14 Hery Haerudin

8/14/2019 14 Hery Haerudin

1/27

RCChem-LIPI

By By By By

Hery Haerudin, Oman Zuas, Harry Budiman,Achmad Hanafi Setiawan

May 19May 19May 19May 19----23, 200823, 200823, 200823, 2008Daejeon, KoreaDaejeon, KoreaDaejeon, KoreaDaejeon, Korea

DEVELOPMENT AND PROGRESSDEVELOPMENT AND PROGRESS

ON GAS METROLOGY LABORATORYON GAS METROLOGY LABORATORY

At RCChemAt RCChem -- LIPI INDONESIALIPI INDONESIA


2/27

RCChem-LIPI

CONTENT

Metrology System in Indonesia

RCChem-LIPIs activities on Metrology Activities on Gas Metrology


3/27

RCChem-LIPI3

The Indonesian Instituteof Sciences

Chairman

Vice- Chairman

General Secretariat

Deputy of EarthSciences

Deputy of LifeSciences

Deputy of EngineeringSciences

Deputy of Social andHuman Sciences

Deputy of ScientificServices

ResearchCenter for

Biology

Research Centerfor Physics

ResearchCenter for

Society andCulture

Center for Callibrat,Instrumentat and

MetrologyResearchCenter for

GeotechnologyResearch

Center forBiotechnology

Research Centerfor Chemistry

ResearchCenter forEconomic

Center forStandardization and

Quality SystemsResearch CenterforOceanography

Center for PlantConcervation

(Bogor BotanicalGarden)

Research Centerfor Informatics

ResearchCenter for

Demography

Center forDocumentation and

Scientific InformationResearchCenter forLimnology

Research Center forElectrical Power and

Mecatronics

ResearchCenter for

Politics

Center for Innovation

ResearchCenter forMetallurgy

Research Center forElectronics and

Telecommunication

ResearchCenter forRegional

Resources

Unit Implementationfor Appropriate

Technology


4/27

RCChem-LIPI

Research Center for Chemistry - LIPI

Bidang Kimia Analitik dan Standar

Bidang TeknologiLingkungan

Bidang TeknologiProses dan Katalisis

Bidang Kimia BahanAlam, Pangan dan

Farmasi

Bidang Jasa IlmuPengetahuan dan

Teknologi

Subbidang PengembanganKerja Sama dan Jasa

Subbidang SistemInformasi

Subbidang SistemInformasi

Subbidang Promosi KaryaIlmiah

SubbagianKeuangan

SubbagianKepegawaian

Subbagian Sarana danPrasarana Penelitian

PUSAT PENELITIANKIMIA

Bagian Tata Usaha

SubbagianUmum

KelompokPenelitian KelompokPenelitian KelompokPenelitian KelompokPenelitian

Lampiran Keputusan Kepala LIPINomor : 1151/M/20001

Tanggal : 5 Juni 2001

LaboratoriumTerakreditasi


5/27

RCChem-LIPI

LEGISLATIONS

METROLOGY INFRASTRUCTURE

METROLOGY SYSTEM IN INDONESIA


6/27

RCChem-LIPI

METROLOGICAL LEGISLATIONSMETROLOGICAL LEGISLATIONSMETROLOGICAL LEGISLATIONSMETROLOGICAL LEGISLATIONS

The current metrological system based on Law No. 2/1981The current metrological system based on Law No. 2/1981The current metrological system based on Law No. 2/1981The current metrological system based on Law No. 2/1981

and defines the role of production and distribution of goodsand defines the role of production and distribution of goodsand defines the role of production and distribution of goodsand defines the role of production and distribution of goodsand measuring systemand measuring systemand measuring systemand measuring system

The second basic document is Decree No. 2/1989 whichThe second basic document is Decree No. 2/1989 whichThe second basic document is Decree No. 2/1989 whichThe second basic document is Decree No. 2/1989 whichregulates Indonesia National Standard of Measurement Unitregulates Indonesia National Standard of Measurement Unitregulates Indonesia National Standard of Measurement Unitregulates Indonesia National Standard of Measurement Unit

Relevant document No. 237/M/2007 (Head of LIPI) which assignsRelevant document No. 237/M/2007 (Head of LIPI) which assignsRelevant document No. 237/M/2007 (Head of LIPI) which assignsRelevant document No. 237/M/2007 (Head of LIPI) which assignsThe RCChemThe RCChemThe RCChemThe RCChem----LIPI as responsible to manage the technical aspectLIPI as responsible to manage the technical aspectLIPI as responsible to manage the technical aspectLIPI as responsible to manage the technical aspecton national standard for chemical metrology measurement unit.on national standard for chemical metrology measurement unit.on national standard for chemical metrology measurement unit.on national standard for chemical metrology measurement unit.


7/27

RCChem-LIPI

METROLOGY INFRASTRUCTUEMETROLOGY INFRASTRUCTUEMETROLOGY INFRASTRUCTUEMETROLOGY INFRASTRUCTUE

National Metrology National Metrology National Metrology National Metrology InstituteInstituteInstituteInstitute(LIPI)(LIPI)(LIPI)(LIPI) NationalNationalNationalNational

Accreditation Body Accreditation Body Accreditation Body Accreditation Body

NationalNationalNationalNationalStandardization Body Standardization Body Standardization Body Standardization Body

Metrology LegalMetrology LegalMetrology LegalMetrology Legal((((Ministry of Trade Ministry of Trade Ministry of Trade Ministry of Trade ))))

Research Centre forResearch Centre forResearch Centre forResearch Centre forCalibration, Metrology, and InstrumentationCalibration, Metrology, and InstrumentationCalibration, Metrology, and InstrumentationCalibration, Metrology, and Instrumentation

Research Centre forResearch Centre forResearch Centre forResearch Centre forChemistry (RCChem)Chemistry (RCChem)Chemistry (RCChem)Chemistry (RCChem)

Physic:Physic:Physic:Physic:Length, Time, MassTemperature, etc

Chemical:Chemical:Chemical:Chemical:Environmental andFood.


8/27

RCChem-LIPI

GENERAL SITUATION IN INDONESIA Despite of the existence of accreditation (nearly

300 testing laboratories in the field of chemicalanalysis have been accredited in Indonesia) andproficiency testing schemes, the use of CRMs isfar from widespread.

Laboratories trying to acquire CRMs for methodvalidation and for analytical quality assurancepurposes will find a hard facts that access tointernational market or commercial producers

are difficult and therefore high costs areencountered.


9/27

RCChem-LIPI

At present only laboratories having access tointernational market and ready to pay forrelatively high costs are using CRMs in regular

basis. For examples are petroleum products, coal

testing laboratories, but not yet foods,

environmental (except very few ones), clinicaltesting laboratories, etc. Many small and remote medium sized

laboratories are out of question.


10/27

RCChem-LIPI

Some other laboratories are using other types ofreference materials such as spiked samples,spiked blanks, reference materials havingconsensus values from a proficiency testingscheme for the analytical quality assurance oftheir test results.

Despite of the facts, however, concerns for usingCRMs are gradually growing now and thisshould be well anticipated by regulatory bodiesand relevant parties concerned.


11/27

RCChem-LIPI

IN SHORT

RCChem-LIPIs ACTIVITIES

on METROLOGY


12/27

RCChem-LIPI

RCChemRCChemRCChemRCChem- ---LIPILIPILIPILIPI s Activity on Metrology s Activity on Metrology s Activity on Metrology s Activity on Metrology IN SHORT IN SHORT IN SHORT IN SHORT

The application of Metrological Concept at The RCChemThe application of Metrological Concept at The RCChemThe application of Metrological Concept at The RCChemThe application of Metrological Concept at The RCChem- ---LIPI is :LIPI is :LIPI is :LIPI is :

Development of Reference Materials for Chemical Analysis purpoDevelopment of Reference Materials for Chemical Analysis purpoDevelopment of Reference Materials for Chemical Analysis purpoDevelopment of Reference Materials for Chemical Analysis purposes sessesses

Starting from 1997Starting from 1997Starting from 1997Starting from 1997 - --- Study on Reference MaterialStudy on Reference MaterialStudy on Reference MaterialStudy on Reference Materialfor environmental and foodfor environmental and foodfor environmental and foodfor environmental and food

Starting from 1999Starting from 1999Starting from 1999Starting from 1999 - --- Become provider for Proficiency TestingBecome provider for Proficiency TestingBecome provider for Proficiency TestingBecome provider for Proficiency Testing(PT) at National Level (13 t(PT) at National Level (13 t(PT) at National Level (13 t(PT) at National Level (13 times)imes)imes)imes)


13/27

RCChem-LIPI

RCChemRCChemRCChemRCChem- ---LIPILIPILIPILIPI s Activity on Metrology s Activity on Metrology s Activity on Metrology s Activity on Metrology IN SHORT IN SHORT IN SHORT IN SHORT

Starting from 2000Starting from 2000Starting from 2000Starting from 2000 - --- Active on Regional and InternationalActive on Regional and InternationalActive on Regional and InternationalActive on Regional and InternationalKey Comparison (APMP and CCQKey Comparison (APMP and CCQKey Comparison (APMP and CCQKey Comparison (APMP and CCQM)M)M)M)

-APMP QMAPMP QMAPMP QMAPMP QM----P1 (2000) through APMP P1 (2000) through APMP P1 (2000) through APMP P1 (2000) through APMP- ---P10 (2008)P10 (2008)P10 (2008)P10 (2008)

---- CCQM P64.1 (2008)CCQM P64.1 (2008)CCQM P64.1 (2008)CCQM P64.1 (2008)

Starting from 2007Starting from 2007Starting from 2007Starting from 2007 - --- Development of Gas Analysis Laboratory Development of Gas Analysis Laboratory Development of Gas Analysis Laboratory Development of Gas Analysis Laboratory for Metrology and Standard pfor Metrology and Standard pfor Metrology and Standard pfor Metrology and Standard purposesurposesurposesurposes


14/27

RCChem-LIPI

RCChem-LIPIs ACTIVITY ON GAS METROLOGY

( (( ( Commenced in 2007 Commenced in 2007 Commenced in 2007 Commenced in 2007 ) )) )


15/27

RCChem-LIPI

Why does Indonesia need Gas Metrology? Why does Indonesia need Gas Metrology? Why does Indonesia need Gas Metrology? Why does Indonesia need Gas Metrology?

Quick response to support:Industrial needs (Natural gas,

chemical industry, etc)Environmental regulation(vehicle gas emission)Legislation (Medical gases )

- There is no institute taken responsible in developmentof Standard Gas Mixture in Indonesia.

- To support National Metrology Institute in Indonesia

Standard Gas Mixture currently used:From foreign NMIExpensive (+delivery cost)Time consuming


16/27

RCChem-LIPI

ACTIVITY INI 2007 ACTIVITY INI 2007 ACTIVITY INI 2007 ACTIVITY INI 2007

Review the status of the RCChemReview the status of the RCChemReview the status of the RCChemReview the status of the RCChem- ---LIPILIPILIPILIPIs capabilities,s capabilities,s capabilities,s capabilities,includes:includes:includes:includes:

---- personnel of the projectpersonnel of the projectpersonnel of the projectpersonnel of the project---- Equipment (GCEquipment (GCEquipment (GCEquipment (GC- ---FID/ECD)FID/ECD)FID/ECD)FID/ECD)---- Room for gas laboratory (attached to RCCHemRoom for gas laboratory (attached to RCCHemRoom for gas laboratory (attached to RCCHemRoom for gas laboratory (attached to RCCHem- ---LIPILIPILIPILIPIssss

building)building)building)building)

Purchasing mass comparator, scale max. 10 kgPurchasing mass comparator, scale max. 10 kgPurchasing mass comparator, scale max. 10 kgPurchasing mass comparator, scale max. 10 kg

Design Gas Analysis laboratory Design Gas Analysis laboratory Design Gas Analysis laboratory Design Gas Analysis laboratory

Design and construct gas mixture equipment with turboDesign and construct gas mixture equipment with turboDesign and construct gas mixture equipment with turboDesign and construct gas mixture equipment with turbomolecular pumpmolecular pumpmolecular pumpmolecular pump


17/27

RCChem-LIPI

ACTIVITY IN 2007 ACTIVITY IN 2007 ACTIVITY IN 2007 ACTIVITY IN 2007

ISO/IEC 17025ISO/IEC 17025ISO/IEC 17025ISO/IEC 17025- ---2005 Training2005 Training2005 Training2005 Trainingfor personnel involved in thefor personnel involved in thefor personnel involved in thefor personnel involved in theprojectprojectprojectproject

Participating the 5th APMP/TCQMParticipating the 5th APMP/TCQMParticipating the 5th APMP/TCQMParticipating the 5th APMP/TCQM- ---GAWG Workshop in XiGAWG Workshop in XiGAWG Workshop in XiGAWG Workshop in Xi an City,an City,an City,an City,

R.O.C, 22R.O.C, 22R.O.C, 22R.O.C, 22----25 May 200725 May 200725 May 200725 May 2007


18/27

RCChem-LIPI

ACTIVITY IN 2008

Development gas analysis laboratory (Development gas analysis laboratory (Development gas analysis laboratory (Development gas analysis laboratory ( See next slide See next slide See next slide See next slide ))))

MoU collaboration: RCCHem LIPIMoU collaboration: RCCHem LIPIMoU collaboration: RCCHem LIPIMoU collaboration: RCCHem LIPI- ---KRISS in the Field of KRISS in the Field of KRISS in the Field of KRISS in the Field of Chemical Metrology was signed on March 10, 2008Chemical Metrology was signed on March 10, 2008Chemical Metrology was signed on March 10, 2008Chemical Metrology was signed on March 10, 2008

Participating the 6Participating the 6Participating the 6Participating the 6 hhhh APMP/TCQMAPMP/TCQMAPMP/TCQMAPMP/TCQM----GAWG WorkshopGAWG WorkshopGAWG WorkshopGAWG Workshopin Daejeon, Korea, 19in Daejeon, Korea, 19in Daejeon, Korea, 19in Daejeon, Korea, 19- ---23 May 200823 May 200823 May 200823 May 2008

Short Training/Lab Visit at KRISS on next 26Short Training/Lab Visit at KRISS on next 26Short Training/Lab Visit at KRISS on next 26Short Training/Lab Visit at KRISS on next 26- ---28 May 200828 May 200828 May 200828 May 2008


19/27

RCChem-LIPI

DEVELOPMENT GAS ANALYSISDEVELOPMENT GAS ANALYSISDEVELOPMENT GAS ANALYSISDEVELOPMENT GAS ANALYSISLABORATORY LABORATORY LABORATORY LABORATORY (((( Activity in 2008, Cont. Activity in 2008, Cont. Activity in 2008, Cont. Activity in 2008, Cont. ))))

Design Filling and Weighing room (Design Filling and Weighing room (Design Filling and Weighing room (Design Filling and Weighing room ( Jan Jan Jan Jan---- Feb 2008Feb 2008Feb 2008Feb 2008 ))))

Build Filling and Weighing room (Build Filling and Weighing room (Build Filling and Weighing room (Build Filling and Weighing room ( March.March.March.March.----presentpresentpresentpresent ))))

Installment Gas mixture equipmentInstallment Gas mixture equipmentInstallment Gas mixture equipmentInstallment Gas mixture equipment((((In progressIn progressIn progressIn progress ))))


20/27

RCChem-LIPI

Lay out: RCChemLay out: RCChemLay out: RCChemLay out: RCChem----LIPI Building (Floor 1)LIPI Building (Floor 1)LIPI Building (Floor 1)LIPI Building (Floor 1)

Gas Analysis Laboratory Gas Analysis Laboratory Gas Analysis Laboratory Gas Analysis Laboratory


21/27

RCChem-LIPI

Lay out: Gas Analysis Laboratory Lay out: Gas Analysis Laboratory Lay out: Gas Analysis Laboratory Lay out: Gas Analysis Laboratory

Gas filling roomGas filling roomGas filling roomGas filling room

Gas weighing roomGas weighing roomGas weighing roomGas weighing room


22/27


23/27

RCChem-LIPI

RCChemRCChemRCChemRCChem- ---Direction ForDirection ForDirection ForDirection ForGas Standard Development Gas Standard Development Gas Standard Development Gas Standard Development

Vehicles/Industry stack Emission Gas (CO2, CO,Vehicles/Industry stack Emission Gas (CO2, CO,Vehicles/Industry stack Emission Gas (CO2, CO,Vehicles/Industry stack Emission Gas (CO2, CO,NO, CNO, CNO, CNO, C 3333HHHH8,8,8,8, etc.)etc.)etc.)etc.)

Ambient air quality (NAmbient air quality (NAmbient air quality (NAmbient air quality (N 2222O, Benzene, OO, Benzene, OO, Benzene, OO, Benzene, O 3333, etc), etc), etc), etc)

Natural GasNatural GasNatural GasNatural Gas

Special Gas for Indonesian Industries (ChemicalSpecial Gas for Indonesian Industries (ChemicalSpecial Gas for Indonesian Industries (ChemicalSpecial Gas for Indonesian Industries (Chemical

and Electronic industries) (Later)and Electronic industries) (Later)and Electronic industries) (Later)and Electronic industries) (Later)


24/27

RCChem-LIPI

Five Years Planning 2010Five Years Planning 2010Five Years Planning 2010Five Years Planning 2010- ---2014201420142014

In 2010- 2011 :

Plan to prepare CO in N 2 and CO 2 in N 2Plan to prepare NO in N 2 and O 2 in N 2

In 2012- 2013 ( Vehicles emission gases ) :

Plan to prepare CH 4 in N 2Plan to prepare C

3H

8in N2

Plan to prepare SO 2 in N 2


25/27

RCChem-LIPI

Hopefully soon we will

fulfill the Quality System for Gas Analysis Laboratory.

ISO/IEC 17025:2005 (Calibration and Testing

Laboratory ISO 6142 and ISO 6143 (Gas Analysis

Production)

ISO Guide 34 (Production of Reference Material )


26/27

RCChem-LIPI

THERE ISTHERE ISTHERE ISTHERE IS NONONONO SCIENCE WITHOUT MEASUREMENT,SCIENCE WITHOUT MEASUREMENT,SCIENCE WITHOUT MEASUREMENT,SCIENCE WITHOUT MEASUREMENT,

NONONONO QUALITY WITHOUT TESTING,QUALITY WITHOUT TESTING,QUALITY WITHOUT TESTING,QUALITY WITHOUT TESTING,

andandandand NONONONO GLOBAL MARKET WITHOUT STANDARDSGLOBAL MARKET WITHOUT STANDARDSGLOBAL MARKET WITHOUT STANDARDSGLOBAL MARKET WITHOUT STANDARDS


27/27

Documents

14 Hery Haerudin