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    Characterization of Electromagnetic Radiation Absorber

    Materials

    Erik Farias da Silva, Jernimo Silva Rocha, Paulo Ribeiro Lins Junior, Shayenne Diniz da Nbregaand Marcelo Sampaio de Alencar

    Department of Electrical Engineering - Federal University of Campina Grande, CampinaGrande/PB-58.109-970 - Tel/Fax: + 55 83 3101410 - Brazil

    E-mails: [email protected], [email protected], [email protected],

    [email protected], [email protected]

    Abstract This paper describes the comparison ofabsorbing characteristics of ferrite, graphite andcarbon black, in the frequency band of 1.5 GHz to the3 GHz. The substance is mixed in distinct proportionswith synthetic enamel and applied on plates of EPScovered with aluminum paper (NRL Arch technique)and without covering (Insertion Between Antennastechnique). The experimental results show that thegraphite presents the largest attenuation for theelectromagnetic radiation in the in the frequency bandanalyzed.

    Index Terms Absorbing media. Anechoic chamber.Material characteristic. Ferrimagnetic materials.

    I. INTRODUCTION

    Electronic equipments produce electromagnetic energy.

    That energy can provoke degradation or at least

    disturbance in the operation of nearby equipment. With

    the advancement of the technology, the electronic devices

    started to operate at higher frequencies, which cause more

    electromagnetic interference (EMI) [1]. Research

    environments, as well as anechoic chambers, for example,

    are utilized for studies regarding the effects of EMI in

    devices and equipments [2].

    The material utilized as internal covering of thoseenvironments, called Radiation Absorber Materials

    (RAM), presents absorbing characteristics that ought to be

    studied for several frequencies. In this work, three types

    of RAM were studied, in an attempt to observe and

    compare their absorbing characteristics in the frequency

    band of 1.5 GHz to 3 GHz.

    The substances utilized in the study were ferrite,

    graphite and carbon black. They were mixed with

    synthetic enamel in distinct proportions and applied on a

    plate of Expanded Polystyrene (EPS) covered with

    aluminum paper and without covering. Two techniques

    were utilized to analyze the absorption characteristics of

    the material: the technique of NRL arch and the technique

    of insertion between antennas.

    II. ABSORBERMATERIALS

    The Radiation Absorber Materials can be divided into

    dielectric and magnetic absorbers. The dielectric absorber

    presents electrical losses associated to the material

    permittivity. Among the dielectric absorbers one can cite:

    graphite, carbon fibers, conductivity polymers and metal

    particles. The magnetic absorber depends on magneticpermeability and hysteresis characteristics. The magnetic

    absorber more used is the ferrite with several formulations

    and granulations [5].

    In this paper, one uses barium ferrite, graphite and

    carbon black as absorbing material. The ferrite is divided

    into three allotropic varieties: alpha-ferrite (austenite),

    with cubic structure centered in the faces (CCF), it

    remains steady up to 910C. Above 910C the alpha-

    ferrite transforms to gamma-ferrite, with CCF structure.

    Above 1401C, the gamma-ferrite transform to delta-

    ferrite with cubic structure of centered body (CCB). The

    delta-ferrite is formed in the hypoeutectoid region of Fe-C

    phase diagram. Due to CCB crystalline structure of thedelta-ferrite, the crystallographic planes sliding is

    possibility minimal. The delta-ferrite regularly used as an

    electromagnetic absorber [6].

    The graphite is an allotropic form of the diamond. Its

    only constituent is the Carbon. However, its atomic

    structure presents more layers of Carbon atoms,

    hexagonally packed. That contributes to its lamellar

    character and low hardness. This characteristic added to

    high thermal and electric conductivity makes the graphite

    refractory.

    0-7803-9342-2/05/$20.00 2005 IEEE 326

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    The carbon black (CB) is a polymeric additive used as

    radiation absorber and electrical conductor. The CB

    increases the electric conductivity and radiationabsorption. The CB concentration should be low (1%

    generally) in order to not increase the composite viscosity

    and electric conductivity [7].

    III. MEASURING TECHNIQUES

    The characterization of RAM is based on the

    determination of transmission or reflection characteristics.

    There are several characterization techniques with

    reference to reflectivity from RAM. The most commonly

    used are named Radar Cross Section (RCS) and NRL

    Arch (Naval Research Laboratory) [4] both use an

    incident signal in a target and a receiving antenna tomeasure the reflected signal. The target consists of a metal

    plate with one face covered with the RAM.

    For the RCS measurements, the metal plate is fixed in a

    revolving support localized in front of the

    transmitting/receiving antenna inside an ideal open-area

    test site (OATS an outdoor area provided with a ground

    screen and free from obstacles and interfering ambient

    fields [3]) or anechoic chamber. The support can rotate

    360 and the uncovered surface is the reference for the

    measurements.

    For the NRL Arch technique, the metal plate is fixed in

    a static support in a distance in accordance with far field

    condition. The antennas are localized in a reference arch

    (manufactured in wood, commonly) used for alignment of

    the two antennas, using the same angle for emission and

    reception. The reflectivity is determined with reference to

    uncovered metal plate and is expressed in decibels (dB).

    There are several characterization techniques based in

    transmitting features. The waveguide technique is

    regularly used. This consists in disposing a sample of

    RAM inside the waveguide for signal attenuation

    measurements. The transmission coefficient is expressed

    in (dB).

    Another technique used is the Insertion between

    Antennas [8]. In this technique, a plate covered with the

    RAM is positioned between the transmitting and

    receiving antennas. The plate should be transparent to the

    electromagnetic waves in the used bandwidth. In this

    paper, one uses the Insertion between Antennas and NRL

    arch techniques.

    IV. DESCRIPTION OF THE EXPERIMENT

    Two types of experiment were performed, the NRL

    Arch Method and the Insertion Between Antennas

    Method. For both experiments, the measurements were

    made using a network analyzer (Agilent 8753ET). The

    frequency band ranged from 1.5 to 3GHz. The antennas

    were a horn antenna, as transmitter, and a hornet antenna(with aperture of 60) as receiver.

    A. NRL Arch Method

    For each material tested, the reflective base used was

    an EPS plate measuring 40cm on side and with 8mm of

    thickness, one of the plate faces was covered by a thin

    aluminum paper which has been glued to the plate. The

    absorber materials were mixed with a synthetic enamel

    and this mix impregnated to the plate. Twenty plates were

    made, and four materials, each one with five

    concentrations, were tested. Table 1 shows the absorber

    materials percentage in the mix.

    The network analyzer was calibrated using a reflexiveplate attached to the support; this plate was made of

    aluminum paper (without the RAM). The antennas were

    placed in order to maximize the received signal. That

    signal was considered the reference for all the

    measurements. This calibration significantly reduced the

    effects of the ambient reflections.

    A support was made of electromagnetic transparent

    materials and was placed in front of the antennas. The

    antennas stood on a wooden table. The antennas were

    placed at the distance of 1.22m from each other.

    B. Insertion Between Antennas Method

    In this test an EPS plate was used, measuring 40cm on

    each side and with 15mm of thickness. The absorber

    materials were mixed with a synthetic enamel and this mix

    impregnated the plate. Four plates were made, and four

    materials, each one with one concentration, and tested.

    Table 2 shows the RAM percentage in the mix. In this

    test the two antennas were placed in front of the each

    other, and the plate under test was placed between the

    antennas. For all the plates, tests of reflection were made

    and the results show that the reflection phenomena do not

    occur.

    For the calibration of the instrument, an unpainted plate

    was placed between the antennas at a distance of 12cm of

    the receiving antenna (where all the plates were placed

    one by one) and at 1m of the transmitting antenna. The

    signal measured was used as reference for the calibration

    of the analyzer.

    V. RESULTS ANALYSIS

    The NRL arch test was inconclusive in the

    determination of the EMR attenuation, because peaks and

    valleys (in adjacent frequencies) were observed.

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    TABLE I

    NRL ARCH METHOD MATERIALSConcentration (%)

    Material I II III IV V

    Enamel/Ferrite 90/10 85/15 80/20 70/30 50/50

    Enamel /CB/Ferrite 89/1/10 84/1/15 79/1/20 69/1/30 49/1/50

    Enamel/Ferrite/Graphite 80/10/5 80/15/5 72/20/8 60/30/10 50/35/15

    Enamel/Graphite 95/5 90/10 85/15 80/20 70/30

    TABLE IIINSERTION BETWEEN ANTENNAS METHOD MATERIALS

    Concentration (%)

    Material I II III

    Enamel/Ferrite 85/15 70/30 50/50Enamel/CB/Ferrite 84/1/15 69/1/30 49/1/50

    Enamel/Ferrite/Graphite 80/15/5 60/30/10 50/35/15

    Enamel/Graphite 90/10 70/30 50/50

    Therefore, only the data related to the insertion between

    antennas have been analyzed.

    Table III presents the results obtained using the

    insertion between antennas method. It shows the average

    attenuation (in dB) for two bands of frequency, the chosen

    central frequencies were 1.8 and 2.4 GHz, and the

    frequency span was 300MHz.

    It is possible to observe from the results that the best

    absorber material under test was the Enamel/Graphite for

    a percentage of 70/30, the results are shown in Fig. 1. The

    largest absorption was -5.74 dB in the frequency of 1.77

    GHz. Fig. 1 also indicates the best average absorption in

    the analyzed frequency bandwidth (as shown in Table III).

    Another large attenuation result was obtained from the

    measurements with the Enamel/Graphite substrate for a

    percentage of 50/50. This result indicates that there is no

    direct relationship between the amount of material and the

    increase in the absorption results. The third considerable

    absorption was found for the Enamel/Ferrite/Graphite

    substrate for a percentage of 50/35/15.

    VI. CONCLUSIONS

    It was observed, from the data obtained with the method

    of the insertion between antennas that the mixtures based

    on Enamel and Graphite present larger attenuation for the

    electromagnetic radiation in the band of 1.5 to 3 GHz.

    The best results were obtained for the Enamel/Graphite II

    (70/30), for which the average attenuation was -3.7dB. For

    further work, it is interesting to vary the width of the

    absorber substrate and observe the corresponding

    absorption.

    Fig. 1. Enamel-Graphite (at the percentage of 70-30) attenuationversus frequency.

    REFERENCES

    J. L. Wallace, Broadband magnetic microwave absorbers:fundamentals limitations, IEEE Trans.

    [1]Magnetics, vol.29,

    [2]

    Compatibility, vol. 39, no. 1, pp. 33-47,

    [3]

    Compatibility, vol. 38, no. 1, pp.

    no. 6, pp. 4209-4214, November 1993.C. L. Holloway, R. R. Delyser, R. F. German, P. Mckenna,and M. Kanda, Comparison of electromagnetic absorberused in anechoic and semi-anechoic chambers for emissionsand immunity testing of digital devices, IEEE Trans.

    ElectromagneticFebruary 1997.C. L. Holloway, and E. F. Kuester, Modeling semi-anechoic electromagnetic measurement chambers, IEEETrans. Electromagnetic79-84, February 1996.

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    [4]Miacci, Medidas de refletividade de materiaisabsorvedores de radiao eletromagntica usando astcnicas RCS e NRL, Revista de Fsica Aplicada a

    Instrumentao, vol. 16, no. 1, pp. 30-36, March 2003.

    [5] J. C. Dias, F. S. Silva, M. C. Rezende, and I. M. Martin,Absorvedores de radiao eletromagntica aplicados nosetor aeronutico, Revista de Cincia e Tecnologia, Ed.Unimep, vol. 8, no. 15, pp. 33-42, June 2000.

    [6] F. H. Norton,Refractories, New York: McGraw-Hill, 1949.[7] M. F. Rabelo,Aditivao de polmeros, So Paulo: ETDA,

    1998.[8] E. L. Nohara, Materiais absorvedores de radiao

    eletromagntica (8-12 GHz) obtidos pela combinao decompsitos avanados dieltricos e revestimentosmagnticos, Ph.D Thesis, ITA, So Jos dos Campos, 2003.

    M. C. Rezende, E. V. Nohara, I. M. Martin, and M. A. S.

    TABLE

    INSERTION BETWEEN ANTENNAS

    III

    METHOD MATERIALSrage Attenuation (dB)Ave

    Mater II IIIial I

    Hz 1.80.3 GHz 2.40.3 GHz 1.80.3 GHz 2.40.3 GHz1.80.3 GHz 2.40.3 G

    E 278 0.0220 -0.0432 0.0456namel/Ferrite -0.0224 0.0215 -0.0

    E 505 0.0339 -0.0712 0.0332namel/CB/Ferrite -0.0337 0.0395 -0.0

    E 88 -0.1505 -2.6529 -1.9810namel/Ferrite/Graphite -0.0251 0.0115 -0.32

    Enam 98 -4.1139 -3.1995 -2.3207el/Graphite -0.0429 0.0085 -4.79

    329