TSL Solutions K.K.

TSL- OIM-Analysis 4

6-29-8TEL 042-732-5760 FAX 042-732-5251

e-mail : tsl-j@wb3.so-net.ne.jp

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OIM-A4 Map

2-1. Map 2-2. 3.

3-1. Discrete Plot 3-2. 4. (Chart)

4-1. Chart 4-2. Chart 4-3. Chart Excel 5. 6. 7. 8. 9. Map Plot Highlight (Highlight) Partition Properties

10. Map 11. 13. Crop

12. 14. Merger 15.

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0. OIM-Analysis(OIM-A) Version OIM-A OIM-AOIM-A (Map)(Plot) (Chart)

1. OIM-A4 OIM-A4 OIM-A4 1-1 Fig.1-1

Project Tree

1-1OIM A4 3

OIM OIM-A4 () [File] [New] [Open] Prject [New] 1-2 Project Tree Project Project [New] 1-3 [Dataset] Sample Dual Phase Titanium 1-4 1-4 Project All data, Titanium(Alpha), Titanium(Beta) OIM Dual Phase Titanium Data Set Partition All data Partition 1-4Project Tree 1-3 1-2Project

Partition Dataset Partition Partition CI 0.2 Partition Map Chart Plot Partition OIM-A4 OIM-A2.8 Project File(.osc ) (.ang ) OIM-A4 1 Dataset

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2. Map 2-. Partition( All data) 2-1 New Map Map Map 2-2 New Map Map Style Grayscale Color Coded 2 Map Map Map Map [Edit>>] Grayscale Color Coded Map Image Quality Fit Phase Inverse Pole Figure Map Confidence Index Detector Signal EDS (Element map :Option) Crystal Direction 2-2: Map Map 2-1

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Crystal Orientation Unique Grain Color Map Grain Shape Orientation Grain Average IQ Grain Average Fit Kernel Average Misorientation Grain Average Misorientation Taylor factor Elastic Stiffness

Euler Angle RGB Grain Size Grain Shape Aspect Ratio Grain Average CI Grain Average Video Signal Grain Orientation Spread Grain Reference Orientation Deviation Schmidt factor Twin Parent/Daughter

Default Image Quality map [OK] 2-3 Image Quality map (Inverse Pole Figure Map: IPF map) Grayscale [none] Color Coded Inverse Pole Figure [Edit] 2-4 ND ND () RD RD ( 2-4 ) ND [Inversion Symmetry] Grayscale Color Coded 2-5 ND IPF map 2-6 ND (0001) ND 2-4: 2-3: IPF

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2-5: IPF map(ND ) 2-6:

2-2. 2-2 Boundaries Second Partition Type (Type) Rotation Angle Rotation Axis Axis Angle Grain Phase Shape Ellipses Reconstructed Reconstructed Plane trace ()

Plane trace Rotation Angle Rotation Angle [Add] 2-7 Add Boundary 15 180 Segment 2-7: Rotation Angle

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515 2-8 Type Rotation Angle CSL CSL Rotation Angle CSL 2-9 Legend 2-2 Map style Grayscale Color Coded 2-10 2-8 Copy Image 2-9: (Legend) 2-8: IPF

2-10:

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3. Discrete Plot: Texture Plot:

3-1. Discrete Plot Discrete Plot 2-1 Map Discrete Plot 3-1 Discrete Plot (New Discrete Plot)Plot 3-1 3 Second Partition Rodorigues Misorientation Axis/Angle Misorientation 3-1: New Discrete Plot / Plot Plot Type

Partition Titanium(Beta) Discrete Plot 3-1 Plot Type Plot Plot Type Pole Figure: Inverse Pole Figure: Euler Space: Rodorigues Orientations: Rodorigues Misorientations: Axis/Angle Misorientations: (ODF) /

Pole Figure Sections () Default [Add] 3-2 Add Section Titanium(Beta) Phase Titanium(Beta) Pole(Plane) Plane Normal Direction ()

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Crystal Direction map Add Section Plane Normal Direction Crystal Direction map Titanium(Alpha) [OK] (001)(101)(111) 3 3-1 [Enforce Orthotropic Sample Symmetry (Rolled Sheet)] 3-3 Plot Type [Edit] (ODF) 3-2. Intensity() Counter() (Texture ) (Harmonic Series Expansion) (Discrete Binning) ( Default ) 2-1 Texture 3-4 New Texture Phase Titanium(Beta) Partition Texture Titanium(Beta) Harmonic Series Expansion Discrete Binning 3-3: Discrete Plot 3-2: Discrete Plot

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[Add PF]/[Add IPF]/ [Add ODF]/ [Add Fiber] / Inversion Symmetry 3 2 ( EBSP X 3-4: New Texture

(hkl)(-h-k-l)) Discrete Plot (001)/(011)/(111) 3 [Add PF] 1 3-4 [OK] 3-5 Titanium(Beta) Partition Harmonic L-16, HW-5.0 (Harmonic Series Expansion) 16 5 Harmonic L-16, HW-5.0 New Texture Plot 3-6 Texture Plot Properties Plot Style Pole Figure Section Plot Style Plot Type Plot [OK] 3-7 Legend 3-7 Legend Default Log 3-6: New Texture 3-5: New Texture

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3-6 Plot Type [Edit]Pole Figure Pole Figure (Projection) Stereographic Scale 3-8 3 3-8 Scale Level () Auto Generator Settings [Auto Maximum] Off Maximum No. Level 0 Level] Chart Type Chart 4-1 New Chart Type Grain Size Grain Size Chart PointDiameterAreaASTM 4 Point Diameter 4-1: New Chart

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Area ASTM ASTM Area Grain Size (Area) 4-2 Range Method Chart 0 100(%) (Percentage) (Absolute) Chart Partition (Minimum)(Maximum) (Average) Percentage Minimum Maximum 20.0 80.0 4-3: Grain Size 4-2: Grain Size

100 20% 80% Chart Type Minimum/Maximum/Average [Calculate] Parameter 4-3 Parameter (Liner Log)

4-4: Log

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() Log Liner () 4-4 Log 12 Area Fraction Chart Window Legend Number Area Number: Area: ( ) Area () : Chart Default Partition Properties

4-2. Chart Copy Image Chart OIM 4-5: Copy Image Copy Image 4-5 Chart Chart Chart Chart Chart Project Tree

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Partition Chart Open

4-3. Chart Excel Chart Excel Export

5. Map Plot OIM Color Coded Map Plot / 5-1 Map Map Style Color Coded Crystal Direction Edit [Add] Color Gradient (Minimum)(Maximum) Minimum Maximum Crystal Direction Tolerance 0 20 5-1 0 20 10 5-1: Map

[Reverse] Minimum Maximum () Grayscale

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6.

(Highlight) OIM 6-1

6-1: Record Map Plot Map Interactive Clear Highlight MapPlot Chart Tolerance Angle Map Plot ( ) Trace Plane hkl Trace Plane () Map: Point Map Map Interactive Interactive Properties Maps: Tolerance Tolerance Map Maps: Grain Grain Map Partition

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(Properties ) Maps: Boundary Map Map Interactive Maps: Triple Junction Map Map Interactive Maps: Profile Vector Vector Map Misorientation Angle Maps: Crystal Direction Map Maps: Plane Trace Maps: Crystal Lattice Map Plots: Maps: Tolerance Plot Tolerance Plot Plots Misorientation Plot 2 Interactive Highlighting Color Highlighting Gradient Highlight Highlight Highlight

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7.

Highlight Highlight Map Plot(Discrete Plot) Chart(Liner) Chart Map/Plot 7-1 MapPlotChart Chart(Liner) 020m2 6m2 Highlighting color Map Show Highlighting Plot Show Highlighting Chart Map Plot Show Highlighting Highlight Highlight MapPlot(Discrete Plot) Chart(Liner) Map Plot Chart Map Plot Maps: Tolerance Maps: Grain Plots: Tolerance Tolerance Angle

7-1: Highlight

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Highlight 7-2 Map Highlighting -> Partition Non-Highlighted -> Partition Partition New Highlight Partition Dataset Map/Plot/ Chart Partition 7-3 Highlight -> Partition IPF map Phase map 7-2: Highlighting->Partition

Partition Map/Plot/Chart

7-3: Highlight

OIM-Analysis OIM-A4

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8.

Preferences Setting 8-1 Preferences 8-2 Preference 8-1: Preference

Preferences 8-2

8-2: Preference

Status bar text: 1-1 (hkl) (integers) Hough peaks mode: OIM-A4 Hough peak Hough peak Pole Figure Coordinate Setting: RD/TD ND

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Minimum boundary misorientation: OIM-A4 ( ) 1 OIM-A4 Monitor size (viewable diagonal length): OIM-A4 Custom QuickGen Template: OIM-A4 Crystal Direction Map Template Template Maps [ - ] Browse Template 1-1 Project Tree Partition map plot Template Map/Plot/Chart Export Template

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Partition Properties OIM Partition 2-1 Partition Properties 9-1 Partition Properties [Grain Size] 9-2 Partition Grain Tolerance Angle 9-1: Partition Properties

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Minimum Gain Size Grain Tolerance Angle Minimum Confidence Index CI CI -1 4-1 Chart (Twin Boundary) OIM-A4 [Define] 9-3 Tolerance Angle [Add] 60 9-4 Cu 9-3: Partition Properties 9-2: Partition Properties

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: : : 0.3582m2

0.2169m2

0.2840m2

9-4:

9-1 Formula IC Cu OIM 9-5 Cu IPF IPF IQ

SEM Image

IQ ma p

IPF map

9-5: Cu

IQ CI SEM 9-1 IQ IQ OIM IQ 9-1 Formula [Image Quality]

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9-6 (Absolute)(>) OK Partition Properties OK Partition IQ 9-7 IQ 283853 IQ 28 53 Formula Plot 9-6: IQ

IQ>23 IQ>28

IQ>29 IQ>38

IQ>35 IQ>53

9-7: IQ

10. Map Map 10-1 Map Show Highlighting: Show SEM Image: Detector Signal Show OIM Map Detector Signal(Video Signal) SEM SEM 10-1: Map

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Show OIM Map: OIM Show Boundaries: Show Grain IDs: OIM Show Fleixview Labels: Map Flexiview Show Micron Bar: Set Micron Bar Set Micron Bar Length: Fix to Window: Zoon In: Zoom Out: Zoom Off: / / Magnification: 8-2 Apply Colors As Highlighted: Highlight Highlighted -> Partition: Highlight Partition Project Tree Non-Highlighted -> Partition: Highlight Partition Project Tree

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Export Template: Export Data OIM4 Grayscale

Close: Project Tree

Copy Document: Project Tree Partition

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11. OIM-A4.0 RD ND TD OIM-Analysis RD 90 11-1 Dataset (Ni_Sample:) Rotate 11-2 Rotation RD/TD/ND +/- RD 90 Operation Rotate inplace Texture Rotate and add to project as new dataset Project Rotate and export as new data file () 11-1: Dataset

11-2:

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12. OIM 11-1 Dataset Rotate Cleanup 12-1 Cleanup Dataset Cleanup Type Grain Dilation On-Line Help Grain Dilation Grain Tolerance Angle Minimum Grain Size Grain Grain Minimum Grain Size Single Iteration Operation Rotate 12-1

12-2: IPF

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Dataset 12-2 Ni IPF OIM4 Single (Average) Orientation per Grain 13. Crop Cr 11-1 Dataset Cleanup Crop 13-1 Crop Dataset 13-1 13-1Crop Dataset IQ IQ Properties 13-2 13-1 Project Dataset

13-2Crop 14. Merge Merge Merge Step Size 11-1 Dataset Crop Merge

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14-1 Merge Dataset DataSet Select Dataset to merge with: [OK] 14-1Merge

15. OIM-A4.0 File () Map/Chart/Plot DTP Map Map/Chart/Plot Window

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