Quotation for laboratory analytical service in 2016 · 2018. 10. 2. · (Zircon and other coarse minerals) sample 300 7 Individual mineral sample target made (Uranium mineral ) sample

核工业北京地质研究院分析测试研究所 Analytical Laboratory Beijing Research Institute of Uranium Geology

地址(Address)：北京市朝阳区安外小关东里 10 号院（No 10, Anwai Xiao Guan Dongli, Chaoyang District , Beijing 100029）；电话（Tel）:0086-10-64965990;

传真（ F a x） : 0 0 8 6 - 1 0 - 6 4 9 6 5 9 6 0；网址（W e b s i t e）： h t t p : / / w w w, a l b r i u g . c o m ; 电子邮箱（ e - m a i l） : h d f x @ a l b r i u g . c o m

Quotation for laboratory analytical service in 2016

Note to sample delivery

1) The number of samples exception of isotopic analysis and age dating sent to the laboratory less

than 5 will be considered to 5 samples for price;

2 ) Special sample price is negotiable;

3 ) The detailed characteristics of the samples, such as lithology, water (liquid) type, etc should be

described in the sample delivery list.

1、Sample preparation

Type Nr. Service Item Method Unit Price(Yuan) Sample

requirement

Sample

preparation

1 Sample crushing Regular

method sample 30-50 ≤0.074μm，50g

2 Mineral handpicking sample 400

400 Yuan for each

mineral, but

negotiable for

some mineral

purity over 95%.

3 Individual mineral handpicking

(Easy handpicking) g 98


(Normal handpicking) g 292


(difficult handpicking) g 1939

6

Individual mineral sample

target made

(Zircon and other coarse

minerals)

sample 300

7

Individual mineral sample

target made

(Uranium mineral )

sample 500




2、Major and minor element analysis

Type Nr. Service Item Method Price(Yuan)/S

ample

Sample

requirement

Rock，

soil and

sediment

1 SiO2

XRF

59

180-200 mesh，

50g sample，

sum of all items

close to 100%。

2 Al2O3 43

3 Fe2O3 40

4 CaO 40

5 MgO 50

6 K2O 29

7 Na2O 29

8 MnO2 29

9 P2O5 40

10 TiO2 40

11 Cr2O3 43

12 SO3 Carbon sulfur analyzer 59

13 FeO titration 50

14 CO2 Non-aqueous titration 40

15 H2O+ Muffle furnace at 1000℃ 29

16 LOI Muffle furnace at 1000℃ 29

17 H2O- Oven at 105℃ 29




Type Service Item Method Price(Yuan)/Sampl

e

Sample

requirement

Silicate, soil, stream

sediment

Al2O3、CaO、K2O、

MgO、MnO、Na2O、

P2O5、Fe2O3、SiO2、

TiO2，（LOI）、FeO、S

XRF fusion method ;

gravimetric method ;

Titration method

450

180-200 mesh，

50g sample，

sum of all items

close to 100%。

H2O+ gravimetric method 50

H2O- gravimetric method 50

CO2 Titration method 100

TOC Carbon sulfur analyzer 100

F

Alkali fusion , ion

selective electrode

method

100

Cl

Alkali fusion ,ion

selective electrode

method

100


sediment

LOI gravimetric method 50

180-200 mesh，

50g sample

FeO Titration method 50

SiO2、Al2O3、Fe2O3、

MgO、CaO、Na2O、

K2O、MnO、TiO2、

P2O5、Ba、Cr、Ni、

Cu、Sr、Zr

XRF fusion method 200

40 elements in

silicate, soil, stream

sediment

SiO2、Al2O3、Fe2O3、

MgO、CaO、Na2O、

K2O、MnO、TiO2、

P2O5、F、S、Cl、Br、

Co、Ni、Cu、Zn、Pb、

Ga、As、Rb、Sr、Y、

Zr、Nb、Th、U、Ba、

La、Ce、Nd、Ge、Yb、

W、Hf、Sc、Sn、Mo、

Cs

XRF powder pressing

method 240

180-200 mesh，

50g sample




3. Trace element analysis


e

Sample

requirement


sediment

Al2O3、CaO、K2O、

MgO、MnO、Na2O、

P2O5、Fe2O3、SiO2、

TiO2，（LOI）、FeO、S

XRF fusion

method ;gravimetric

method ;Titration

method

450

180-200 mesh，

50g sample，

sum of all items

close to 100%。

Li、Be、Sc、V、Cr、

Co、Ni、Cu、Zn、Ga、

Rb、Sr、Y、Mo、Cd、

In、Sb、Cs、Ba、La、

Ce、Pr、Nd、Sm、Eu、

Gd、Tb、Dy、Ho、Er、

Tm、Yb、Lu、W、Re、

Tl、Pb、Bi、Th、U、

(Ti)、(Mn)

Mixed acid

digestion ICP-MS

260

180-200 mesh，

10g sample.

Ti and Mn is not

included for trace

element analysis

Nb、Ta、Zr、Hf

Alkali fusion or high

pressure digestion

ICP-MS

200

180-200 mesh，

10g sample.

B ICP-MS, ICP-AES 120

U、Th、K ICP-MS, ICP-AES 200

As、Se、Sb、Ge、Re ICP-MS 200

Element speciation ICP-MS Sequential

extraction 200/specie

Sequential

extraction

procedure required.

Ground water,

surface water

（TDS≤0.2%）

Li、Be、Sc、V、Cr、

Co、Ni、Cu、Zn、Ga、

Rb、Sr、Y、Nb、Mo、

Cd、In、Sb、Cs、Ba、

La、Ce、Pr、Nd、Sm、

Eu、Gd、Tb、Dy、Ho、

Er、Tm、Yb、Lu、Ta、

W、Re、Tl、Pb、Bi、

Th、U、Ti、Mn

ICP-MS 200 100mL, nitric acid

acidified to pH




Extraction solution,

leaching solution

containing organic

matter

Trace elements

required by user

Pretreatment

ICP-MS 350

100mL, sample

information should

be provided by user




4、Water analysis

Type Service Item Method Price(Yuan)/

Sample

Sample

requirement

Ground water,

surface water

（TDS≤0.2%

Anion (F-、Cl-、NO3

-、

SO42-

) Ion chromatography 100

500mL, original

water without any

additives

Cation（K+，Na+，Ca2+，

Mg2+）

on chromatography or

ICP-OES 100

HCO3-、CO3

2- pH Titration method 50

High salinity water

(sea water, Saline

Lake water, sewage,

etc.)

Anion (F-、Cl-、NO3

-、

SO42-

) Ion chromatography 150

00mL, original

water without any

additives

Cation（K+，Na+，Ca2+，

Mg2+）

on chromatography or

ICP-OES 150

HCO3-、CO3

2- pH Back titration method 100

Ground water,

surface water

Borate , silicate ICP-MS ICP-AES 100/item 100mL，

Polyethylene plastic

bottle

NH4+、PO4

3- Spectrophotometric

method 100/item

pH、Conductivity 、

Eh pH meter 20/item




5 Individual item and element analysis

Type Service Item Method Price(Yuan)/Sa

mple

Sample

requirement

Rock, soil, sediment

pH DI water leaching pH

meter 50

180-200 mesh

50g

Eh DI water

leaching—Potentiometer 50

△Eh

Potassium dichromate

leaching -potential

subtraction

50

Rock, soil, sediment

Individual element

（As、Hg 、Au、Ag、

Cu、Pb、Zn）

AFS、mercury analyzer、

AAS 100/element

180-200 mesh

50g

U

Time resolved laser

induced fluorescence

spectroscopy

200

180-200 mesh

20g

Ore、mineralized

samples

Individual element

（As、Hg 、Au、Ag、

Cu、Pb、Zn）

AFS、mercury analyzer、

AAS 、Titration method 150/element

180-200 mesh

50g

U Potentiometric titration 300

Th Titration method 300

Uranium Valence

（U4+、U6+）

Time resolved laser

induced fluorescence

spectroscopy (TRLIFS)

400

180-200 mesh

20g




6. Organic and indoor air analysis


mple

Sample

requirement

Rock, soil,

sediment

Gaseous hydrocarbon

（C1-C7）

Acid hydrolysis extraction

-GC0 200

180-200 mesh

200g, cross

contamination

controlled.

Volatile hydrocarbon

（C8-C15） Pyrolysis GC-MS 400

Semi volatile

hydrocarbon

（C16-C30）

Solvent extraction GC-MS 400

Indoor air

Ammonia Spectrophotometric

method 300

After 1 hour

closure, sampling

in field

Benzene GC 300

Formaldehyde Spectrophotometric

method 300

Total volatile organic

compounds （TVOC） GC 300

Radon Radon analyzer 300

After 24 hour

closure, sampling

in field




7、Isotope and isotopic geochronology analysis


mple

Sample

requirement

Individual mineral,

Bulk rock

Rb-Sr isotopes and

isochron ages

Isotope Dilution

TIMS

1400 Bulk rock

180-200 mesh，

2g；individual

mineral sample

weight more

than 0.5g，

lithology and

Rb-Sr、Sm-Nd

preliminary

results needed.

Geological

background of

sampling is

needed.

Sm-Nd isotopes and isochron

ages 1400

Uraninite or

pitchbllende

U-Pb apparent age

1200

Purity more than

95%，10mg

zircon U-Pb age 1200 More than 20

grain

Uranium bearing

rock U-Pb isochron age 1200

180-200 mesh

2g ， U 、 Pb

preliminary

content results;

226Ra results for

sandstone type

samples needed

Quartz fluid

inclusion Rb-Sr isochron age 1600

Quartz，60-80

mesh, 20g

Rock, soil,

sediment, mineral,

water

Sr isotopes（87Sr/86Sr）

TIMS

600 Bulk sample

180-200 mesh，

2g ； individual

mineral sample

weight more

than 0.5g;

lithology of

sample needed.

Nd isotopes

（143Nd/144Nd） 600

Pb isotopes（206Pb/204Pb、207

Pb/204

Pb、208Pb/204Pb） 600

U isotopes（234U、235U、236U、238

U） 600

Lithium products 6Li/7Li ICP-MS

600

Boron products 10B/11B 1500

8. Stable isotope analysis




Type Service Item Method Price(Yuan)/Sample Sample

requirement

Water δD、δ18O

Gas isotopic

ratio mass

spectrometry

600 more than 2mL

carbonate δ13

C、δ18O 300 500mg\200 mesh

Bulk rock of quartz

and silicate δD、δ18O 1200 1g\40-60 mesh

sulfide δ34

S 350 30mg\200 mesh

Sulfate and total S in

bulk sample δ

34S 600

Sulfur

20mg\200 mesh

Plant, animal, nitrate δ15

N 500 100mg\100 mesh

Hydrocarbon

(individual species),

organic carbon

δ13

C 500 200mL

Quartz and bulk

silicate δ

30Si 800 100mg\100 mesh

Mineral inclusion δ13

C 900 10g\60 mesh

Mineral inclusion δD 900 10g\60 mesh

Water δD

900 0.2g\100 mesh

Nitrate in water δ15N 1000 More than 5L

Sulfide, quartz and

other minerals; gas;

groundwater;

He、Ne、Ar、Kr、Xe

isotopic composition

Inert gas mass

spectrometry 2500/项

Mineral 2g/40

mesh、purity more

than 98%

长石、云母、角闪石、

石英、辉绿岩、玄武

岩等

Feldspar, biotite ,

hornblende, quartz,

diabase, basalt, etc.

40Ar/

36Ar age dating

method

Inert gas mass

spectrometry 7000

Mineral 2g/40

mesh、purity more

than 98%

K-Ar age sandstone, mudstone,

Illite in fault mud

Inert gas mass

spectrometry

10000/ sample

（4500/

measurement only）

Including sample

selection, purity

and speciation

analysis, age

measurement.3-5kg

for normal sample。

Fission track age Apatite, zircon, etc.

Fission track

method

3000/sample

Number of pure

mineral particles

per sample more

than 100.




9. Nuclide and radioactivity analysis


requirement

Aerosol and fallout Grossα、Grossβ α、β counting 1000 /item

Drinking water, surface

water, ground water

γ nuclide analysis γ spectrometry 2000

γ nuclide analysis γ spectrometry 2000

1） γ nuclide

analysis、137Cs、90Sr: 40L

water;

2））Grossα、

Grossβ、210Po、210Pb、226Ramore

than 4L water

3）3H analysis

1L water

4）14C: 50L，sent

at the form of

precipitation

（For salt

brine , seawater,

effluent ,

solution

containing heavy

metal, please

contact the

laboratory to

consult testing

method）

Grossα、Grossβ α、βcounting 1000 /item

238U TRLIFS

ICP-MS 200 232Th ICP-MS

40K AAS 100

3H

Low background

liquid

scintillation

1000

14C

CO2 absorption

method , Low

background

liquid

scintillation

1500

210Pb γ spectrometry 1200

210Po αcounting 1200

226Ra Radiochemical

method 300

90Sr βcounting 2000

137Cs Radiochemical

method 1500

α（234U/238U） αspectrometry 300

α（230Th/232Th） αspectrometry 300

Soil, sediment, rock,

biological samples

γnuclide analysis γspectrometry 2000 Soil:180-200

mesh 500g

Biological

sample：20kg

238U、232Th、226Ra、40K γspectrometry 1000

Grossα、Grossβ α、βcounting 1000

90Sr βcounting 2000 Soil、sediment、

rock : 180-200 137Cs Radiochemical 1500




method mesh 50g

Biological

sample：20kg 226Ra

Radiochemical

method 300

210Pb γspectrometry 1200 210Po αcounting 1200

3H

Low background

liquid

scintillation

1200

14C

CO2 absorption

method , Low

background

liquid

scintillation

1500

α（234U/238U） αspectrometry 300 180-200 mesh,

10g α（230Th/232Th） 300

Soil rock (geochemical

exploration)

210Po 150 180-200

mesh ,20g Thermoluminescence 120

Radioactivity of

building materials

Internal and external

exposure index 1000

180-200 mesh,

500g

Construction site Radon in soil 300/point

Field testing Environmental air

X—γ dose rate 150/point

α、β surface

contamination 150/point




10 inclusion analysis


e

Sample

requirement

Fluid inclusion slice Disc Abrasion Slice made 100

Original rock

Fluid inclusion slice of

Fourier infrared

spectrum

Disc Abrasion Slice made 200

Fluid inclusion

Observation and

identification ,GOI

analysis

Optical

microscope 800

composition analysis Laser Raman 360/point &

800/hour

Homogenization

Linkam Thms 600 700

Salinity 400

Composition analysis Fourier infrared

spectrum 540/point

Organic vapor

components

Gas

chromatography 400

Individual

mineral at 60-80

mesh

Inorganic gas composition Gas

chromatography 600

Liquid composition Ion

chromatography 600

Liquid

composition(include

HCO3-)

Ion

chromatography 800

Trace element ICP-MS 600

Magmatic Fluid

inclusions

Homogenization Linkam Ts 1500 2000/point Original rock




11. Micro beam analysis for rock and mineral


requirement

Electron microprobe

analysis (EMPA)

Carbon coating

polished thin

section ：50/piece；

light section

：100/piece

Samples with

EMPA section or

light section

wavelength dispersive

quantitative analysis

100/point（≤10

elements. If extra

elements increased,

5 Yuan for each

increased element; if

detection limit

needing improving

and increasing

measurement time,

considered one extra

element cost）

Energy dispersive

quantitative analysis

80 /point（element

items without

limitation）

Surface analysis 600 /hour

Line analysis 800 /hour

Take photos

Back scattering

image or second

electron image

：100 /photo

Energy spectrum

：80 /photo

X-ray diffraction

(XRD)

Phase analysis 200/sample

Quantitative analysis for

sedimentary rock

200/ sample sedimentary

rock，≥1g

Clay mineral quantitative

analysisf 400/ sample

Sedimentary

rock, the sample

volume of not

less than 30 g,

crushing to

200 mesh




Lattice parameters 200/ sample ≥300mg

Micro zone analysis 800/hour Diameter≥300μ

m

Dolomite sequentiality 200/ sample Dolomite

content ≥50%

Scanning electron

microscope (SEM)

Electron microscope

observation 800/ hour

Cathode luminescence

imaging 50 /photo




12. Physical property measurement


requirement

Rock

Density, natural remanent

magnetism, magnetic susceptibility,

resistivity and polarizability

50 /item，200 元/5items Core or massive

rock

Porosity, specific surface, porosity

and permeability 200/item

Massive rock

and large

granular rock

Sieve

Dry sieve 200 /item、wet

sieve 200/items、Laser

particle size analyzer

50/item

Laser particle

size analyzer is

good for fine

particles

Zeta-potential

relationship of

Isoelectric point, zero

point, pH and

zeta-potential, electric

conductivity，200 /items

Powder

Ore

mineral processing

Leaching test of

uranium ore:

150000/items;

Non-ferrous metal

processing:

150000/items

50kg samples

Ore

Process mineralogy

Process mineralogy

100000/items;

relationship of Process

mineralogy

characteristics and

dressing Smelting:

150000/items

Representative

Massive rock

Others

Cooperative parameter

RoHS, CEtesting,

Mechanical property

testing, Soil sediment

Magnetic measurement,

contact angle, Bulk

density, etc.

Inquiry




13. Analytical instruments available

Instrument Type Method Price(Yuan)/I

nstrument Specifications

Uranium Analyzer MUA

plus

Time resolved

laser induced

fluorescence

spectroscopy

(TRLIFS)

200k

Liner range:0.2-20μg/L;

Detection limit: 0.02μg/L;

Computer controlled.

Radium-Radon

Analyzer PC2100

Emanation

scintillation

method

200k

Detection limit:

3.3×10-14 g 226Ra/g;

Computer controlled.

Documents

Quotation for laboratory analytical service in 2016 · 2018. 10. 2. · (Zircon and other coarse minerals) sample 300 7 Individual mineral sample target made (Uranium mineral ) sample