification, drying & crystallization.
UNIT-I
DIFFUSION Diffusion in fluids: Molecular and eddy diffusion, measurement and calculation of diffusivities. Ordinary diffusion in multi component gaseous mixtures. Diffusion in solids. Theories of Diffusion.
UNIT-II
INTERPHASE MASS TRANSFER AND ABSORPTION Interphase Mass Transfer: Mass Transfer Coefficients, theories of Mass Transfer. Concept of NTU and HTU. Analogies between momentum and mass transfer. Equilibrium and Operating lines.JD Factor. Absorption: Theories of Gas Absorption-design of absorption Towers. Absorption with chemical reactions. Tower packing and characteristics.
UNIT-III
HUMIDIFICATION Humidification, Theory, psychometric charts. Methods of humidification and dehumidification. Air Conditioning and Cooling Tower Design.
UNIT-IV
DRYING Drying characteristics of materials. Theory and mechanism of drying. Estimation of drying rates. Different types of dryers. Design and performance of continuous and batch dryers.
UNIT-V
CRYSTALLISATION Factors governing nucleation and crystal growth. Theory of crystallization, Classification of crystallizer and their applications. Product size distribution. Design of Industrial crystallizers.
TEXTBOOKS
1. R.E.Trebal,”Mass Transfer Operations: , 3rd Edn., McGraw-Hill Book Co., New York,1980.
44
2. W.L.McCabe, J.C.Smith and P.Harriot, “Unit Operations of Chemical Engineering”, 5th Edn. , McGraw-Hill Book Co., New York, 1993.
3. Christie J.Geankoplis, “Transport Processes and unit operations”, 3rd Edn., Prentice Hall of India Pvt. Ltd, New Delhi, 2000.
REFERENCE BOOKS
1. J.M.Coulson and J.F.Richardson,”Chemical Engineering”, Vol.I, II, III, Pergamon Press, N.Y. 1977.
2. Alan S.Foust, Leonard A.Wenzel, Curtis W.Clump, Louis Maus, L.Bryce Andersen, “Principles of unit operations”, 2nd Edn., John Wiley & Sons (Asia) Pvt. Ltd.
3. C.O.Bennett, J.E.Myers, “Momentum, Heat & Mass Transfer”, 3rd Edn., McGraw Hill Book Company.
CT0095 PROCESS EQUIPMENT DESIGN
L: 4 T: 2 Cr: 4 TM: 100
OBJECTIVE
To understand the design concepts of various process equipments UNIT-I
BASIC CONSIDERATIONS, MATERIALS OF CONSTRUCTION AND DESIGN ASPECTS Basic Considerations In Process Equipment Design-General Design Procedure, Fabrication Techniques, Equipment Classification. Materials of Construction-Materials, Protective Coatings, Corrosion Prevention, Linings for Chemical Plants and Equipments, Choice of Materials. Design Considerations.
UNIT-II
PRESSURE VESSELS Pressure Vessels-Operating Conditions, Selection of Material, Vessels Operating at Low and Elevated Temperatures, Design Condition, Supports, Stresses, Fabrication. High Pressure Vessels.
UNIT-III
STORAGE VESSELS Storage Vessels-Storage of Fluids, Volatile and Non Volatile Liquids, Gases, Design of Tanks and Rectangular Tank. Nozzles and Mountings, Large Capacity Storage Tanks.
UNIT-IV
REACTION VESSELS AND HEAT EXCHANGERS Reaction Vessels-Materials of Construction, Agitation, Classification of Reaction Vessels, Heating Systems, Design Consideration. Heat Exchangers-Introduction, Types of Heat Exchangers, Design of Shell and Tube Heat Exchangers, Numerical Problems
45
UNIT-V
TALL COLUMNS Distillation and Absorption Towers/Columns-Introduction. Basic Features of Columns, Data, Column Intervals, Stresses in Column Shell, Determination of Columns Shell, Determination of Shell Thickness, Allowable Deflection, Column Internals, Supports for Column, Numerical Problems
TEXT BOOKS
1. M.V.Joshi and V.V.Mahajan, “Process Equipment Design”, Macmillan India Limited, 3rd Edition, 1996
2. B.C.Bhattacharyya, “Introduction To Chemical Equipment Design Mechanical Aspects”, CBS Publishers and distributors, New Delhi, Ist Edn., 1985
REFERENCE BOOKS
1. S.D.Dawande, “Process Design Of equipments” Central Techno publishers, Nagpur, Vol.I&II, 2003
2. L.E.Brownell and E.H.young, “Process Equipment Design”, John wiley, New York, 2004 3. R.H.Perry, “Chemical Engineers Hand Book”, 7th Edn., McGraw Hill, New York, 1998.
CTS115 PETROLEUM REFINING TECHNOLOGY
L: 4 T: 0 Cr: 4 TM: 100 OBJECTIVE
To make the student understand the basic concepts involved in the crude processing and testing of petroleum products.
UNIT-I GENERAL
Orgin, Exploration and production of petroleum, Types of Crudes, Crude Composition, Characteristics and Classification, Indigenoues and Imported Crudes, Availability Vs Demands.
UNIT-II TESTING OF PETROLEUM PRODUCTS
IS 1448: Standard, Testing of petroleum crude, Products: Specifications & their Significance: ASTM, TBP and EFV curves, Midpercent and Yield curves.
46
UNIT-III CRUDE PROCESSING
Pretreatment of crude for Refining – Dehydration and Desalting, Atmospheric Distillation, Vacuum Distillation of residue products & Distillation practice.
UNIT-IV SECONDARY PROCESSES
Thermal Cracking, Visbreaking, Coking, Fluid Catalytic Cracking, Hydro Cracking, Catalytic Reforming and Alkylation Process, Sulphur Removal Techniques.
UNIT-V
LUBE DISTILLATE TREATMENT TECHNIQUES Treatment Techniques for Vaccum Distillates with different processes like Solvent Extraction, Deasphalting, Dewaxing and Hydrofining, Production of Lubricating Oils, Lube Blending, Production of Bitumen.
TEXT BOOKS
1. Dr. Ram Prasad, “Petroleum Refining Technology”, Khanna Publishers, New Delhi.2000. 2. B.K. Bhaskara Rao, “Modern Petroleum Refining Processes” Edn.3, Oxford & IBH Publishing
Company Pvt. Ltd. New Delhi.1998. REFERENCE BOOKS
1. Watkins.R.N, “Petroleum Refinery Distillation”, 2nd Edn. Gulf Publishing Company, Texas, 1981.
2. Hobson.G.D, “Modern Petroleum Refining Technology”, 4th Edn., Institute of Petroleum, U.K. 1973.
3. Nelson.W.L, “Petroleum Refinery Engineering”, McGraw Hill Publishing Company Ltd., New York, 1985.
EN0045 GENERAL PROFICIENCY- III
L: 0 T: 2 Cr: 1 TM: 50
OBJECTIVE
The main objective is to improve the students Communication, writing presentation skills and quantitative analysis skills for their future career.
47
UNIT-I
COMPOSITION ANALYSIS Technical and Nontechnica1 Passages (GRE Based); Differences in American and British English; Analyzing Contemporary Issues; Expanding Terminology
UNIT-II
DEXTERITY IN WRITING Importance of Writing; Written vs. Spoken Language; Formal and Informal Styles of Writing; Resources for Improving Writing; Grammar and Usage; Letter- Writing; Application Essays; Project Proposals
UNIT-III
PRESENTATION SKILLS Collecting and Organizing Materials; Audience; Content; Rehearsing; Delivering Matter; Questions; Controlling Anxiety; Seminar Presentations (Subject Oriented General Topics); Language lab Practice
UNIT-IV
QUANTITATIVE ANALYSIS Aptitude Tests; Puzzles; Psychometric Tests
TEXT BOOKS
1. Leigh, Andrew and Michael Maynard. The Perfect Presentation. Random House Business Books, 1999.
2. Thorpe, Edgar. Test of Reasoning. Tata McGraw4lill, 2003. 3. A.K.Paliwal, “Communication skills in English”, Surabhi Publications.
REFERENCE BOOKS
1. Bhatnagar, R.P and Rajul Bhargava. English for Competitive Examinations. Macmillan, 1999. 2. Thorpe, Edgar and Showick Thorpe. Objective English. Pearson Education 2004. 3. Staff of Kaplan. GRE Exam 2004. Simon and Schuster, 2003.
CTP115 PETROLEUM PRODUCT TESTING LAB-I
P: 3 Cr: 2 TM: 100
1. Determination of flash point by Pensky Marten Closed cup apparatus. 2. Determination of flash point by Abel Open cup Apparatus. 3. Determination of kinematic viscosity by Redwood Viscometer. 4. Determination of kinematic viscosity by Saybolt Viscometer. 5. Determination of kinematic viscosity by Engler Viscometer. 6. Determination of kinematic viscosity by U tube Viscometer. 7. API gravity Determination.
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8. Moisture Determination by Dean and Stark Method. 9. Water determination by Karl-Fischer conductometr Apparatus. 10. ASTM Distillation. 11. Vacuum Distillation. 12. Determination of Calorific Value By Junker’s Gas Calorific meter. 13. Reid Vapor Pressure Estimation.
CTP145 MASS TRANSFER LABORATORY-1
P: 3 Cr: 2 TM: 100
LIST OF EXPERIMENTS
1. To determine the critical moisture content and drying rate under atmospheric conditions. 2. To determine the critical moisture content and drying rate under vacuum. 3. To verify Rayleigh equation. 4. To determine the efficiency of Steam distillation. 5. To determine diffusion coefficient. 6. To determine HETP. 7. To optimize the number of leaching stages. 8. To determine the break point for Adsorption. 9. To relate mass transfer coefficient with Reynolds Number.
CTP155 HEAT TRANSFER LABORATORY
P: 3 Cr: 2 TM: 100
LIST OF EXPERIMENTS 1. To determine the conduction parameters. 2. To relate Heat transfer coefficient with Reynolds Number. 3. To determine Stefan Boltzman law constant. 4. To determine condensing Heat transfer coefficient. 5. To study the effect of stirring on Heat transfer coefficient. 6. To study the effect of coil diameter on Heat transfer coefficient. 7. To determine overall Heat transfer coefficient. 8. To study the effect of open pan evaporation.
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VI SEMESTER
CT0106 TRANSPORT PHENOMENA
L: 4 T: 1 Cr: 4 TM: 100 OBJECTIVE To make the student understand the fundamentals of heat, mass and momentum transfer. UNIT-I
BASIC CONCEPTS Phenomenological equations and transport properties. Rheological behavior of fluids, balance equations-Differential and integral equations. Applications of Differential Equations of change: Applications in laminar and turbulent in compressible and incompressible fluids, Boundary Layer theory.
UNIT-II
APPLICATIONS OF INTEGRAL EQUATIONS OF CHANGE Macroscopic Balances of isothermal and non isothermal systems and their applications in momentum, heat and its applications for packed bed –mass transport problems.
UNIT-III
INTERPHASE AND MULTIPHASE MOMENTUM TRANSFER Friction Factor, Fluid-fluid systems-Flow patterns in vertical and horizontal pipes. Formation of bubbles and drops and their size distribution, Solid-fluid systems-forces acting on stagnant and moving solids. Flow through porous medium- Capillary tube model and filters, fluidized bed, solid fluid conveying, settling and sedimentation.
UNIT-IV
INTERPHASE TRANSPORT IN NON ISOTHERMAL AND RADIATION HEAT TRANSFER: Heat Transfer Coefficient, Forced Convection in tubes, around submerged objects, through packed beds. Heat transfer by free convection, film wise and drop wise condensation and equations of Heat transfer Coefficients for both, Heat transfer in Boiling Liquids.
UNIT-V
INTERPHASE MASS TRANSPORT AND MACROSCOPIC BALANCES FOR MULTI COMPONENT SYSTEM Mass Transfer Coefficient in one and two phases at low and high mass transfer rates, Film Theory, Penetration Theory, Boundary Layer Theory, Fixed Bed Catalytic reactor, Macroscopic Balances to solve steady and unsteady state problems.
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TEXT BOOKS
1. Bird.R.B., W.E.Stewart and E.N.Light foot-Transport Phenomena- John Wiley and sons, 2002. 2. William J.Thomson,”Introduction to Transport Phenomena”, Pearson Education Asia, 2000. 3. C.O.Bennett, J.E.Myers, “Momentum, Heat & Mass Transfer”, 3rd Edn. McGraw Hill Book
Company.
REFERENCE BOOKS
1. Welty, J.R., C.E.Wick and R.E.Wilson-Fundamentals of Momentum, Heat and Mass Transfer, John Wiley Sons, 2002.
2. Sissom.L.E., and D.R.Pitts-Elements of Transport Phenomena, McGraw-Hill, NY, 1972 3. Brodkley, R.S. and H.C.Hershey-‘Transport Phenomena, An United Approach’, McGrawHill,
1998.
CT0116 MASS TRANSFER II
L: 4 T: 1 Cr: 4 TM: 100 OBJECTIVE
This subject will enable the students to learn the concepts of principles, applications of distillation, extraction and adsorption operations.
UNIT-I DISTILLATION Vapour Liquid Equilibrium Data, Methods of distillation-batch, continuous, flash, steam,
vacuum, molecular, azeotropic and extractive distillations. UNIT-II CONTINUOUS FRACTIONATION Stage-wise & Continuous contact operations, Design calculations- McCabe-Thiele method,
Ponchon-Savorit Method, elements of multi component distillation. UNIT-III LIQUID-LIQUID EXTRACTION Extraction, Liquid-Liquid Equilibrium data, Liquid-Liquid extraction-Triangular diagrams,
Batch & continuous extractions, Design of Extraction towers. UNIT-IV ADSORPTION Types of adsorption, nature of adsorption, Theories of adsorption, Adsorption isotherms,
Recovery of solvent vapours, Operation of adsorption columns, Batch & continuous operations.
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UNIT-V LEACHING Solid-Liquid extraction, Batch & Continuous operations. TEXT BOOKS
1. R.E. Treybal, “Mass Transfer Operations”, 3rd Edn., McGraw Hill Book Co. New York, 1980. 2. W.L. Mccabe, J.C.Smith and P.Harriot, “Unit Operations in Chemical Engg.”, 5th Edn.,
McGraw Hill Book Co., New York, 1993. 3. C.J. Geankopolis, “Transport Processes in Chemical Operations”, 3rd Edn., Prentice Hall of
India, New Delhi, 1996. REFERENCE BOOKS
1. M.Coulson & J.F. Richardson, “Chemical Engg.”, Vol-II, 3rd Edn., Pergamon Press, New York, 1987.
2. Alan S.Foust, Leonard A.Wenzel, Curtis W.Clump, Louis Maus, L.Bryce Andersen, Principles of unit operations”, 2nd Edn., John Wiley & Sons (Asia) Pvt. Ltd.
3. C.O.Bennett, J.E.Myers, “Momentum, Heat & Mass Transfer”, 3rd Edn., McGraw Hill Book Company.
CT0126 CHEMICAL REACTION ENGINEERING-I
L: 4 T: 1 Cr: 4 TM: 100
OBJECTIVE
This subject gives a knowledge on the kinetics of chemical reaction , design, choice of reactors for single and multiple reactions.
UNIT – I REACTION KINETICS Chemical kinetics, Rate of Chemical Reaction & its representation, Concentration &
Temperature dependent term of rate equation , Searching for a mechanism, Rate controlling step, Interpretation of Batch Reactor data.
UNIT – II REACTOR DESIGN
Chemical Reactors, Ideal Reactors-Batch Reactor, PFR, MFR, Space time, Space velocity, Graphical representation of performance equations, Holding time & Space time for flow reactors.
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UNIT – III CHOICE OF REACTORS Factors affecting choice, optimum yield and conversion, selectivity, reactivity and yield problems, consecutive, parallel and mixed reactions. UNIT – IV DESIGN OF REACTOR FOR SINGLE REACTIONS
Size comparison of single reactors, Batch Reactor with PFR, Comparison of MFR & PFR, Graphical representations, recycle reactor, Auto catalytic reactions, Optimum recycle operations.
UNIT – V DESIGN OF REACTOR FOR MULTIPLE REACTIONS
Reactions in parallel, Reactions in Series, Qualitative discussion about product distribution.
TEXT BOOKS
1. O.Levenspiel, "Chemical Reaction Engineering", 3rd Edn., John Wiley,Singapore, W.S.E. 2. J.M. Smith, "Chemical Engineering Kinetics", 2nd Edn., McGraw Hill, New York. 3. D.Dawande, “Principles of Reaction Engineering”, 1st Edn., Central Techno Publications,
2001.
REFERENCE BOOKS
1. W. Fogler “Chemical Reaction Engineering” ,3rd Edn., Prentice Hall of India, New Delhi. 2. K.A.Gavanhe,“Chemical Reaction Engineering I”, Niralhi Publications.
CTS126 NATURAL GAS ENGINEERING
L: 4 Cr: 4 TM:100 OBJECTIVE
This subject focuses the students to understand the Properties, Estimation, xploration and Treatment of Natural Gas.
UNIT I PROPERTIES AND COMPOSITION OF NATURAL GAS Thermodynamics properties, Compressibility factor and chart for Natural gas, Heating value and flammability limit of Natural gas, Composition of Natural gas
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UNIT II
ESTIMATION AND PRODUCTION OF NATURAL GAS Estimation of gas Reserve by Volumetric Method, Production –Pressure Decline Method, Problems in the Production of Natural gas
UNTI-III
GAS FROM CONDENSATE OIL FIELDS Processing of Condensate well fluid, Cyclic of gas condensate reservoirs, Sweep Patterns, Katy cyclic plant
UNIT -IV
FIELD SEPARATION AND OIL ABSORPTION PROCESS OF NATURAL GAS Field Separation, Separation of Condensate fluids, Expansion Refrigeration system with desiccant, Flow Diagram for Absorption and stripping of Natural gas
UNIT –V
FRACTIONAL DISTILLATION, DEHYDRATION AND SWEETING OF NATURAL GAS Flow diagram of Rich Oil Deethanizer and gasoline plant, Dehydration of Natural Gas using Glycol, Sweating of Natural Gas by Amine Treatment Process.
TEXT BOOKS
1. Katz and Lee “ Hand Book of Natural Gas Engineering” McGraw Hill, New York 1968 2. Nelson W.L. “Petroleum Refinery Engineering”,4th Edition ,McGraw-Hill Book Company Inc,
New York,1958
REFERENCE BOOKS
1. Donald L.Katz and Robert L.Lee, Natural Gas Engineering, McGraw Hill, New York 1990 2. Dring, M. M. – The Natural Gas Industry – A review of World Resources and Industrial
Applications, Butterworth, London, 1974. 3. Speight, J. G. Fuel Science and Technology Handbook, Marcel Decker Inc. 1990.
CTS136 PETROCHEMICAL TECHNOLOGY-I L: 4 T: 0 Cr: 4 TM: 100 OBJECTIVE
To Make The Students Understand The Importance Of Petrochemical Industry And Various Unit Processes Involved In Manufacture Of Petrochemicals.
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UNIT-I IMPORTANCE AND GROWTH
Overview of Petrochemical Industry. The Growth Area of India, Economics, Feedstock Selections for Petrochemicals, Brief Introduction of Petrochemicals from Acetylene, Ethylene, Propylene, Naphthalene and BTX.
UNIT-II SOURCE OF PETROCHEMICALS
Steam Cracking Of Gas and Naphtha to Produce Olefins, Diolefins and Production of Acetylene, Cracker Product Separation, BTX Separation.
UNIT-III SYNTHESIS GAS PRODUCTION
Steam Reforming of Natural Gas, Naphtha and Heavy Distillate to Produce Hydrogen and Synthesis Gas, Production of Methanol, Oxo Process.
UNIT-IV PETROCHEMICALS FROM C2 AND C3
Alternate Routes with Flow Diagram for Production of Ethylene Oxide, Ethylene Glycol, Vinyl Chloride, Glycerol. Epichlorohydrin, Acrylonitrile and Caprolactum.
UNIT-V PETROCHEMICALS FROM AROMATICS:
Alternate Routes with Flow Diagram for Production of Phenol, Styrene, Pthalic Anhydride, Malic Anhydride, Aniline, Benzoic Acid, Cumene, Terepthalic Acid And DMT.
TEXT BOOKS
1. B.K.Bhaskara Rao, “A Text On Petrochemicals”, Khanna Publishers, New Delhi,2000. 2. Sukumar Maiti, “Introduction To Petrochemicals”, 2nd Edn., Oxford & IBH Publishers, New
Delhi,2002. REFERENCE BOOKS
1. Austin.G.T., “Shereve’s Chemical Process Industries” 5th Edn, Mcgraw Hill, 1984. 2. Pandey G.N, “Text Book of Chemical Technology” Vol.II, Vikas Publishing Company, 1997. 3. Gopal Rao.M And M.Sitting, “Dryden,S Outline Of Chemical Technology”, 3rd Edn, Affiliated
East West Press, 1997.
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EN0056 GENERAL PROFICIENCY-IV L: 0 T: 2 Cr: 1 TM: 50 OBJECTIVE
This enables the students how to attend an interview and also gives an idea about the preparation of resumes and other group activities.
UNIT –I
RESUMES Introduction to Resumes; Types of Resumes; Organization of Resume Formats; Presenting Information and Content.
UNIT-II
GROUP DISCUSSIONS/ ACTIVITIES Introduction; Defining Group Discussions; Types of Group Discussions; preparation; Participation; Group Dynamics; Intra/Inter Dept. Group Discussions; Team-work; Negotiation Skills; Introduction to Organizational Behavior; Language lab Practice
UNIT-III
INTERVIEWS Introduction; Honing Verbal and Non-verbal Skills; Rehearsing; Listening Skills; Taking the Interview; Facing Questions; Mock Interviews
UNIT-IV
QUANTITATWE ANALYSIS Aptitude Tests; Psychometric Tests; Puzzles
TEXT BOOKS
1. Prasad, H.M. How to Prepare for Group Discussion and Interview. Tata McGraw-Hill, 2001. 2. Kenendy, Gavin. The Perfect Negotiation. Random House Business Books, l999. 3. A.K.Paliwal, “Communication skills in English”, Surabhi Publications.
REFERENCE BOOKS
1. Career Press Editors. 101 Great Resumes. Jaico Publishing House, 2003. 2. Robins, Stephen. Organizational Behavior. Prentice-Hall, 2003 3. Aggarwal, R.S. A Modern Approach to Verbal & Non-verbal Reasoning. S. Chand&Co., 2004.
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CTP166 CHEMICAL REACTION ENGINEERING LABORATORY
P: 3 Cr: 2 TM: 100 LIST OF EXPERIMENTS
1. Reversible reaction in a batch reactor 2. Irreversible reaction in a batch reactor 3. Plug flow reactor 4. Mixed flow reactor 5. Adiabatic reactor 6. Semi batch reactor 7. Heterogeneous catalytic reactor 8. Biochemical reactor 9. RTD studies
CTP176 MASS TRANSFER LABORATORY-II
P: 3 Cr: 2 TM: 100
1. To determine the critical moisture content and drying rate under atmospheric conditions. 2. To determine the critical moisture content and drying rate under vacuum. 3. To verify Rayleigh equation. 4. To determine the efficiency of Steam distillation. 5. To determine diffusion coefficient. 6. To determine HETP. 7. To optimize the number of leaching stages. 8. To determine the break point for Adsorption. 9. To relate mass transfer coefficient with Reynolds Number.
CTP126 PETROLEUM PRODUCT TESTING LAB-II P: 3 Cr: 2 TM: 100
1. Determination of Aniline Point and Diesel Index. 2. Softening Point of Bitumen by Ring and Ball Method. 3. Ductility of Bitumen. 4. Penetration Number of Bitumen. 5. Drop Point of Greases. 6. Cloud and Pour point Determination. 7. Smoke Point Determination. 8. Copper Corrosion Testing of Petroleum Products. 9. Determination of Sulphur by Lamp method. 10. Coking Tendency of Oil
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11. Saybolt Color of Petroleum Products / Lovibond Tintometer. 12. Water Separability of Petroleum Products. 13. Refractive index of Petroleum Products. 14. Hydrocarbon types in Petroleum Products.
VII SEMESTER
CT0137 PROCESS DYNAMICS AND CONTROL
L: 4 T: 1 Cr: 4 TM: 100
OBJECTIVE This subject deals with the applications of controls in process industry. UNIT –I
FIRST ORDER SYSTEMS Linear open to loop systems - First order and Linear first order systems -Response to various disturbances.
UNIT –II
HIGHER ORDER SYSTEMS First order in series - Higher order systems - Response to various disturbances. UNIT – III
BLOCK DIAGRAM Controls - Block Diagram - closed loop transfer function - Transient response - Simple modes of control and controller characteristics.
UNIT – IV
STABILITY ANALYSES Stability - Routh analysis - Frequency response - Control system design - Controller tuning.
UNIT –V
SPECIAL CONTROLS Cascade - feed forward and ratio control - dead time compensation - Internal Model Control - Control valves - Process identification.
TEXT BOOKS
1. D.P. Coughnowr, “Process Systems Analysis and Control”, 2nd Edn., McGraw Hill, New York, 1991.
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2. C.A. Smith and A.B. Corripio, “Principles and Practice of Automatic Process Control”, 2nd Edn., John Wiley, New York, 1997.
3. George Stephanopoulous, “Chemical Process control”, Prentice Hall of India Pvt. Ltd, New Delhi, 1999.
REFERENCES
1. P. Harriot, “Process Control”, Tata McGraw Hill, New Delhi, 1984. 2. Curtis Johnson, “Process control Instrumentation technology”, 4th Edn., Prentice Hall of India
Pvt. Ltd, New Delhi, 1999. 3. Ray Chaudhuri Uttam, Ray Chaudhuri Utpal, “Process Instrumentation, Dynamics & control
for Chemical Engineers”, Asian Books Pvt Ltd, New Delhi.
CT0147 COMPUTER AIDED PROCESS DESIGN
L: 4 T: 2 Cr: 4 TM: 100 OBJECTIVE
The ultimate aim of this subject is to have a complete knowledge on chemical process plant with the aid of a computer.
UNIT – I
AN OVERVIEW OF VISUAL BASIC Introduction to VB, Adding code and events – Intrinsic VB controls – Working with String and numbers – Using control statements and dialog boxes – Using menus in VB applications
UNIT – II
THERMODYNAMIC PROPERTIES FOR DESIGN Physical properties evaluation, Thermodynamic properties of gases and binary mixtures,
methods of calculations -Vapor-liquid equilibrium data for ideal and non-ideal mixtures. Bubble points and dew points, flash distillation calculation.
UNIT – III
HEAT EXCHANGER AND EVAPORATOR DESIGN Equipment design and Development of software for the following systems: Heat exchange
systems: Double pipe, shell & tube exchangers and Condensers, Evaporator- single and multiple effects
UNIT – IV
COLUMN DESIGN Design of Distillation Columns, Absorption Columns, Liquid – Liquid extraction Systems.
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UNIT – V
PUMPS, FANS AND COMPRESSORS Pumps, Fans and Compressors – Types and its applications – Characteristics - Piping and
pressure drop calculations – Performance analysis of pumps, fans and compressors. TEXT BOOK
1. Bhattacharya and Narayanan “Computer aided design of Chemical Process equipments” New Central Book Agency, Calcutta (1992)
2. Groover & Zimmers, “Computer aided design and manufacturing, CAD/CAM” Prentice Hall of India Pvt. Ltd., New Delhi (1985)
REFERENCE BOOKS
1. M.E. Leeshey, “Computer aided process plant design” Gulf Publishing Co., 2. C.D. Holland, “Fundamentals and modeling of simulation process” Prentice Hall (1975).
CT0157 CHEMICAL REACTION ENGINEERING II
L: 4 T: 1 Cr: 4 TM: 100
OBJECTIVE
This gives the student a clear exposure on Non-ideal reactors, Heterogeneous catalytic and Non-catalytic reactions.
UNIT –I
NON-IDEAL REACTORS Residence time distribution function and its measurement, Characteristics of tracer, Mean
residence time, Conversion in non ideal flow reactors.
UNIT –II
HETROGENEOUS PROCESS AND SOLID CATALYSIS Rate equation for heterogeneous reactions, Nature of catalysis, adsorption isothermal and rates
of adsorption, Desorption and surface reaction analysis of rate equation and rate controlling steps.
UNIT –III
GAS-SOLID CATALYTIC REACTORS Characteristics of catalyzed reactions, Mechanism of solid catalyzed reactions, Pore diffusion
resistance combined with surface kinetics, Performance equations for reactors containing porous catalysts.
60
UNIT –IV
GAS-SOLID NON-CATALYTIC REACTORS Selection of the kinetic model, Progressive-conversion model, Shrinking-core model,
Shrinking-core model for spherical particles of unchanging size, Shrinking-core model for cylindrical particles of unchanging size.
UNIT – V
GAS-LIQUID REACTIONS Various ways of carrying out gas-liquid reactions catalysed by solids, General Rate equation, Resistances in series in the gas-liquid reaction on catalyst surface.
TEXT BOOKS
1. O. Levenspiel, “Chemical Reaction Engineering”, 3rd Edn., Wiley Asian Ed/, New York, 1990.
2. J. M. Smith, “Chemical Engineering Kinetics”, 2nd Edn., McGraw Hill, New York, 1984.
REFERENCE BOOKS 1. Fogler “Elements of Chemical Reaction Engineering”, Ed. 2, Prentice Hall of India, New
Delhi. 2. K.A.Gavanhe, “Chemical Reaction Engineering I”, Niralhi Publications.
CTS147 PETROCHEMICAL TECHNOLOGY-II
L :4 T :0 Cr :4 TM :100
OBJECTIVE
The main objective is to have a wide knowledge on the production methods and the various unit processes involved in the treatment of organics.
UNIT- I
UNIT PROCESSES Fundamental and technological principles involved in Alkylation, Oxidation, Nitration, Chlorination
UNIT –II
UNIT PROCESSES Fundamental and technological principles involved in Sulphonation, Isomerisation, Hydrolysis, Esterfication
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UNIT- III
POLYMERISATION Modes & Techniques, Production of Polyethylene, Polypropylene, Polyacrylonitrile, LDPE, HDPE.
UNIT –IV
POLYMERISATION PRODUCTS Production of polystyrene, Polycarbonate, Polyurethane, SAN, ABS, SBR. UNIT- V
COPOLYMERISATION PRODUCTS Production of, Nylon 6, Nylon 66, PET, Formaldehyde resins. TEXT BOOKS
1. B.K.Bhaskara Rao, “A Text on Petrochemicals”, Khanna Publishers, New Delhi,2000. 2. Sukumar Maiti, “Indroduction to Petrochemicals”, 2nd Edn., Oxford & IBH Publishers, New
Delhi, 2002. 3. Groggins, “Unit Processses in Organic Synthesis”, Edn 5, Tata McGraw Hill. REFERENCE BOOKS
1. Austin.G.T., “ Shreve’s Chemical Process Industries” 5th Edn, McGraw Hill,1984. 2. Pandey G.N, “Text book of Chemical Technology” Vol.II, Vikas Publishing Company, 1997. 3. Gopal Rao.M and M.Sitting, “Dryden’s outline of Chemical Technology”, 3rd End, Affiliated
East West Press, 1997.
CTE1X7 PETROLEUM EXPLORATION AND EXPLOITATION TECHNIQUES L: 4 T: 0 Cr: 4 TM: 100
OBJECTIVE
To study the different techniques involved in petroleum exploration and oil recovery
UNIT –I
PETROLEUM ORIGIN AND MODE OF OCCURRENCE Origin and mode of occurrence of Petroleum,Geological structures favorable to accumulation
of petroleum,Sedimentary environment. UNIT – II
EXPLORATION METHODS Petroleum exploration methods,Well prognosis and economic analysis,Drilling fluids
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UNIT –III
EVALUATION METHODS Geologging, Formation evaluation using wire line logging data, Diagnostic services UNIT –IV
TROUBLE SHOOTING Formation testing practices, Well completion, stimulation and work over operations. Well complication and remedies. UNIT –V
OFF-SHORES TECHNOLOGY Off-shore technology, Enhanced Oil recovery techniques, Documentation and computing method.
TEXT BOOK
1. Bhagwan Sahay “Petroleum exploration and exploitation practices” Allied Publishers Ltd., Chennai, 1994.
2. Richard Dawe, “Modern petroleum Technology”, Vol 1, Upstream, 6th edition, John and wiley sons Ltd, 2000.
REFERENCE BOOK 1. Howard B, Bradley, Editor, “Petroleum Engineering Handbook”, Society of Petroleum
Engineers, Texas, USA, 1987. 2. Nontechnical Guide to Petroleum Geology, Exploration, Drilling and Production, Norman J.
Hyne, Norman J. Ph.d Hyne, 2nd edition, Pennwell Books,2001.
CTP137 PETROCHEMICAL ANALYSIS LAB
P :3 Cr :2 TM :100
1. Sulphur content determination 2. Flue gas Analysis – Orsat Apparatus 3. Aromatic Content determination 4. Hydrogen sulphide content determination 5. Carbon residue determination apparatus (Conradson apparatus) 6. Mercaptan as sulphur estimation apparatus 7. Determination of Lead, Acid, Salt content of crude petroleum products (Dual Extraction
Apparatus) 8. Determination of sediment content of crude oil and fuel oils by extraction with toluene
(Sediment Extraction Apparatus) 9. Determination of Oxidation stability of Gasoline and Aviation fuels (Oxidation Stability
Apparatus) 10. Rust preventing characteristics of lube oil (Standard and Horizontal methods)
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11. Bearing and Grease Noise Characteristics (Grease-Noise Tester) 12. Oil separation from lubricating Grease (Oil Separation Apparatus)
CTP187 PROCESS DYNAMICS AND CONTROL LABORATORY
P: 3 Cr: 2 TM: 100 LIST OF EXPERIMENTS:
1. Analog Simulator
2. Process trainer
3. Solid level measurement
4. Temperature measurement
5. Flapper – Nozzle system
6. Valve characteristics
7. Level control system
8. Purge control
9. Transducer characteristics
10. Manometer dynamics
11. Pressure control system
12. Frequency Response
13. Flow Control
CTP127 MINI PROJECT
VIII SEMESTER
CT0168 SAFETY AND RISK MANAGEMENT IN INDUSTRIES
L: 4 T:0 Cr: 4 TM: 100
OBJECTIVE To create awareness on environmental pollution and safety procedures to be followed in
industries.
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UNIT-I
INDUSTRIAL SAFETY Concepts of Safety. Hazard Classification Chemical, Physical, Mechanical, Ergonomics, Biological and Noise Hazards. Hazards from utilities like air, water, steam.
UNIT-II
HAZARD ANALYSIS Hazard Identification and Control: HAZOP, Job Safety Analysis, Fault Tree Analysis, Event Tree Analysis, Failure Modes and Effect Analysis and Relative Ranking Techniques.
Safety Audit, Safety Survey, Plant Inspection, Past Accident Analysis. UNIT-III
RISK MANAGEMENT: Overall risk analyais –generation of meterological data-ignition data-population data-overall risk contours for different failure scenarios-disastar management plan- emergency planning-onsite&offsite emergency planning-risk management &ISO14000-EMS models-case studies marketing terminal, gas processing complex,refinery.
UNIT-IV
SAFETY PROCEDURES Safety in Plant Design and Layout. Safety Acts and Regulations for Industries. UNIT-V
SAFETY IN HANDLING & STORAGE OF CHEMICALS Safety measures in handling and storage of Chemicals. Fire chemistry and its control. Personal protection. Emergency Preparedness plans.
TEXT BOOKS
1. K.V. Raghavan and A.A Khan, “Methodologies in Hazard Identification and Risk Assessment”, Manual by CLRI, 1990.
2. R.P.Blake,”Industrial Safety”, 1953, Prentice Hall. 3. F.P.Lees,”Loss prevention in Process Industries”,2nd Edition., 996,Butterworth Heinemann.
REFERENCE BOOKS
1. “A Guide to Hazard Operability Studies”, Chemical Industry Safety Council, 1977. 2. Geoff Wells,”Hazard Identification and risk assessment”, I.ChE, UK.
65
CT0178 INDUSTRIAL MANAGEMENT
L: 4 T: 2 Cr: 4 TM: 100 OBJECTIVE To expose the students on various concepts and principles of management and economics. UNIT-I
PERSONNEL MANAGEMENT Principles and functions of Management.Scientific, Administrative and labour management. Industrial Relations. Organization Types: Merits and Demerits.
UNIT-II
TQM : TOOLS AND TCHNIQUES Basic concepts, Benchmarking, Reasons to Bench markings, Benchmarking Processes – Quality Fnctions Dployment, QFD Process, Benefit, Tacuchi Laws fuctions – Total Protective Maintanance conceps and improvements – Various stages of FMVA.
UNIT-III
QUALITY AND ENVIRONMENTAL MANAGEMENT SYSTEMS Benefits of ISO registration – Concepts of ISO 9000 , 14000, 18000 Standards – Documentation and Registration – Internal Quality Audit
UNIT-IV
FEATURES OF ENGINEERING ECONOMICS Micro and Macro Economics. Elasticity of demand and supply. Demand forecasting methods.BEP. Fixed and Variable costs. Cost indices and money value. National income,GNP.Income statement, Balance sheet.
UNIT-V
ECONOMICS OF SELECTING ALTERNATES Amortization, Capital recovery, depreciation, depletion. Economics of selecting alternates. Annual cost method, present worth method, equivalent alternates, rate of return and payout time method. Economic balance.
TEXT BOOKS
1. John.A.Kermath case and David prat”Principles of engineering economics”Ed.4, John-Wiley Publishers, 1997.
2. Arun Monappa, Mirza S.Saiyadain, “Personnel Management”,2nd Edn, Tata McGraw-Hill Publishing Company Ltd, New Delhi.
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3. L.M.Prasad, “Principles of practice of management”, Sultan Chand & Sons, New Delhi. REFERENCE BOOKS
1. Peters and Timmerhaus”Plant design and economics for chemical engineering”McGraw Hill book co.Ed.4 1991
2. K.Shridhara Bhat “TQM” I edition, Himalaya publishing house, 002.
CTE2X8 ELECTIVE II
CTP138 PROJECT MINI AND MAJOR PROJECT P Cr TM Mini Project(CTP127) 3 3 100 Project Work(CTP138) 12 12 300
The project may be considered as the ultimate exercise presented to the final semester student before graduation to measure accumulated engineering knowledge and experience. At the same time, the project itself should provide the students with some new skills and information, and strengthen the acquired knowledge.
The mini and major project may be assigned to a group of two/ three students or individuals. The project topic allotted may be of theoretical, experimental or industrial projects to be carried out under the supervision of a internal and external guides (in case of industrial projects). The same topic may be done as phase-I (mini project) and its continuation work Phase-II as (Major project work) or different topics may be taken as mini and major project work.
Both mini and major projects are to be executed strictly as per the project schedule prepared during VII & VIII semesters. A committee of departmental faculty members comprising the project guide, one faculty member and the Head of Department will monitor and review the progress achieved by the student at various stages. The internal assessment will be done by the committee based on the progress. On completion of the project work, each student has to prepare a project report and submit the same in duplicate to the department. The activities performed during a project may cover one or more of the following;
• Data collection • Critical literature review • Laboratory experience and tests • Mathematical modeling • Software application • Industrial visits • Design and/or assembly • Process analysis
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The mini project will carry a total marks of 100 and 3 credits will be assigned to the mini project work. The internal assessment mark will carry 50 marks and External Assessment will carry 50 marks.
The major project will carry a total mark of 300 and 12 credits will be assigned to the project
work. The internal assessment mark will carry 100 marks and External Assessment will carry 200 marks.
