บทบาท หน้าที่ ห้องปฏิบัติการ ในการสนับสนุนการส่งออกสินค้าเกษตรและอาหารของกรมปศุสัตว์

บทบาท หนาท หองปฏบตการ ในการสนบสนนการสงออกสนคาเกษตรและ

อาหารของกรมปศสตว

19 Julu 2014Sujittra Phongvivat BQCLP DLD @ Maruay Hotel

toBureau of Quality Control of Livestock Products (BQCLP),

Department of Livestock Development

Welcome


3

สำ�นกตรวจสอบคณภ�พสนค�ปศสตว กรมปศสตว

ในก�รสนบสนนด�นคว�มปลอดภยอ�ห�ร บทบ�ท หน�ท

หองปฏบตก�รอ�งองตรวจสอบอ�ห�รของอ�เซยนด�นส�รตกค�งย�สตว ASEAN Food Reference Laboratory for Veterinary Drug Residue (AFRL for VDR)บทบ�ทหน�ท

สำ�นกตรวจสอบคณภ�พสนค�ปศสตว

Sujittra Phongvivat BQCLP DLD @ Maruay Hotel 9 Julu 2014

Bureau of Quality Control of Livestock Products (BQCLP)

4

91 Moo 4 Tiwanon Rd., Bangkadi sub-district, Muang district, Pathumthani province, 12000 Thailand

Tel. +66-2-967-9700 Fax. +66-2-967-9747E-mail address: [email protected]

http://dld.go.th/qcontrol

BQCLP Building 1

BQCLP Building 2


BQCLP: Personnel & Budget

5

Total = 356 positions

49 official (16 veterinary officials ,1 para-veterinary official and 25 scientists, 6 administrators )4 permanent employee, 303 contracted employee (อตร�สวน ข�ร�ชก�ร : พนกง�น�ชก�ร 1 : 6)

Director; 1Expert; 3

Administrator; 6

Veterinary official; 13 Para-veteri-

nary of -ficial; 1

Scientist; 25

Perma-nent em-

ployee; 4

Contracted employee; 303


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50,000,000.00

100,000,000.00

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200,000,000.00

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aht)

2. บทบ�ท หน�ท

6Sujittra Phongvivat BQCLP DLD @ Maruay Hotel 9 Julu 2014

Vision วสยทศน

7

“To be an internationally recognized testing laboratory for safety and quality control of

livestock products”เปนหองปฏบตก�รอ�งองของประเทศ ทไดรบก�ร

ยอมรบในระดบส�กลในด�นก�รตรวจสอบคณภ�พสนค�ปศสตว


Mission พนธกจ

8

Surveillance and monitoring livestock products for food safety control ตรวจตดต�มเฝ�ระวงด�นคว�มปลอดภยอ�ห�รของสนค�ปศสตว Providing technical assistance and training on quality and safety of

livestock products ใหคว�มชวยเหลอด�นวช�ก�ร โดยจดก�รฝกอบรมด�นคณภ�พและคว�มปลอดภยของ

สนค�ปศสตว Performing research & development for food safety and quality testing

methods ทำ�ง�นวจยและพฒน�วธวเคร�ะหด�นคณภ�พและคว�มปลอดภย Strengthening laboratory network capacity with local service laboratory

and collaboration with other outbound laboratories to meet International Standard

สร�งเครอข�ยเสรมศกยภ�พหองปฏบตก�รทใหบรก�รในพนท ใหคว�มรวมมอกบหองปฏบตก�รทงในและนอกประเทศ เพอพฒน�ศกยภ�พหองปฏบตก�รใหเปนทยอมรบต�มม�ตรฐ�นส�กล


Mission พนธกจ

9

As the National Reference Laboratories for quality control testing of animal feed, veterinary medicinal products, hazardous substances and livestock products หองปฏบตก�รอ�งองระดบช�ตในด�น ก�รตรวจสอบควบคมคณภ�พอ�ห�รสตว ผลตภณฑย�สตว วตถอนตร�ย และสนค�ปศสตว

As the ASEAN Food Reference Laboratory for Veterinary Drug Residue หองปฏบตก�รอ�งองก�รวเคร�ะหอ�ห�รของอ�เซยนด�นส�รตกค�งย�สตว


บทบ�ท หน�ท

10

ใหบรก�รก�รตรวจสอบคณภ�พสนค�ปศสตว ด�นคว�มปลอดภยอ�ห�ร กจกรรมต�ง ๆ เชนตรวจ เฝ�ระวงส�รตกค�ง กจกรรมตรวจ

รบรองเพอสงออก เนออน�มย ฯลฯ วธวเคร�ะห (พฒน�วธ, พสจนคว�มใชได, ขอก�รรบรอง ISO/IEC

17025:2005) ฝกอบรม ถ�ยทอดเทคโนโลยก�รตรวจสอบ เพอสร�งเสรม

ศกยภ�พคว�มส�ม�รถหองปฏบตก�ร ก�รดำ�เนนก�รถ�ยโอนภ�รกจ ใหบรก�ร คำ�ปรกษ�แนะนำ� หองปฏบตก�ร ผประกอบก�ร

เกษตรกร


BQCLP Organization Chart

11

1. General Administration Section ฝ�ยบรห�รง�นทวไป

1. Feed Quality Control Laboratory Div. กลมตรวจสอบคณภ�พอ�ห�รสตว

2. Veterinary Drug Assay Divisionกลมตรวจสอบคณภ�พย�สตว

3. Veterinary Public Health Laboratory Div. กลมตรวจสอบคณภ�พเนอสตวและผลผลตจ�กสตว

Bureau of Quality Control

of Livestock Products3. Laboratory Quality System Division กลมพฒน�ระบบคณภ�พ

หองปฏบตก�ร

4. Milk and Milk Products Quality ControlLaboratory Div. กลมตรวจสอบคณภ�พนมและผลตภณฑนม

2. Laboratory Management Division สวนบรห�รง�นจดก�รหองปฏบตก�ร

4. Laboratory Audit Divisionกลมรบรองหองปฏบตก�ร 4 Laboratory

divisions

4 Supporting units

BQCLP

Samples for testing

12

Feed & feed additive

Livestock products

Veterinary medicinal products

Fat


13

BQCLP Testing Activities

Farm, Manufacture of animal feed, port of entry

Farm,slaughterhouse, processing plants, port of entryDairy farm, Milk collecting center

Farmer,DLD Inspector

Authorized personnel/

veterinarian

Feed additives and

Animal feed

Meat & animal products

Milk & Milk products

Samples reception

Sample analysis

Test results

Veterinary drugs,

Hazardous Substances

Farm, Drug stores

DLD Regional officer

(Veterinarian)

DLD Traceability

database

LIMS

Test Reports

Farmer, DLD Inspector

Source of samples Sample collectors(Customer)Test samples BQCLP


14

1. Feed Quality Control Laboratory Division (FQCL)กลมตรวจสอบคณภ�พอ�ห�รสตว

Quality and safety

Monitoring and quality control of feed to fulfill feed quality control acts BE 2525 and additional BE 2542 (1982) and international standard (EU , FDA etc.)

Method development and method validation

Research for feed quality control and feed safety in farm

Setting the standardFeed analysis

• Quality Assurance System• Monitoring Plan

• Inspection and collection for quality control

• Research on public health implications of animal feed

RESPONSIBILITY


15

1. Feed Quality Control Laboratory Division (FQCL) กลมตรวจสอบคณภ�พอ�ห�รสตว

HPLC-UV

Physical inspectionMicroscopeELISACHARM II

LC-MSLC-MS/MS

Screening test

Determination

Confirmation

Analytical method & Instrummentation


16

Test Samples : Raw Materials, Feed, Feed Additives, Premixes, etc.

Physical : Drugs, Vitamins and Minerals Screening test, Ingredient and Adulteration

Chemical : Proximate and Nutrient analysis, Vitamins, Minerals, Urea, Urease activity and Heavy metal

Microbiological : Pathogenic bacteria, Total bacteria and Mould count, Microbiological assay, DNA&GMOs (Real-time PCR) and Probiotics

Toxicology and Biochemistry Mycotoxins : Aflatoxin, Ochratoxin, Zearalenone, Fumonisin and T-2 Toxin, Deoxynivalenol(DON)Hormone, Veterinary Drug andPesticides, PCBs, MelamineDioxin, etc.

1. Feed Quality Control Laboratory Division (FQCL)กลมตรวจสอบคณภ�พอ�ห�รสตว


17

2. Veterinary Drug Assay Division (VDAD) กลมตรวจสอบคณภ�พย�สตว (และวตถอนตร�ย)

RESPONSIBILITY1. Testing samples • Post-marketing veterinary

medicinal products• Hazardous substance

products• Livestock drinking water• Antimicrobial resistant

microorganisms

2. Method development & Method validation

3. Research in related fields


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ANALYTICAL METHODS 1. Veterinary medicinal products• Identification• Assay of active ingredients

colistin/gentamicin/ oxytetracycline/ streptomycin/ tylosin amoxicillin/ enrofloxacin/ doxycycline/ lincomycin/ penicillin/ sulphonamide/ trimethoprim/ tiamulin albendazole/ ivermectin/ chlortetracycline/ clorsulon

• pH• Water content/Loss on

drying[Pharmacopoeia]

2. Hazardous substance products• Assay of Active

ingredients Aldehyde group Quaternary

Ammonium compounds

Hypochlorite as available chlorine

Hydrogen peroxide and Peracetic acid

• Efficiency testing Phenol coefficient/

AOAC used dilution technique

3.Prohibited substances• Determination of

prohibited substances in feed water

Nitrofurans Chloramphenicol Nitroimidazole Beta – agonist


4. Antimicrobial resistance (AMR)• Disk diffusion• MIC• PCR


Annual surveillance of veterinary medicinal products quality

AFVC = Division of Animal Feed and Veterinary Products Control กองควบคมอาหารและยาสตวBQCLP = Bureau of Quality Control of Livestock Products สำานกตรวจสอบคณภาพสนคาปศสตวDLD, MOAC = Department of Livestock Development, Ministry of Agriculture and CooperativeThai FDA, MOPH = Food and Drug Administration, Ministry of Public Health

Veterinary Drug

Supplier / Farm

77 Provincial Livestock

Offices

BQCLP AFVCThai

FDA / MOPH

19


DLD, MOAC


20

3. Veterinary Public Health Laboratory Division (VPHL) กลมตรวจสอบคณภ�พเนอสตวและผลผลตจ�กสตว

RESPONSIBILITY ภ�รกจ

1. Livestock products food safety, quality surveillance and monitoring testing for

•National residue control plan (NRCP)•Microorganisms (e.g. food hygienic indicators, food borne pathogens•Veterinary drug residues, pesticide residues, contaminants, mycotoxins•Food authenticity (e.g. species identification for Halal food)•Others:- dyes

2. As Reference Laboratory (National / ASEAN Food Reference Laboratory)Information center for test method, RM/CRM, expertsTraining centerProficiency Testing Provider (PTP) / Inter-Laboratory comparison (ILC)

3. As a leading laboratory:- Research and development for high efficient and performance test methods


21

3. Hygiene and Food Microbiology

Food hygienic microorganism

Food borne pathogens Microbiological Assay (6-plate test) Porcine DNA by RT-

PCRby conventional culture

method, ELISA and molecular method

2. Veterinary Drug and Hormones Residues

[ASEAN Food Reference Laboratory for Veterinary drug residues]

Screening test by ELISA, Biosensor, HPLC, etc.

Screening and confirmation by LC-MS/MS,

Multi residue screening and confirmation by

LC-QToF

1. Food Chemistry, chemical residues and contaminants

Pesticide residues analyzed by GC-ECD, HPLC-UV, GC-MS/MS, LC-MS/MS

Heavy metal analyzed by AAS, ICP-MS

Aflatoxins by HPLC-FD

Dye e.g. Canthaxantin

VPHL comprises 3 sections of laboratories

3. Veterinary Public Health Laboratory Division (VPHL) กลมตรวจสอบคณภ�พเนอสตวและผลผลตจ�กสตว


4. Milk and Milk Product Quality Control Laboratory (MMPQCL) กลมตรวจสอบคณภ�พนมและผลตภณฑ

Physical

Biological

Chemical

Screening

• Reduction test• pH• Freezing point

• Standard plate count• Lab. Pasteurization count• Coliform

• Milk composition (fat, protein, etc)• Somatic cell

• Antibiotic screening test• ก�รเตมนมผงในนำ�นมดบ -Deoxyketone

22

บทบ�ทหน�ท: ตรวจควบคมมคณภ�พนำ�นมดบ ซงเปนวตถดบ ในก�รผลตนมและผลตภณฑเพอคว�มปลอดภยในก�รบรโภค เพอก�รปรบปรง ตดต�ม เฝ�ระวง คณภ�พนำ�นมระดบฟ�รม ศนยรวบรวมนำ�นมดบ ก�รขนสง เพอใหผลตภณฑนมมคณภ�พด ปลอดภย ส�ม�รถแขงขนได


3. ก�รทดสอบคณภ�พนำ�นมดบ

4. ประเมนคณภ�พ ใหคำ�แนะนำ� เพอปรบปรงใหดขน

2. ศนยรวบรวมนำ�นม

Improve farm management for good quality and

better price 1. Farm

ฟ�รม

23

4. Milk and Milk Product Quality Control Laboratory (MMPQCL) กลมตรวจสอบคณภ�พนมและผลตภณฑ


24

แผนและผลก�รตรวจตวอย�งตอป

LABORATORY

Plan/Results (Samples)2011 2012 2013 2014

VPHL 44,575 / 77,681

39,755 / 56,671

53,799 / 80,358

47,183 /

FQCL 6,786 / 7,557

6,902 / 7,111

8,569 / 8,949

8,600 /

VDAD 1,365 / 1,362

1,654 / 1,496

1,558 / 1,199

1,558 /

MQCL 24,000 / 57,576

52,000 / 55,193

52,000 / 62,997

52,000 /


25

Laboratory

Method development 2011

FQCL 1. Sudan Red I analysis in animal feed by LC-MS/MS

2. Inhibitory in animal feed microbiological assay sensitivity test of 5 reference bacteria with 10 antibiotics

3. Coccidiostat group : Nicarbazin analysis in animal feed by LC-MS/MS

Laboratory

Method validation 2011

FQCL 1. Deoxynivalenol analysis in chicken feed by LC-MS

2. Aflatoxins analysis in corn by Immunoaffinity column / Fluorometry3. Nitroimidazole analysis in animal feed by LC-MS/MS

4. Organochlorinated pesticides and polychlorinated l biphenyls analysis in animal feed by GC-MS/MS

5. Crude fiber analysis in chicken feed

ก�รพฒน�และก�รพสจนคว�มใชไดของวธวเคร�ะห


26

Laboratory

Method validation 2011 (cont)

FQCL 6. Aflatoxins analysis in chicken feed with IAC – post column photochemical reaction by HPLC – Fluorescence detection AFB1, AFB2, AFG1, AFG2

7. Cadmium analysis in corn by ICP-OES

8. Adulterant in corn meal by microscopic analysis

9. Adulterant in soybean meal by microscopic analysis

10. Tetracyclines analysis in animal feed by HPLC: oxytetracycline, chlortetracycline, doxycycline

11. Total mold count by ISO21527 – 2 : 2008 for animal feed ; Total mold count from < 10 to 10n cfu/g



27

Laboratory

Method development 2012

FQCL • Development for the detection enumeration of Enterobacteriaceae in animal feed

• Development and validation of detection protein content in corn, soybean and fish meal by NIRS

• Validation of aflatoxins analysis in cattle feed with IAC-post column photochemical reaction by HPLC-fluorescence detection

• Validation of aflatoxins analysis in chicken feed by immunoaffinity column / fluorometry

• Method validation for determination of cadmium in poultry feed by ICP-OES

• Method validation for determination of carbadox in swine feed by LC-MS/MS

Laboratory research and development


28

Laboratory Method development 2013FQCL • Application of Near Infrared Spectroscopy for determination of

nutrients content in fish meal adulterated with feather meal• Development of the dioxins method in animal feed using high

resolution GC-MS• Method validation for determination of nicarbazin, salinomycin and

narasin in layer chickens feed by LC-MS/MS• Validation of aflatoxins analysis in swine feed with IAC-post column

photochemical reaction by HPLC-fluorescence detection

• Validation of zearalenone analysis in corn by immuno-affinity column / fluorometry

• Validation of aflatoxins analysis in cattle feed by immuno-affinity column / fluorometry

• Method validation for determination of cadmium in soy meal (wet digestion) by ICP-OES

• Validation of enumeration of Enterobacteriaceae in animal feed (ISO 21528-2: 2004)

• Method validation for determination of enrofloxacin in chicken feed by LC-MS/MS

Laboratory research and development


Laboratory

Method development & validation 2011

VDAD2011

• Method development and validation of penicillin G and streptomycin assay in veterinary medicinal products

• Method development and validation of coumatetralyl assay in hazardous substance products for livestock

• Method development and validation for trace analysis of fluoroquinolones in livestock drinking water using LC-MS ion trap

• Method development and validation for trace analysis of Beta-agonists in livestock drinking water using LC-MS ion trap

• Method development and laboratory set-up procedure for testing of hazardous substance products

29



VDAD2012

• Method validation for amitraz determination in hazardous substance products using

HPLC-DAD• Method development for active ingredient assay of hazardous substance

products• Method development and laboratory set-up procedure for testing of hazardous

substance productsVDAD2013

• Method development for phenolic compounds determination in hazardous substances products for livestock using HPLC-DAD

• Method validation for amitraz determination in hazardous substance products for livestock using HPLC-DAD

• Method development and capacity building of hazardous substance products for livestock testing laboratory

Laboratory

Method development & validation 2011

VPHL • Determination of mercury and lead contaminant in animal tissue and liver

2011 • Determination of Aminoglycosides in honey by LC-MS/MS

• Study on application of real-time ultrasound for screening Beta-agonist abused in finishing pigs

30



VPHL2012

• Development method for the determination of 16 PAHs in sausage by GC-MS/MS

• Method development of spinosad in animal fat analysis by HPLC-UVD

• Method development and validation for confirmation of aminoglycosides in pig muscle by LC-MS/MS

VPHL2013

• Method development for confirmation of tetracyclines residues in honey by LC-MS/MS

• Development and method validation for determination of meat contaminations using Real-time PCR

• Validation for confirmatory method for tetracyclines residues in honey by LC-MS/MS

• Method development for confirmation of amitraz residues in honey by GC-MS/MS

31

2. In-house Calibration Laboratory ใหบรก�รก�รสอบเทยบ เครองแกว เครองชง ทใชใน สตส (ISO/IEC 17025:2005 accredited)

1. Laboratory Quality System Section พฒน�ระบบคณภ�พหองปฏบตก�รของ สตส ใหเปนไปต�มขอกำ�หนดทวไปว�ดวยคว�มส�ม�รถของหองปฏบตก�รทดสอบและหองปฏบตก�รสอบเทยบ

(ISO/IEC 17025:2005)

Laboratory quality system development division กลมพฒน�ระบบหองปฏบตก�ร


Laboratory section Testing scope

Food Chemistry, Residues and Contaminants

7

Veterinary Drug and Hormone Residues 6Food Hygiene and Microbiology 15Veterinary Drugs and Hazardous Substances Assay

5

Feed Quality Control 15Calibration 2

Total 50

Laboratory Accreditation (ISO/IEC 17025:2005)


Laboratory Section

Testing Scope (ISO/IEC 17025

Accredited)Type of Sample

Food Chemistry, Residues and Contaminants

- Total Arsenic- Cadmium- Lead- Total Mercury

Liver, MuscleHoney

- Organochlorine Pesticides (OCPs)

Animal fat

ISO/IEC 17025:2005 Accreditation


34

Laboratory Section

Testing Scope(ISO/IEC 17025


Veterinary Drug and Hormone Residues

- Sulfonamides Muscle

- Protein-bound Nitrofurans Metabolites

- Animal tissue and processed animal tissue

- Egg- Honey

- Beta-agonist Brombuterol, Cimaterol,

Cimbuterol, Clenbuterol, Hydroxymethylclenbuterol, Mabuterol, Mapenterol, Ractopamine, Salbutamol and Zilpaterol

- Urine- Muscle- Liver



35

Laboratory Section



Veterinary Drug and Hormone Residues

- Chloramphenicol - Animal tissue

- Egg- Honey- Milk

- Fluoroquinolones; Enrofoxacin and

Ciprofloxacin

- Muscle- Egg

- Tetracyclines; Oxytetracycline, Tetracycline, Chlortetracycline Doxycycline

- Muscle



36

Laboratory Section



Food Hygiene and Microbiology

- Anti-bacterial substances residues

- Clostridium perfringens - Escherichia coli and

Coliform- Enterococcus - Enterococcus (in water and

ice) - Enterobacteriaceae- Listeria monocytogenase- Salmonella spp.- Staphylococcus aureus (BPK)- Staphylococcus aureus (RPF)- Staphylococal enterotoxin- Total bacterial count- Yeast & Mould- Presumptive Determination

of Escherichia coli (Water and Ice)

- Determination of Salmonella spp.

Meat and Meat Products

Laboratory Accreditation


37

Laboratory Section

Testing Scope

(ISO/IEC 17025 Accredited)

Type of Sample

Feed quality control - Aflatoxins in corn- Total Aflatoxins in corn- Adulteration feather meal

in fish meal- Adulteration in soybean

by microscope- Adulteration in corn by

microscope- Determination of

Cadmium in soybean meal

- Determination of Cadmium in corn by ICP-OES

Raw material and animal feed

Laboratory Accreditation


38

Laboratory Section

Testing Scope


Type of Sample

Feed quality control

- Antibiotic inhibitory microbiological assay

- Beta-agonist in complete feed for swine

- Fiber in poultry feed- Protein in poultry feed- Salmonella spp. in feed

and animal feeding stuffs- Tetracycline,

Oxytetracycline Chlotetracycline, Doxycycline in poultry feed

- Total plate count in feed and animal feeding stuffs

Raw material and animal feed



39

Laboratory Section

Testing Scope


Type of Sample

Veterinary Drugs and Hazardous Substances Assay

- Quality assay of enrofloxacin drug using HPLC

- Determination of Beta-agonist drug in livestock water using LC-MS iontrap

- Tylosin

- pH

- Use dilution

Veterinary medicinal productsLivestock drinking

water

Injectable Solution

Veterinary medicinal

Disinfectant



หองปฏบตก�รเอกชนทผ�นเกณฑก�รประเมนและไดรบมอบก�ร ถ�ยโอนภ�รกจแลว จำ�นวน 47 หองปฏบตก�ร

ป พ.ศ. 2554 จำ�นวน 26 หองปฏบตก�ร ป พ.ศ. 2555 จำ�นวน 12 หองปฏบตก�ร ป พ.ศ. 2556 จำ�นวน 9 หองปฏบตก�รTotal 47 laboratories

กลมรบรองหองปฏบตก�รก�รดำ�เนนก�รถ�ยโอนภ�รกจ ต�มมตครม 11 พ.ค. 2553


43

• AFRLs network was initiated at the Workshop and Expert Consultation on “Strategies for Strengthening Food Testing in ASEAN”

In Jakarta, Indonesia on 7 – 11 June 2004 under the EC- ASEAN Economic cooperation Programme on Standards, Quality and Conformity Assessment.

• Veterinary Public Health Lab was selected and assigned as AFRL for Veterinary Drug Residues since then.

ASEAN Food Reference Laboratory for Veterinary Drug Residues Since 2004

International Activities


44

AFRL for VDR activities

Provide training & technical advice & services to ASEAN Member Countries (AMCs)

Become resource & information center i.e. test method for vet drug residues, experts, Certified Reference Materials/ Reference Materials (CRM/RM)

Coordinate inter-laboratory comparisons or proficiency testing scheme for veterinary drug residues

Strengthening laboratory cooperation network for consumer protection



45

BQCLP :- VDAD – AHRI (Taiwan) Building Capacity of Veterinary Drugs Testing Laboratory between Thailand and Taiwan (R.O.C) Since 2011 (study visit)

18 - 22 September 2012 3 person

22 - 26 July 20132 person

9 - 15 May 2011 2 person



BQCLP staff participation in international committee

CODEX Committee of Food Contaminants

CODEX Committee of Food Hygiene (CCFH)

CODEX Committee on Residue of Veterinary Drugs in Food (CCRVDF)

CODEX Committee on Method of Analysis and Sampling (CCMAS)

CCFH Physical Working Group on Revision of the Principles for the Establishment and Application of Microbiological Criteria for Foods

ISO Technical Committee for Microbiology : ISO/TC 34/SC9 Meeting

34/SC9 MeetingISO Technical Committee for Horizontal Methods for Molecular Biomarker Analysis : ISO/TC 34/SC16 MeetingSujittra Phongvivat BQCLP DLD @

Maruay Hotel 469 Julu 2014

47

BQCLP as a learning organization (LO) through knowledge management (KM):-

BQCLP encourages our staff to continually self studying and to improve their working performances:-By - Internet accessible - Library - Internal broadcasting - In house training - Attending seminar, conference &

workshop by close collaboration/ communication through

- Coffee time open discussion - Knowledge/best practice sharing

through - Community of Practitioner (CoP), KM

forum by production of work manual/SOP to be followed for highest quality of work.

BQCLP as a Learning Organization


4. Laboratory plan: 2014-2018


1. Extending scope of accredited method

49

Plan / Year 2014 2015 2016 2017 2018FQCL 1. Testing method in animal feed 3 scopes 3 scopes VDAD 1. Testing method in VD & HS & feed water 3 scopes 2 scopes VPHL 1. Pesticide residues in animal fat 2 scopes

2. Nitrofuran metabolites residue (Total residues) in egg and honey using LC-MS/MS

1 scope

3. Sulfonamides residue in honey using LC-MS/MS 1 scope

4. Avermectin using HPLC-FD 1 scope

5. Campylobacter in food 1 scope 6. Testing method for veterinary drug residues in meat

and meat product 1 scope 1 scope

MMPQC 1. Aerobic plate count in milk (raw and processed) 1 scope 2. Coliform in milk (raw and processed) 1 scope 3. Testing method in milk (raw and processed) 3 scopes


2. Method development and validation

50

Plan / Year 2014 2015 2016 2017 2018FQCL 1. Dioxin in meat and bone meal / (MD) 2. GMOs in meat and bone meal / (MD) 3. Species identification in meat and bone meal / (MD) 4. Color additive in animal feed / (MD) 5. Testing method for heavy metals and veterinary drugs

in animal feed / (MD)

6. Molecular method development for DNA base sequencing using MALDI-TOF MS

/ (MD)

7. Testing method development for heavy metals and mineral using ICP-MS

/ (MD)

VDAD 1. Veterinary drugs & Hazardous substance products 2 (MD/MV) 2 (MD/MV) 2 (MD/MV) 2 (MD/MV) 2 (MD/MV)

2. Hazardous substances laboratory development 4 items 4 items 4 items 4 items 4 itemsVPHL 1. Arsenic speciation analysis in food of animal origin by

ICP-MS1 (MD) 1 (MV)

2. Veterinary drug residue by LC-MS/MS and LC-QToF

1 (MD/MV) 1 (MD/MV)


3. Laboratory facilities development

51

Plan / Year 2014 2015 2016 2017 2018FQCL 1. Bio-molecular laboratory for animal feed testing / 2. Rapid alert and monitoring system development for animal feed

safety /

3. Sample preparation for inter-laboratory comparison of contamination of veterinary drugs, mycotoxins and heavy metals in animal feed

/

4. Reference animal feed quality testing laboratory (i.e. adulteration, mycotoxins, nutrition enrichment (protein, fat, fiber, moisture, etc.))

/

5. Training center for analysis of contaminant in animal feed and corrective action for feed quality control of Thailand

/

VDAD 1. Monitoring and surveillance project for antimicrobial resistant

microorganism in livestock products/ (pilot) / / / /

VPHL 1. PT scheme for veterinary drug residues (round/year) 1 1 2 2 2 2. Microbiological assay interlaboratory comparison (round/year) 1 1 1 1 1

MMPQC 1. Ring test for milk and milk products quality control laboratory

(round/year)4 4 4 4 4


4. Training course

52

Plan / Year 2014 2015 2016 2017 2018VDAD 1. Pharmaceutical analysis workshop 1 1 1 1 1 2. Antimicrobial resistant (AMR) workshop 1 1 VPHL 1. Hygiene and food microbiological training course 1 1 1 1 1 2. Veterinary drug residue analysis/ AFRL veterinary drug

residue workshop1 1 1

MMPQC 1. Milk and milk products quality testing course 1 1 1 1 1


5. Capacity building project & Testing service

53

Plan / Year 2014 2015 2016 2017 2018VDAD 1. Capacity Development of Veterinary Drugs Testing

Laboratory between Thailand and Taiwan (R.O.C) /

2. Capacity Building for Testing of Hazardous Substances in Livestock Production Testing Laboratory under TCPF with FAO

/ /

3. Plan to propose for twinning laboratory project (Veterinary medicinal products) with OIE Collaborating Center (France)

/

4. Project Proposal Application for Enhancing National Capacities for Antimicrobial Resistance Risk Management in Food Animal Production in Thailand with FAO (ongoing)

/


Plan / Year 2014 2015 2016 2017 2018VDAD

Efficiency of disinfectant by Use-dilution /

T h a n k y o u


Documents

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