*Kiroptikai spektroszkpiasszelltotta: Pl Krisztina

*BevezetA kiroptikai spektroszkpik jelentsge abban ll, hogy segtsgkkel klnbsget tehetnk enantiomerek kztt, vagy diasztereomerek kzt.Polarimetria (optikai forgats adott hullmhosszon), ORD /optikai rotcis diszperzi/ (optikai forgats a hullmhossz fggvnyben) CD /cikulris dikroizmus/ (jobbra s balra cirkulrisan polarizlt fny abszorpcija kzti klnbsget mri a hullmhossz fggvnyben)Mindegyik technika az (optikailag aktv) anyag s a polarizlt fny kzti klcsnhats mrsn alapszik.

*Optikailag aktv, kirlis anyagAz olyan anyagokat, amelyek a polros fny rezgsi skjt elforgatjk, optikailag aktv anyagoknak nevezzk. (A jelensget kezdetben csak a kristlyos anyagok szerkezetnek aszimmetrijval hoztk sszefggsbe).Arago, kvarckristly (1811)Biot, borksav vizes oldat (1838)Pasteur, aszimmetria optikai aktivits (1848-53)Kekul (1856-1863), Le Bel s van't Hoff (1874); aszimmetrikus, tetraderes C-atomKirlis: tkrkpvel nem fedsbe hozhat. Az egymssal fedsbe nem hozhat tkrkpi szerkezetek olyan viszonyban vannak egymssal, mint a jobb s bal kz (a kz grg nevbl - kheir - szrmazik az ilyen szerkezetek kirlis elnevezse). Optikai aktivits = forgatkpessg; kirlis molekulk nem racm halmaza optikailag aktv

*Enantiomerek (1)Egy enantiomer az egyike annak a kt sztereoizomernek, amelyek egymsnak fedsbe nem hozhat tkrkpei (mint a jobb s bal keznk; ugyanazok, de mgis ellenttei egymsnak).Szimmetrikus krnyezetben: azonos fizikai s kmiai tulajdonsgok Aszimmetrikus krnyezetben: klnbz tulajdonsgok. Kirlis molekulk egymshoz val viszonya

*Enantiomerek (2)Azonos olvads- s forrspont, trsmutat, oldhatsg, UV-lthat, IR- s NMR spektrum.A klnbz viselkeds kirlis genssel val klcsnhats esetn rvnyesl: Kirlis oldszerekben oldhatsguk klnbzikKirlis vegyletekkel klnflekpp reaglnak (pl. diasztereomer kpzs, rezolvls alapja)Kirlis fnnyel klnflekpp hatnak klcsn

(Diasztereomerek: rszleges tkrkpei egymsnak; 1 vagy tbb aszimmetriacentrum abszolt konfigurcija eltr. Epimerek: csak egy aszimmetriacentrum abszolt konfigurcija ms)

*Kiralits fajti

Centrlis kiralitsVonal kiralitsAnza kiralitsHeliklis kiralits

*A fny polarizcijaAz elektromgneses sugrzs (fny) egy halad hullm, amely oszcilll elektromos- s mgneses trbl ll, melyek klcsnsen merlegesek egymsra. ltalban az elektromos tr oszcillcija NEM egy fix (y,x) skon trtnik. Ilyenkor a sugrzs NEM polarizlt.xyzNem polarizlt fnySkban polarizlt fny

*Skban polarizlt fny ellltsaPolarizlatlan fnyA vertiklisan polarizlt komponens tjut.A horizontlisan polarizlt komponens abszorbeldik (nem jut t a szrn).A polarizcis szr a polarizlatlan fnyt skban (linerisan) polarizlt fnny alaktja. Erre j plda a Polaroid szr, mely hosszks molekulk prhuzamosan rendezett szlaibl ll. Csak a megfelel irnyban polarizlt fnykomponens jut t a szrn (az erre merleges komponens tkletesen abszorbeldik).

*A linerisan polarizlt fny kt cirkulris komponense

*Optikai forgatsA kirlis minta trsmutatja ms a skban polarizlt fny kt cirkulrisan polarizlt komponensre (jobbra s balra cirkulrisan polarizlt fny) nzve.nbalnjobbEbbl kvetkezen a kt cirkulris komponens sebessge ms s ms, amint kirlis mintn haladnak t.n=c/v Eredmny: a skban polarizlt fny polarizcis skja elfordul ( szggel).

*Optikai forgats (2)

*Polarimetria: Az optikai forgats adott hullmhosszon/589nm (Na D-vonal)/

*Optikai forgatsltalban specifikus forgatsknt van megadva [], melyet adott hmrskleten (T) s hullmhosszon (, lt. 589 nm) mrnek (a minta adott koncentrcij, adott oldszerrel kszlt oldatt alkalmazva).Megadsa: []D25 = +65 (c=1.0, EtOH) +, ramutat jrsval megegyez irny , ramutat jrsval ellenttesTisztasg meghatrozs: Mrt specifikus forgats*100 specifikus forgats(Pl.: (+6,76/+13,52)*100=50%)

*Optikai rotcis diszperzi (ORD)Az optikai forgatst mrjk a hullmhossz fggvnyben. (diszperzi = a hullmhossz fggvnyben)Polikromatikus fnyforrsDetektor: fotoelektron sokszoroz

*ORD spektrumEgyenletes lefuts grbe (n. plain curve) - ha a kirlis molekulban nincsen kromofr (nincs elnyels).Kromofrt tartalmaz kirlis minta esetn n. Cotton effektus (anomlia) rakdik a plain curve-re, ott ahol a minta elnyel. A cscs s a vly kzti metszspont hullmhossza jl egyezik az abszorpcis max al..

*Cirkulris dikroizmus

*Cirkulris dikroizmus (2)A skban polarizlt fny kt cirkulris komponense (jobbra s balra cirkulrisan polarizlt fny) klnbz mrtkben nyeldik el (abszorbeldik) kirlis mintn thaladva.Linerisan polarizlt fnyElliptikusan polarizlt fnysszegk:

*CD spektrumA CD spektrumban A-t, -t (egyezmnyesen bal-jobb) tntetik fel a hullmhossz fggvnyben. (nha az ellipticitst (), a molris ellipticitst [])AbalAjobb A /cl (A=Abal-Ajobb)= bal-jobb

l=190-800nm, e- gerjesztsAAjobbAbal

*Enantiomerek CD spektrumajobb,(R)= bal,(S), bal,(R)= jobb,(S) bal, (R)- jobb,(R) = (R) = jobb, (S)- bal,(S) = (S)bal, (S)- jobb,(S)= (S)= jobb, (R)- bal,(R)= (R)

TKRKPI VISZONY

Diagram3

0.145678-0.145678

0.1431755-0.1431755

0.145624-0.145624

0.150861-0.150861

0.1483205-0.1483205

0.148069-0.148069

0.15208-0.15208

0.147598-0.147598

0.149542-0.149542

0.1519625-0.1519625

0.159704-0.159704

0.162678-0.162678

0.155568-0.155568

0.1430205-0.1430205

0.1418535-0.1418535

0.1442705-0.1442705

0.149299-0.149299

0.161563-0.161563

0.180604-0.180604

0.190772-0.190772

0.1969525-0.1969525

0.193187-0.193187

0.1784595-0.1784595

0.1635295-0.1635295

0.1660295-0.1660295

0.166937-0.166937

0.155297-0.155297

0.1445435-0.1445435

0.1393755-0.1393755

0.1428765-0.1428765

0.156191-0.156191

0.176162-0.176162

0.189028-0.189028

0.18875-0.18875

0.1933415-0.1933415

0.191861-0.191861

0.1943835-0.1943835

0.194-0.194

0.194408-0.194408

0.189193-0.189193

0.182947-0.182947

0.179842-0.179842

0.1744015-0.1744015

0.1695945-0.1695945

0.1680825-0.1680825

0.170753-0.170753

0.179082-0.179082

0.1761575-0.1761575

0.176591-0.176591

0.1758395-0.1758395

0.1719985-0.1719985

0.160309-0.160309

0.1551565-0.1551565

0.158066-0.158066

0.1648575-0.1648575

0.16513-0.16513

0.1725505-0.1725505

0.170663-0.170663

0.166629-0.166629

0.172394-0.172394

0.1757125-0.1757125

0.1721685-0.1721685

0.164869-0.164869

0.158937-0.158937

0.1452175-0.1452175

0.1416955-0.1416955

0.142084-0.142084

0.142287-0.142287

0.137589-0.137589

0.1321745-0.1321745

0.1297445-0.1297445

0.125201-0.125201

0.1278885-0.1278885

0.133232-0.133232

0.1384925-0.1384925

0.1354975-0.1354975

0.1284305-0.1284305

0.1221715-0.1221715

0.1220075-0.1220075

0.1259985-0.1259985

0.1319635-0.1319635

0.1287255-0.1287255

0.125589-0.125589

0.126227-0.126227

0.1345205-0.1345205

0.132087-0.132087

0.1182065-0.1182065

0.1105675-0.1105675

0.1092585-0.1092585

0.109012-0.109012

0.105648-0.105648

0.108863-0.108863

0.108411-0.108411

0.1011235-0.1011235

0.1000895-0.1000895

0.1020945-0.1020945

0.095546-0.095546

0.099334-0.099334

0.097811-0.097811

0.096172-0.096172

0.096384-0.096384

0.092768-0.092768

0.0988615-0.0988615

0.1047315-0.1047315

0.11881-0.11881

0.123761-0.123761

0.121056-0.121056

0.119763-0.119763

0.1163505-0.1163505

0.1173975-0.1173975

0.1235135-0.1235135

0.1228555-0.1228555

0.1203085-0.1203085

0.1163805-0.1163805

0.1216135-0.1216135

0.1164275-0.1164275

0.1081805-0.1081805

0.0987745-0.0987745

0.090489-0.090489

0.1018075-0.1018075

0.107617-0.107617

0.114935-0.114935

0.123686-0.123686

0.1299605-0.1299605

0.128228-0.128228

0.1216235-0.1216235

0.126638-0.126638

0.1349615-0.1349615

0.1345185-0.1345185

0.1330605-0.1330605

0.127987-0.127987

0.12271-0.12271

0.120125-0.120125

0.110186-0.110186

0.1150865-0.1150865

0.12075-0.12075

0.124915-0.124915

0.123173-0.123173

0.123269-0.123269

0.124134-0.124134

0.122272-0.122272

0.1204395-0.1204395

0.116522-0.116522

0.112584-0.112584

0.1088465-0.1088465

0.1042565-0.1042565

0.099236-0.099236

0.097558-0.097558

0.108932-0.108932

0.1260215-0.1260215

0.135912-0.135912

0.1396945-0.1396945

0.141866-0.141866

0.135166-0.135166

0.131461-0.131461

0.1228345-0.1228345

0.1214825-0.1214825

0.124225-0.124225

0.13141-0.13141

0.135391-0.135391

0.1279585-0.1279585

0.128908-0.128908

0.136101-0.136101

0.1470735-0.1470735

0.1566075-0.1566075

0.1615935-0.1615935

0.17056-0.17056

0.17763-0.17763

0.175262-0.175262

0.169505-0.169505

0.1625495-0.1625495

0.1596025-0.1596025

0.1505045-0.1505045

0.1483195-0.1483195

0.157404-0.157404

0.1727285-0.1727285

0.182918-0.182918

0.1855005-0.1855005

0.1851585-0.1851585

0.186814-0.186814

0.1849715-0.1849715

0.1764595-0.1764595

0.1614175-0.1614175

0.1517815-0.1517815

0.1514965-0.1514965

0.1538715-0.1538715

0.161709-0.161709

0.1661155-0.1661155

0.1681565-0.1681565

0.169812-0.169812

0.1673045-0.1673045

0.162911-0.162911

0.1554925-0.1554925

0.1551445-0.1551445

0.160333-0.160333

0.16086-0.16086

0.1581085-0.1581085

0.1542315-0.1542315

0.1621435-0.1621435

0.162463-0.162463

0.164486-0.164486

0.1638065-0.1638065

0.1682495-0.1682495

0.173578-0.173578

0.1722585-0.1722585

0.1750575-0.1750575

0.1696665-0.1696665

0.158712-0.158712

0.153773-0.153773

0.15031-0.15031

0.1480105-0.1480105

0.14803-0.14803

0.1459375-0.1459375

0.1469305-0.1469305

0.149047-0.149047

0.1440125-0.1440125

0.1429845-0.1429845

0.139001-0.139001

0.1398855-0.1398855

0.1321-0.1321

0.1237105-0.1237105

0.122532-0.122532

0.118612-0.118612

0.111952-0.111952

0.110958-0.110958

0.1152115-0.1152115

0.122727-0.122727

0.1231325-0.1231325

0.12214-0.12214

0.1188105-0.1188105

0.117277-0.117277

0.112319-0.112319

0.1018405-0.1018405

0.098176-0.098176

0.097584-0.097584

0.0942815-0.0942815

0.089333-0.089333

0.086392-0.086392

0.085962-0.085962

0.0939755-0.0939755

0.106045-0.106045

0.107664-0.107664

0.102595-0.102595

0.0994715-0.0994715

0.0996235-0.0996235

0.0985095-0.0985095

0.0938465-0.0938465

0.0952555-0.0952555

0.098805-0.098805

0.1037245-0.1037245

0.115359-0.115359

0.1194795-0.1194795

0.1160115-0.1160115

0.11553-0.11553

0.1171625-0.1171625

0.118825-0.118825

0.122893-0.122893

0.1225585-0.1225585

0.117145-0.117145

0.1133095-0.1133095

0.1119665-0.1119665

0.102962-0.102962

0.094204-0.094204

0.091235-0.091235

0.087522-0.087522

0.0859915-0.0859915

0.086621-0.086621

0.0814855-0.0814855

0.0763675-0.0763675

0.0670445-0.0670445

0.0675325-0.0675325

0.061973-0.061973

0.060827-0.060827

0.0581315-0.0581315

0.0590955-0.0590955

0.064395-0.064395

0.065137-0.065137

0.0532305-0.0532305

0.051917-0.051917

0.05777-0.05777

0.056862-0.056862

0.0553095-0.0553095

0.0532135-0.0532135

0.0502795-0.0502795

0.04896545-0.04896545

0.056058-0.056058

0.0637075-0.0637075

0.0707965-0.0707965

0.0719615-0.0719615

0.0720595-0.0720595

0.0721545-0.0721545

0.074759-0.074759

0.081632-0.081632

0.090545-0.090545

0.099568-0.099568

0.112276-0.112276

0.1184495-0.1184495

0.1301725-0.1301725

0.143922-0.143922

0.1512045-0.1512045

0.1526365-0.1526365

0.1617745-0.1617745

0.1732125-0.1732125

0.1712255-0.1712255

0.1723265-0.1723265

0.177952-0.177952

0.1720615-0.1720615

0.175221-0.175221

0.1774985-0.1774985

0.18185-0.18185

0.1974505-0.1974505

0.2127955-0.2127955

0.216062-0.216062

0.2264335-0.2264335

0.241332-0.241332

0.245693-0.245693

0.2501995-0.2501995

0.2494035-0.2494035

0.2444875-0.2444875

0.249372-0.249372

0.24887-0.24887

0.2531385-0.2531385

0.2556275-0.2556275

0.262488-0.262488

0.268981-0.268981

0.270376-0.270376

0.2617175-0.2617175

0.2520745-0.2520745

0.2573465-0.2573465

0.263204-0.263204

0.2647955-0.2647955

0.262253-0.262253

0.261295-0.261295

0.257266-0.257266

0.258584-0.258584

0.263666-0.263666

0.2723845-0.2723845

0.281071-0.281071

0.282067-0.282067

0.285509-0.285509

0.282735-0.282735

0.28016-0.28016

0.2789085-0.2789085

0.281448-0.281448

0.2852775-0.2852775

0.2914795-0.2914795

0.2919395-0.2919395

0.2965755-0.2965755

0.3086165-0.3086165

0.3124245-0.3124245

0.3151655-0.3151655

0.3212965-0.3212965

0.3252675-0.3252675

0.325105-0.325105

0.329738-0.329738

0.332493-0.332493

0.3302535-0.3302535

0.3296755-0.3296755

0.329687-0.329687

0.3405455-0.3405455

0.353248-0.353248

0.3518425-0.3518425

0.354046-0.354046

0.356901-0.356901

0.3574805-0.3574805

0.353935-0.353935

0.3589785-0.3589785

0.364644-0.364644

0.355599-0.355599

0.3450375-0.3450375

0.345597-0.345597

0.353197-0.353197

0.3623915-0.3623915

0.3699195-0.3699195

0.368133-0.368133

0.3641615-0.3641615

0.367093-0.367093

0.362452-0.362452

0.3482225-0.3482225

0.3420855-0.3420855

0.331177-0.331177

0.3174285-0.3174285

0.31859-0.31859

0.320317-0.320317

0.323674-0.323674

0.3238375-0.3238375

0.331671-0.331671

0.3419405-0.3419405

0.3470805-0.3470805

0.3568065-0.3568065

0.3676055-0.3676055

0.368343-0.368343

0.369207-0.369207

0.369639-0.369639

0.373258-0.373258

0.3679165-0.3679165

0.3687565-0.3687565

0.374282-0.374282

0.383835-0.383835

0.394064-0.394064

0.3999645-0.3999645

0.404413-0.404413

0.417887-0.417887

0.4235375-0.4235375

0.419694-0.419694

0.413574-0.413574

0.41289-0.41289

0.422915-0.422915

0.429748-0.429748

0.432347-0.432347

0.429606-0.429606

0.442578-0.442578

0.4520475-0.4520475

0.4636705-0.4636705

0.47016-0.47016

0.473977-0.473977

0.480056-0.480056

0.489224-0.489224

0.4946325-0.4946325

0.4954055-0.4954055

0.4933925-0.4933925

0.492943-0.492943

0.4985875-0.4985875

0.4930225-0.4930225

0.4924305-0.4924305

0.50163-0.50163

0.4998975-0.4998975

0.500185-0.500185

0.50359-0.50359

0.51591-0.51591

0.51776-0.51776

0.52744-0.52744

0.533765-0.533765

0.5324-0.5324

0.5407-0.5407

0.54307-0.54307

0.54276-0.54276

0.552675-0.552675

0.558255-0.558255

0.561395-0.561395

0.5724-0.5724

0.58648-0.58648

0.594935-0.594935

0.59808-0.59808

0.60348-0.60348

0.612915-0.612915

0.62233-0.62233

0.622395-0.622395

0.62611-0.62611

0.622035-0.622035

0.619465-0.619465

0.621605-0.621605

0.6288-0.6288

0.63756-0.63756

0.644735-0.644735

0.64945-0.64945

0.660985-0.660985

0.66908-0.66908

0.66769-0.66769

0.665035-0.665035

0.66832-0.66832

0.673145-0.673145

0.664385-0.664385

0.66424-0.66424

0.66314-0.66314

0.661045-0.661045

0.66801-0.66801

0.674715-0.674715

0.684985-0.684985

0.694845-0.694845

0.701625-0.701625

0.713905-0.713905

0.72617-0.72617

0.727405-0.727405

0.72926-0.72926

0.730665-0.730665

0.735845-0.735845

0.74275-0.74275

0.74162-0.74162

0.740865-0.740865

0.74402-0.74402

0.741815-0.741815

0.75629-0.75629

0.76837-0.76837

0.769835-0.769835

0.780645-0.780645

0.78895-0.78895

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2.01009-2.01009

2.071005-2.071005

2.113915-2.113915

2.115045-2.115045

2.140495-2.140495

2.19661-2.19661

2.298335-2.298335

2.378475-2.378475

2.52472-2.52472

2.65763-2.65763

2.71857-2.71857

2.9076-2.9076

3.020115-3.020115

3.183295-3.183295

3.320805-3.320805

3.365465-3.365465

3.49058-3.49058

3.653405-3.653405

3.72551-3.72551

3.7537-3.7537

3.794855-3.794855

3.84882-3.84882

3.85659-3.85659

3.90189-3.90189

3.955655-3.955655

4.212065-4.212065

4.42175-4.42175

4.55857-4.55857

4.556695-4.556695

4.57663-4.57663

4.59124-4.59124

4.648125-4.648125

4.727535-4.727535

4.7039-4.7039

4.67133-4.67133

4.627005-4.627005

4.57993-4.57993

4.558925-4.558925

4.575285-4.575285

4.61553-4.61553

4.55152-4.55152

4.39617-4.39617

4.301315-4.301315

4.321505-4.321505

4.180015-4.180015

4.028015-4.028015

3.983765-3.983765

3.99636-3.99636

3.949945-3.949945

3.80916-3.80916

3.665205-3.665205

3.60567-3.60567

3.556125-3.556125

3.54541-3.54541

3.651765-3.651765

3.595795-3.595795

3.75516-3.75516

3.87267-3.87267

3.845015-3.845015

3.933385-3.933385

4.13698-4.13698

4.30855-4.30855

4.44407-4.44407

4.62129-4.62129

4.89613-4.89613

4.897325-4.897325

5.16895-5.16895

5.21555-5.21555

5.1897-5.1897

5.21295-5.21295

5.26485-5.26485

5.17305-5.17305

4.994975-4.994975

5.17645-5.17645

5.25765-5.25765

5.14525-5.14525

hullmhossz [nm]

De [dm3 mol-1 cm-1]

Munka1

AZMAmademadee

400-0.4505430.2913564000.145678-0.145678

399.9-0.4578260.286351399.90.1431755-0.1431755

399.8-0.4609240.291248399.80.145624-0.145624

399.7-0.4568340.301722399.70.150861-0.150861

399.6-0.4553990.296641399.60.1483205-0.1483205

399.5-0.4581240.296138399.50.148069-0.148069

399.4-0.4723630.30416399.40.15208-0.15208

399.3-0.4888530.295196399.30.147598-0.147598

399.2-0.4907560.299084399.20.149542-0.149542

399.1-0.4890410.303925399.10.1519625-0.1519625

399-0.4939180.3194083990.159704-0.159704

398.9-0.4904660.325356398.90.162678-0.162678

398.8-0.4881260.311136398.80.155568-0.155568

398.7-0.4992150.286041398.70.1430205-0.1430205

398.6-0.5072710.283707398.60.1418535-0.1418535

398.5-0.4928320.288541398.50.1442705-0.1442705

398.4-0.4714130.298598398.40.149299-0.149299

398.3-0.4547890.323126398.30.161563-0.161563

398.2-0.432020.361208398.20.180604-0.180604

398.1-0.4285930.381544398.10.190772-0.190772

398-0.4207310.3939053980.1969525-0.1969525

397.9-0.4213260.386374397.90.193187-0.193187

397.8-0.4314260.356919397.80.1784595-0.1784595

397.7-0.4315580.327059397.70.1635295-0.1635295

397.6-0.4249170.332059397.60.1660295-0.1660295

397.5-0.4248910.333874397.50.166937-0.166937

397.4-0.4447350.310594397.40.155297-0.155297

397.3-0.4643280.289087397.30.1445435-0.1445435

397.2-0.4706750.278751397.20.1393755-0.1393755

397.1-0.4587020.285753397.10.1428765-0.1428765

397-0.4395480.3123823970.156191-0.156191

396.9-0.3962640.352324396.90.176162-0.176162

396.8-0.3807070.378056396.80.189028-0.189028

396.7-0.400380.3775396.70.18875-0.18875

396.6-0.4104990.386683396.60.1933415-0.1933415

396.5-0.4110730.383722396.50.191861-0.191861

396.4-0.4088420.388767396.40.1943835-0.1943835

396.3-0.4013440.388396.30.194-0.194

396.2-0.3839410.388816396.20.194408-0.194408

396.1-0.3741390.378386396.10.189193-0.189193

396-0.3749760.3658943960.182947-0.182947

395.9-0.3672630.359684395.90.179842-0.179842

395.8-0.3662410.348803395.80.1744015-0.1744015

395.7-0.3584750.339189395.70.1695945-0.1695945

395.6-0.3465840.336165395.60.1680825-0.1680825

395.5-0.3295240.341506395.50.170753-0.170753

395.4-0.3016010.358164395.40.179082-0.179082

395.3-0.2894290.352315395.30.1761575-0.1761575

395.2-0.2865320.353182395.20.176591-0.176591

395.1-0.299530.351679395.10.1758395-0.1758395

395-0.3051990.3439973950.1719985-0.1719985

394.9-0.3239950.320618394.90.160309-0.160309

394.8-0.3374980.310313394.80.1551565-0.1551565

394.7-0.3424920.316132394.70.158066-0.158066

394.6-0.3323910.329715394.60.1648575-0.1648575

394.5-0.3200710.33026394.50.16513-0.16513

394.4-0.3033120.345101394.40.1725505-0.1725505

394.3-0.2977810.341326394.30.170663-0.170663

394.2-0.2952240.333258394.20.166629-0.166629

394.1-0.2944370.344788394.10.172394-0.172394

394-0.2795670.3514253940.1757125-0.1757125

393.9-0.2665440.344337393.90.1721685-0.1721685

393.8-0.2679530.329738393.80.164869-0.164869

393.7-0.257150.317874393.70.158937-0.158937

393.6-0.2709880.290435393.60.1452175-0.1452175

393.5-0.2748470.283391393.50.1416955-0.1416955

393.4-0.2630620.284168393.40.142084-0.142084

393.3-0.260710.284574393.30.142287-0.142287

393.2-0.2707480.275178393.20.137589-0.137589

393.1-0.2842510.264349393.10.1321745-0.1321745

393-0.2892080.2594893930.1297445-0.1297445

392.9-0.30640.250402392.90.125201-0.125201

392.8-0.3220440.255777392.80.1278885-0.1278885

392.7-0.3197470.266464392.70.133232-0.133232

392.6-0.3234820.276985392.60.1384925-0.1384925

392.5-0.3462830.270995392.50.1354975-0.1354975

392.4-0.3632680.256861392.40.1284305-0.1284305

392.3-0.3584270.244343392.30.1221715-0.1221715

392.2-0.3496460.244015392.20.1220075-0.1220075

392.1-0.3506190.251997392.10.1259985-0.1259985

392-0.3434760.2639273920.1319635-0.1319635

391.9-0.3473510.257451391.90.1287255-0.1287255

391.8-0.3353540.251178391.80.125589-0.125589

391.7-0.3396010.252454391.70.126227-0.126227

391.6-0.323210.269041391.60.1345205-0.1345205

391.5-0.3076040.264174391.50.132087-0.132087

391.4-0.310590.236413391.40.1182065-0.1182065

391.3-0.3163210.221135391.30.1105675-0.1105675

391.2-0.3319390.218517391.20.1092585-0.1092585

391.1-0.3504530.218024391.10.109012-0.109012

391-0.3761280.2112963910.105648-0.105648

390.9-0.3891070.217726390.90.108863-0.108863

390.8-0.3825340.216822390.80.108411-0.108411

390.7-0.3954440.202247390.70.1011235-0.1011235

390.6-0.4128550.200179390.60.1000895-0.1000895

390.5-0.4192250.204189390.50.1020945-0.1020945

390.4-0.4450910.191092390.40.095546-0.095546

390.3-0.4634470.198668390.30.099334-0.099334

390.2-0.4747690.195622390.20.097811-0.097811

390.1-0.4786950.192344390.10.096172-0.096172

390-0.4726430.1927683900.096384-0.096384

389.9-0.4695150.185536389.90.092768-0.092768

389.8-0.4416360.197723389.80.0988615-0.0988615

389.7-0.4190070.209463389.70.1047315-0.1047315

389.6-0.4056140.23762389.60.11881-0.11881

389.5-0.3957180.247522389.50.123761-0.123761

389.4-0.3891630.242112389.40.121056-0.121056

389.3-0.3809310.239526389.30.119763-0.119763

389.2-0.3750640.232701389.20.1163505-0.1163505

389.1-0.3745080.234795389.10.1173975-0.1173975

389-0.3837720.2470273890.1235135-0.1235135

388.9-0.4151340.245711388.90.1228555-0.1228555

388.8-0.4391830.240617388.80.1203085-0.1203085

388.7-0.4435620.232761388.70.1163805-0.1163805

388.6-0.4228540.243227388.60.1216135-0.1216135

388.5-0.4375950.232855388.50.1164275-0.1164275

388.4-0.4421840.216361388.40.1081805-0.1081805

388.3-0.4436980.197549388.30.0987745-0.0987745

388.2-0.4585790.180978388.20.090489-0.090489

388.1-0.4600080.203615388.10.1018075-0.1018075

388-0.4675750.2152343880.107617-0.107617

387.9-0.4548330.22987387.90.114935-0.114935

387.8-0.4436420.247372387.80.123686-0.123686

387.7-0.4332230.259921387.70.1299605-0.1299605

387.6-0.420920.256456387.60.128228-0.128228

387.5-0.4272870.243247387.50.1216235-0.1216235

387.4-0.4300760.253276387.40.126638-0.126638

387.3-0.429190.269923387.30.1349615-0.1349615

387.2-0.4339010.269037387.20.1345185-0.1345185

387.1-0.4243530.266121387.10.1330605-0.1330605

387-0.4199840.2559743870.127987-0.127987

386.9-0.4043930.24542386.90.12271-0.12271

386.8-0.394520.24025386.80.120125-0.120125

386.7-0.4000530.220372386.70.110186-0.110186

386.6-0.3850840.230173386.60.1150865-0.1150865

386.5-0.3695840.2415386.50.12075-0.12075

386.4-0.3749820.24983386.40.124915-0.124915

386.3-0.3758050.246346386.30.123173-0.123173

386.2-0.3725550.246538386.20.123269-0.123269

386.1-0.3663570.248268386.10.124134-0.124134

386-0.3593340.2445443860.122272-0.122272

385.9-0.350230.240879385.90.1204395-0.1204395

385.8-0.3447050.233044385.80.116522-0.116522

385.7-0.3384980.225168385.70.112584-0.112584

385.6-0.3339450.217693385.60.1088465-0.1088465

385.5-0.3277890.208513385.50.1042565-0.1042565

385.4-0.3356180.198472385.40.099236-0.099236

385.3-0.3561810.195116385.30.097558-0.097558

385.2-0.3585530.217864385.20.108932-0.108932

385.1-0.3318940.252043385.10.1260215-0.1260215

385-0.3233570.2718243850.135912-0.135912

384.9-0.3152030.279389384.90.1396945-0.1396945

384.8-0.3034740.283732384.80.141866-0.141866

384.7-0.3032620.270332384.70.135166-0.135166

384.6-0.2950520.262922384.60.131461-0.131461

384.5-0.2996680.245669384.50.1228345-0.1228345

384.4-0.3010310.242965384.40.1214825-0.1214825

384.3-0.2863410.24845384.30.124225-0.124225

384.2-0.2593630.26282384.20.13141-0.13141

384.1-0.2296370.270782384.10.135391-0.135391

384-0.2170390.2559173840.1279585-0.1279585

383.9-0.186740.257816383.90.128908-0.128908

383.8-0.1632060.272202383.80.136101-0.136101

383.7-0.1423870.294147383.70.1470735-0.1470735

383.6-0.1345470.313215383.60.1566075-0.1566075

383.5-0.137580.323187383.50.1615935-0.1615935

383.4-0.1461160.34112383.40.17056-0.17056

383.3-0.1542850.35526383.30.17763-0.17763

383.2-0.1778020.350524383.20.175262-0.175262

383.1-0.1902070.33901383.10.169505-0.169505

383-0.19460.3250993830.1625495-0.1625495

382.9-0.1892030.319205382.90.1596025-0.1596025

382.8-0.1995930.301009382.80.1505045-0.1505045

382.7-0.2198530.296639382.70.1483195-0.1483195

382.6-0.2292320.314808382.60.157404-0.157404

382.5-0.2280650.345457382.50.1727285-0.1727285

382.4-0.2247920.365836382.40.182918-0.182918

382.3-0.2204690.371001382.30.1855005-0.1855005

382.2-0.2305390.370317382.20.1851585-0.1851585

382.1-0.2245540.373628382.10.186814-0.186814

382-0.2167210.3699433820.1849715-0.1849715

381.9-0.1991160.352919381.90.1764595-0.1764595

381.8-0.2146350.322835381.80.1614175-0.1614175

381.7-0.2362650.303563381.70.1517815-0.1517815

381.6-0.2334950.302993381.60.1514965-0.1514965

381.5-0.2274010.307743381.50.1538715-0.1538715

381.4-0.2027920.323418381.40.161709-0.161709

381.3-0.1783120.332231381.30.1661155-0.1661155

381.2-0.1762530.336313381.20.1681565-0.1681565

381.1-0.1624510.339624381.10.169812-0.169812

381-0.1709420.3346093810.1673045-0.1673045

380.9-0.193560.325822380.90.162911-0.162911

380.8-0.2213270.310985380.80.1554925-0.1554925

380.7-0.2330690.310289380.70.1551445-0.1551445

380.6-0.2491610.320666380.60.160333-0.160333

380.5-0.2746930.32172380.50.16086-0.16086

380.4-0.303120.316217380.40.1581085-0.1581085

380.3-0.3237440.308463380.30.1542315-0.1542315

380.2-0.3229130.324287380.20.1621435-0.1621435

380.1-0.3173980.324926380.10.162463-0.162463

380-0.3003510.3289723800.164486-0.164486

379.9-0.2931810.327613379.90.1638065-0.1638065

379.8-0.286440.336499379.80.1682495-0.1682495

379.7-0.2810150.347156379.70.173578-0.173578

379.6-0.2952070.344517379.60.1722585-0.1722585

379.5-0.3005490.350115379.50.1750575-0.1750575

379.4-0.3140780.339333379.40.1696665-0.1696665

379.3-0.3184620.317424379.30.158712-0.158712

379.2-0.3210840.307546379.20.153773-0.153773

379.1-0.3342370.30062379.10.15031-0.15031

379-0.337910.2960213790.1480105-0.1480105

378.9-0.3308050.29606378.90.14803-0.14803

378.8-0.334730.291875378.80.1459375-0.1459375

378.7-0.3477780.293861378.70.1469305-0.1469305

378.6-0.3541560.298094378.60.149047-0.149047

378.5-0.3710670.288025378.50.1440125-0.1440125

378.4-0.3700190.285969378.40.1429845-0.1429845

378.3-0.3818220.278002378.30.139001-0.139001

378.2-0.3845030.279771378.20.1398855-0.1398855

378.1-0.4165690.2642378.10.1321-0.1321

378-0.4533010.2474213780.1237105-0.1237105

377.9-0.4696950.245064377.90.122532-0.122532

377.8-0.4742120.237224377.80.118612-0.118612

377.7-0.4786480.223904377.70.111952-0.111952

377.6-0.4855020.221916377.60.110958-0.110958

377.5-0.4835140.230423377.50.1152115-0.1152115

377.4-0.4815320.245454377.40.122727-0.122727

377.3-0.46340.246265377.30.1231325-0.1231325

377.2-0.4474770.24428377.20.12214-0.12214

377.1-0.4444490.237621377.10.1188105-0.1188105

377-0.4507120.2345543770.117277-0.117277

376.9-0.4652530.224638376.90.112319-0.112319

376.8-0.4843410.203681376.80.1018405-0.1018405

376.7-0.5071440.196352376.70.098176-0.098176

376.6-0.5279660.195168376.60.097584-0.097584

376.5-0.5341840.188563376.50.0942815-0.0942815

376.4-0.5387730.178666376.40.089333-0.089333

376.3-0.5460.172784376.30.086392-0.086392

376.2-0.5570620.171924376.20.085962-0.085962

376.1-0.538130.187951376.10.0939755-0.0939755

376-0.5239280.212093760.106045-0.106045

375.9-0.5184220.215328375.90.107664-0.107664

375.8-0.515240.20519375.80.102595-0.102595

375.7-0.5175390.198943375.70.0994715-0.0994715

375.6-0.5118810.199247375.60.0996235-0.0996235

375.5-0.5041920.197019375.50.0985095-0.0985095

375.4-0.4998430.187693375.40.0938465-0.0938465

375.3-0.4949520.190511375.30.0952555-0.0952555

375.2-0.4738910.19761375.20.098805-0.098805

375.1-0.4721820.207449375.10.1037245-0.1037245

375-0.4549260.2307183750.115359-0.115359

374.9-0.45390.238959374.90.1194795-0.1194795

374.8-0.4536430.232023374.80.1160115-0.1160115

374.7-0.4487270.23106374.70.11553-0.11553

374.6-0.4351370.234325374.60.1171625-0.1171625

374.5-0.4328670.23765374.50.118825-0.118825

374.4-0.4396850.245786374.40.122893-0.122893

374.3-0.44350.245117374.30.1225585-0.1225585

374.2-0.4351240.23429374.20.117145-0.117145

374.1-0.4296320.226619374.10.1133095-0.1133095

374-0.4351560.2239333740.1119665-0.1119665

373.9-0.456960.205924373.90.102962-0.102962

373.8-0.4735710.188408373.80.094204-0.094204

373.7-0.4658630.18247373.70.091235-0.091235

373.6-0.4560680.175044373.60.087522-0.087522

373.5-0.4597340.171983373.50.0859915-0.0859915

373.4-0.4605620.173242373.40.086621-0.086621

373.3-0.447740.162971373.30.0814855-0.0814855

373.2-0.4402420.152735373.20.0763675-0.0763675

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3