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SSRL Crystal Mounting System

SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

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Page 1: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

SSRL Crystal Mounting System

Page 2: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

Sample Storage Cassette

Stores 96 samples mounted on standard Hampton pins

NdFeB ring magnet

Teflon washer

Hampton pin

Page 3: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

Sample Storage Cassette

Page 4: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

The Dispensing Dewar

Page 5: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

Vertically Opening Gripper Arms

The Robot and Gripper Arms

Z

U

θ1

θ2

Fingers to HoldDumbell Magnet Tool

Cryo-tong Cavity

Epson ES553 Robot

Page 6: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

How do I transport my cassette?

Mount 3 cassettes at the beam lineup to 288 samples

Ship 2 cassettes inside a Taylor Wharton or MVE dry shipper

Store 20 cassettes inside a Taylor Wharton HC35 storage device

Cassette transfer handle

Page 7: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

Robot Demonstration

Page 8: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

(A) Sample Cassette and Hampton pins

(B) Guide Tool – to aid mounting pins into cassettes

(C) Transfer Handle – for handling cold cassettes

(D) Magnetic Tool – to mount pins in cassette & to test pin size

(E) Dewar Canister – replaces stock canister in dry shipping dewars

(F) Styrofoam Spacer – keeps single cassette in place when shipping

(G) Teflon Ring – to support the canister in the shipping dewar

Styrofoam box holds liquid nitrogen for loading cassettes

How do I put crystals into cassettes?

Page 9: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

How do I put crystals into cassettes?

Page 10: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

Is It Easy to Use?

Page 11: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

Standard Pins → Cross Compatibility

Page 12: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

What pins work with the system?

Page 13: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

How do I get the cassettes and tools?

www.hamptonresearch.com www.QMPmachine.com

Manufacturing directions are available online at smb.slac.stanford.edu/hardware

Page 14: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

Can the robot be used remotely?

Page 15: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

Blu-Ice for beam line control

• Can run locally or remotely.• Multiple copies may run simultaneously.• Security features prevent unsafe actions.

Beam line video system• Monitor sample in beam,

experimental hardware, and crystals under microscope.

• Video streams may be viewed via Blu-Ice or through a web browser.

Archive System

• Back up data to multi-terabyte robot tape system at SDSC over network.

• Simple web interface for data archival and retrieval.

• No need to use backup tapes.Remote Unix desktop

• Fully functional Unix desktop environment.• Blu-Ice and all data processing software may be run remotely.• Free ICA client from Citrix.

Remote Access Requirements:

Page 16: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

Remote Access Requirements:

Sorry - I cannot make it to work today.

1. Reliability 2. Feedback

A collision has occurred!

Ouch!

Page 17: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

How Reliable is the System?

In operation for more than a year JCSG screened > 3000 crystals in < 6 months Capable of mounting 100s of samples without problems

Learn as much as we can from any problems

Page 18: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

What Problems Have Occurred?

Pass

Failures

Pin Tester

Excess glue or grease spilled on pins

Page 19: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

How Reliable is the System?

Routine Preventative CareMaintenance / Inspection Schedules

Feedback for sample and hardware protectionLaser Displacement Sensors

pin on/off the goniometersample position check

Force Sensor collision detectiontoolset calibration checkscassette insertion checks

Page 20: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

Feedback

Sensor

ATI Industrial Automation force/torque sensor

Page 21: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

Automated Calibration

Page 22: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

Speedy Recovery Time

Tongs are easily replacedSpare robot and parts readily availableMenu driven automated recalibrationEasy for all support staff to repair and maintain

Page 23: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

The Macromolecular Crystallography Group

SSRL Director: Keith HodgsonSMB Leader: Britt HedmanMC Leader: Mike Soltis

Günter Wolf, Scott McPhillips, Paul Ellis, Aina Cohen, Jinhu Song, Zepu Zhang, Henry Van dem Bedem, Ashley Deacon, Amanda Prado, Jessica Chiu, John Kovarik, Ana Gonzalez, John Mitchell, Panjat Kanjanarat , Mike Soltis, Hillary Yu, Ron Reyes, Lisa Dunn, Tim McPhillips, Dan Harrington, Mike Hollenbeck, Irimpan Mathews, Joseph Chang, Irina Tsyba, Ken Sharp, Paul Phizackerley

http://smb.slac.stanford.edu

Page 24: SSRL Crystal Mounting System. Sample Storage Cassette Stores 96 samples mounted on standard Hampton pins NdFeB ring magnet Teflon washer Hampton pin

Thanks For Your AttentionThanks For Your Attention