(2 ) Muestreo de Liquidos

8/18/2019 (2 ) Muestreo de Liquidos

1/5

REFINERIA ORO NEGROPROCEDIMIENTO OPERATIVO STANDAR

Documento No.RON-LAB-POS-002Revii!n No. " 0Fec#$ "%&-Se't.0(

M)ESTREO DE LI*)IDOS + DERIVADOSASTM D-&0,(

CONTENIDO

1.0ALCANCE DE LA NORMA

2.0SIGNIFICADO Y USO

3.0SUMARIO DEL METODO

4.0PROCEDIMIENTOS

5.0DEFINICIONES

6.0INSTRUCCIONES GENERALES

INDICE DE REVISIONES

Rev.

Fec#$ A'o$/o Po Deci'ci!n 1o o3$ A4ect$/$

0 14-Sept.-07

SER E!"!#$ P%e&!!$'%

%.0 ALCANCE DE LA NORMA.


2/5




E"t'" p%'(t!(' ()*%e e& p%+(e,!!e$t+ '$)'& p'%' +*te$e% )e"t%'"

%ep%e"e$t't!'" ,e pet%#&e+" ,e%!',+"/ + ,e &)!,+"/ "e! - &)!,+"/ + e"t',+

"#&!,+ ()'$,+ &' p%e"!#$ ,e 'p+% e$ (+$,!(!+$e" ,e '*!e$te "e' e$+% ' 14.7

PSI.

2.0 SIGNIFICADO + )SO.

Me(&'" %ep%e"e$t't!'" ,e pet%#&e+ p%+,)(t+" ,e pet%#&e+ "+$ %e)e%!,'" p'%' &'

,ete%!$'(!#$ )!(' p%+p!e,',e" "!('".

E& +*et!+ ,e e"t' t($!(' e" +*te$e% )e"t%'" &+ '" %ep%e"e$t't!'" p+"!*&e".

Re)e%!!e$t+" C+$,!(!+$e" p'%' &' Ap&!('(!#$ ,e M)e"t%'" M'$)'&e"

L'" 'p&!('(!+$e" ,e "te t+,+ e$ )e"t%'" &)!,'" (+$te$!e$,+ (+p+$e$te"

pe"',+" (++ ')'/ e"t' t!e$e te$,e$(!' ' "ep'%'%"e ,e &+" ,e8" (+p+$e$te".

E"te t+,+ t%'t' &'" (+$,!(!+$e" 'p%+p!','" p'%' &' e9t%'((!#$ ,e )e"t%'".

1. De'% %ep+"'% "):(!e$te t!ep+ (++ p'%' )e e& (+p+$e$te pe"',+ "e "ep'%e ,e&

p%+,)(t+ )e ,e"e'+" e9t%'e%.

2. E" $e(e"'%!+ e,!% &+" $!e&e" ,e (+p+$e$te" pe"',+" ;')'< p'%' )e"t%e'%

',e()','e$te e& p%+,)(t+ e$ ()e"t!#$.

3. C)'$,+ )$+ + '" ,e "t'" (+$,!(!+$e" ,e &' )e"t%' $+ "e ()p&e "e '(+$"e' $+

)e"t%e'% '$)'&e$te/ e$ e"e ('"+ "e ep&e'%' )$ t+' )e"t%' ')t+8t!(+.

5.0 S)MARIO DEL METODO

E"t' t($!(' p%+ee e& p%+(e,!!e$t+ p'%' &' +*te$(!#$ ,e )e"t%'" '$)'&e" (+$

e& +*et!+ ,e +*te$e% )e"t%'" %ep%e"e$t't!'" ,e pet%#&e+" ,e%!',+"/ + ,e

&)!,+"/ "e! - &)!,+"/ + e"t',+ "#&!,+ ,e )e"t%'" e$ t'$)e"/ ,)(t+"/

+pe%'(!+$e" ,e ,e"('%'/ et(.

E"t'" (+$,!(!+$e" !$(&)e$ e& e$"'+ ,e '$8&!"!"/ &+" t!p+" ,e )e"t%'" (+$te$!,'"

)"'$,+ &'" !$"t%)((!+$e" %e)e%!,'" p+% &'" )e"t%'" ,e 'te%!'&e" e"pe(!'&e".

&.0 PROCEDIMIENTO"


3/5




1. L'" t+'" ,e )e"t%'" '(+$,!(!+$'!e$t+ ,e &'" !"'" "e &&e'%'$ ' ('*+ ,e

'()e%,+ ' &'" ('%'(te%"t!('" ,e &'" !"'" t!p+" ,e e$"'+" )e "e )!e%'$

p%'(t!('%

2. M)e"t%'" ,e T'$)e "e e9t%'e%8$ )e"t%'" ,e ,!e%e$te" '&t)%'" '(+%,e '& $!e&

,e p%+,)(t+ ' )e"t%e'% e$ e& t'$)e/ "! e& t'$)e "e e$()e$t%' (+$ )$ +&)e$

'+% ' &' !t', "e e9t%'e%8$ t%e" )e"t%'" )$' ' 0.50 et%+" ,e &' ")pe%:(!e/

+t%' )e"t%' ' 0.50 et%+" ,e& +$,+ &' =&t!' "e t+'%' ,e& e,!+ ,e& t'$)e.

3. L'" )e"t%'" ,e $'t'"/ '"+&!$'"/ (+$,e$"',+" ()' T>R ")pe%e &+" ? PSI )$'

e e9t%','" "e '(+$,!(!+$'%'$ e$ )$' (+$"e%',+%' (+$te$!e$,+ @!e&+ p'%'

e!t'% &' p%,!,' ,e 'te%!'&e" &!!'$+". E& %e"t+ ,e &'" )e"t%'" ()' p%e"!#$ ,e

'p+% "e' e$+% ' ? PSI "e%8$ '$te$!,'" ' tepe%'t)%' '*!e$te + ,e

'()e%,+ ' &+" e$"'+" )e "e '$ ' %e'&!'% ,+$,e "e e"pe(!:(' &' tepe%'t)%'

,e &' )e"t%'/ "'&+ ')e&&'" ,e &'" )e "e "+"pe(@' )e e"t8$ (+$t'!$','"

(+$ 'te%!'& +&8t!&.

4. M)e"t%'" ,e M'$!+)&, + D)(t+" p'%' &' (+$"e%'(!#$ ,e )e"t%'" "e "!)e &+"

!"+" p'"+" '$te" e$(!+$',+". P'%' e9t%'e% "e ,e*e p%+(e,e% ' '*%!% &'

8&)&'/ p)%'$,+ @'"t' )e "e (+$"!,e%e )e &' )e"t%' e" %ep%e"e$t't!'/

&)e+ e$)''% e& %'"(+ p+% &+ e$+" ,+" e(e"/ (+e$'% ' %e(!*!% &' )e"t%'

t%'t'$,+ ,e $+ p%+,)(!% t)%*)&e$(!' p'%' e!t'% &'" pe%,!,'" ,e &!!'$+". L'

('e%' p+% ,+$,e "'&e &' )e"t%' ,e*e "e% ,e 1B4 ,e p)&',' ,e*e e"t'%

!$t%+,)(!,+ e$ &' *+te&&' ' )$' '&t)%' ,e 1B2 p)&',' ,e& +$,+.

5. L'" )e"t%'" )$' e e9t%','" "e %+t)&'%'$ (+%%e(t'e$te )$' e )e

&&e)e$ '& &'*+%'t+%!+ "e%8$ '"e$t','" e$ &' p&'$!&&' ,e %e(ep(!#$ ,e )e"t%'"

,+$,e "e !$,!('%' &)'%/ e(@'/ @+%'/ t!p+ ,e )e"t%'/ )e"t%e',+% t!p+" ,e

'$8&!"!" ' %e'&!'%.

6. L'" )e"t%'" '$'&!','" "e%8$ !$+%','" e,!'$te p&'$!&&'" ,e ('&()&+ E9(e& '&

pe%"+$'& ")pe%!+% e$('%',+ ,e& 8%e'/ ,+$,e :)%' e& $+*%e ,e& '$'&!"t'.

7. L'" )e"t%'" "e%8$ )'%,',' p+% )$ &'p"+ $+ '+% ' 30 ,'"/ ,epe$,!e$,+

"t'" ,e &' e"t'*!&!,', ' &' +9!,'(!#$ )e p+"e'$.


4/5




,.0 DEFINICIONES

'< Muet$ Me/i$.- U$' )e"t%' e,!' "e t+'%8 ,e '$e%' )e (+$te$'

p'%te" ,e t+,'" &'" "e((!+$e" ,e& ,ep#"!t+ + ,e& t)*+ p%+p+%(!+$'&e$te '&

+&)e$ ,e (',' p'%te.

*< Muet$ coi/$.- E" &' +*te$!,' ")e%!e$,+ )$ &',%#$ t'p',+ @'"t' )$ p)$t+

&+ '" p+"!*&e '& $!e& ,e ,e"('%'/ ,e"t'p8$,+&+ ")*!e$,+ (+$ )$' e&+(!,',

t'& )e ()'$,+ "e "'(' e"te ('"!/ pe%+ $+ (+p&et'e$te &&e$+.

(< Muet$ /e u'e6cie.- Se t+' e$ p)$t+ "!t)',+ ' )$ 10 ,e &' '&t)%' ,e &'

"e((!#$ t%'$"e%"'& + ' )$ + ' )$ 10 ,e& ,!8et%+ ,e )$ t'$)e (!&$,%!(+

@+%!+$t'&/ p+% ,e*'+ ,e &' ")pe%:(!e ,e& &)!,+.

,< Muet$ /e7 me/io.- "e t+' ' &' !t', ,e &' '&t)%' t'$)e.

e< Muet$ /e7 Fon/o.- Se t+' &' )e"t%' e$ )$ p)$t+ "!t)',+ ' )$ 10 ,e &'

'&t)%' ,e &' "e((!#$ t%'$"e%"'& + ' )$ 10 ,e& ,!8et%+ ,e )$ t'$)e (!&$,%!(+

@+%!+$t'&/ "+*%e e& +$,+ ,e& ,ep#"!t+.

< Muet$ continu$.- E" &' +*te$!,' ,e )$ t)*+ )e &&e' e& p%+,)(t+/ ,e

'$e%' t'& )e , e$ t+,+ +e$t+ )$ p%+e,!+ %ep%e"e$t't!+ ,e t+,'" &'"

"e((!+$e" e&+(!,',e" ,e &' (+%%!e$te ,)%'$te e& pe%+,+ ,e p'"'e.

< Muet$ /e me8c7$.- E" &' +*te$!,' e(&'$,+ + '!t'$,+ )e%tee$te e&

(+$te$!,+ ,e& %e(!p!e$te +%!!$'& e%t!e$,+ + e9t%'e$,+ &' ('$t!,', ,e"e','.

@< Muet$ L$/!n.- E" &' +*te$!,' e,!'$te )$ t)*+ p'%' )e"t%'" ,e",e )$

p)$t+ e"pe(:(+.

!< Muet$ /e 'u9$.- E" &' +*te$!,' '*%!e$,+ &' 8&)&' ,e ,e"('%' "'('$,+

)$' p+%(!#$ (+$e$!e$te ,e 'te%!'&.

< Muet$ /e $eno.- E" &' +*te$!,' %e(+!e$,+ &'" p'%t()&'" ,e"p%e$,!,'"

pe%+%'$,+ (+$ )$ *'%%e$+ ,e",e &' ")pe%:(!e (+$te$!,+ e$ )$ *'%%!&/ (''/ *+&"'

+ t+%t'.

< Muet$ /e !7i/o.- Se +*t!e$e %e(+!e$,+ p+%(!+$e" %ep%e"e$t't!'" ,e

"#&!,+" ,e"e$)',+" e$ ('$t!,',e" !)'& ,e (',' p'%te/ e$'"e + ('%'e$t+/

"):(!e$te p'%' te$e% ,'t+" %ep%e"e$t't!+" ,e &+" t''+" (+p+$e$te".


5/5




:.0 INTR)CCIONES GENERALES

'< M)e"t%'" O:(!'&e".- L'" )e"t%'" +:(!'&e" "e%8$ t+','" p+%/ + *'+ (+$t%+& ,e

)$' pe%"+$' ,e *)e$ (%!te%!+/ ()!,',+"' e9pe%!e$t',' e$ &' t+' ,e

)e"t%'".

*< M)e"t%'" ,e C+$t%+&.- S! @' '&)$' %'#$ ")"t'$(!'& )e !$,!)e )e )$'

)e"t%' + "e%!e ,e )e"t%'" p)e,e "e% $+ %ep%e"e$t't!'/ "e t+'%8 +t%'

)e"t%' + "e%!e ,e )e"t%'".

(< C)!,',+".- Se te$,%8 ()!,',+ 89!+ e$ &' t+' ,e )e"t%'" ,e p%+,)(t+"

%e:$',+"/ "+*%e &+" )e "e %e'&!' (+$t%+& ,e ('&!,',.

P'%' t+,+" &+" p%+,)(t+" "e t+'%8$ p%e(')(!+$e" p'%' '"e)%'% )e &+"

'p'%'t+"/ %e(!p!e$te" $+ e"t$ (+$t'!$',+" (+$ p%+,)(t+" $+ %ep%e"e$t't!+".

E& +pe%',+% e$('%',+ ,e &' t+' ,e )e"t%' te$,%8 ")" '$+" &!p!'" &!*%e"

,e t+,+ 'te%!'& ;"'&+ e& ,e &' )e"t%' e9t%','

Documents

(2 ) Muestreo de Liquidos