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Wiederaufarbeitungsanlage Karlsruhe Rückbau- und Entsorgungs- GmbH Sampling Sampling for for radionuclide radionuclide analysis analysis and and radiological radiological characterisation characterisation for for clearance clearance , , storage storage transport transport and and disposal disposal Michael Vilgis Michael Vilgis Safety Safety Department Department 08.07.2009 08.07.2009

Day 3-2 Vilgis Sampling for radionuclide analysis and ... · Sampling for radionuclide analysis and radiological characterisation for clearance, storage transport and disposal Michael

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Page 1: Day 3-2 Vilgis Sampling for radionuclide analysis and ... · Sampling for radionuclide analysis and radiological characterisation for clearance, storage transport and disposal Michael

Wiederaufarbeitungsanlage Karlsruhe Rückbau- und Entsorgungs- GmbH

SamplingSampling forfor radionuclideradionuclide analysisanalysis and and radiologicalradiological characterisationcharacterisation forfor clearanceclearance, ,

storagestorage transporttransport and and disposaldisposal

Michael VilgisMichael VilgisSafetySafety DepartmentDepartment

08.07.200908.07.2009

Page 2: Day 3-2 Vilgis Sampling for radionuclide analysis and ... · Sampling for radionuclide analysis and radiological characterisation for clearance, storage transport and disposal Michael

M. Vilgis 08.07.2009 2

Steps

• Collect Informations• Radiation Protection for workers• objective (transport, disposal, clearance)• Strategy/Plan for Sampling

• Number, Documentation• contamination level

• Choice of sampling method with respect to analysis methods

Page 3: Day 3-2 Vilgis Sampling for radionuclide analysis and ... · Sampling for radionuclide analysis and radiological characterisation for clearance, storage transport and disposal Michael

M. Vilgis 08.07.2009 3

Historyformer usage

History of incidents, failures

actual radiologicalsituation

decision forfurther steps

schedule for clearance/decommissioning

Page 4: Day 3-2 Vilgis Sampling for radionuclide analysis and ... · Sampling for radionuclide analysis and radiological characterisation for clearance, storage transport and disposal Michael

M. Vilgis 08.07.2009 4

Informations from History

• Dispersal pathway for contamination– water systems– waste air system– dust

• Borders of rooms, systems• Range of radiation (in particular neutrons)• Check of Log Books• Nuclide spectrum expected

Page 5: Day 3-2 Vilgis Sampling for radionuclide analysis and ... · Sampling for radionuclide analysis and radiological characterisation for clearance, storage transport and disposal Michael

M. Vilgis 08.07.2009 5

Radiation Protection

• Implementation of Radiation protection areas• Measurements for the survey of actual radiological situation• measures against dispersal and incorporation• protective measures for workers

Page 6: Day 3-2 Vilgis Sampling for radionuclide analysis and ... · Sampling for radionuclide analysis and radiological characterisation for clearance, storage transport and disposal Michael

M. Vilgis 08.07.2009 6

Measurements

easy, quick, simple

complex, particularized

quick informationoverview

detailed information

Page 7: Day 3-2 Vilgis Sampling for radionuclide analysis and ... · Sampling for radionuclide analysis and radiological characterisation for clearance, storage transport and disposal Michael

M. Vilgis 08.07.2009 7

Aspects for Sampling

• Distribution of Contamination– Activation / surface contamination / intruded contamination– homogenous / heterogenous

• Intention of Sampling: Nuclide vector or specific activity• Required decision: Disposal or Clearance possible• Decontamination useful?• Volume, amount of batch• Number of different materials (concrete, metal, etc.)• Time schedule for dismantling / clearance• Single sample, mixed samples• Minimum activity for analysis method

Page 8: Day 3-2 Vilgis Sampling for radionuclide analysis and ... · Sampling for radionuclide analysis and radiological characterisation for clearance, storage transport and disposal Michael

M. Vilgis 08.07.2009 8

Sampling in practice

marking and numbering sampling under RP conditions

Page 9: Day 3-2 Vilgis Sampling for radionuclide analysis and ... · Sampling for radionuclide analysis and radiological characterisation for clearance, storage transport and disposal Michael

M. Vilgis 08.07.2009 9

Sampling methods

• Surfaces– Wipe tests (if contamination is non-firmly adhering) – Scratch off (e.g. cover painting)– abrasion

• Solid Materials– Drilling (chips, dust, drill cores for depth distribution)– Cutting– (small) parts

• Attention:– sampling method with respect to nuclides to be identified (e.g. H-3)– samples preparation with respect to radiochemical analysis ormeasurements

Page 10: Day 3-2 Vilgis Sampling for radionuclide analysis and ... · Sampling for radionuclide analysis and radiological characterisation for clearance, storage transport and disposal Michael

M. Vilgis 08.07.2009 10

Number of samples

Page 11: Day 3-2 Vilgis Sampling for radionuclide analysis and ... · Sampling for radionuclide analysis and radiological characterisation for clearance, storage transport and disposal Michael

M. Vilgis 08.07.2009 11

Representative Samples!

• for the complete batch of material• for a box, drum, container

Page 12: Day 3-2 Vilgis Sampling for radionuclide analysis and ... · Sampling for radionuclide analysis and radiological characterisation for clearance, storage transport and disposal Michael

M. Vilgis 08.07.2009 12

Conclusion

• Knowledge of history• Actual radiological situation• Distribution of activity• Objective of sampling• Representative samples

Page 13: Day 3-2 Vilgis Sampling for radionuclide analysis and ... · Sampling for radionuclide analysis and radiological characterisation for clearance, storage transport and disposal Michael

M. Vilgis 08.07.2009 13

Thank youThank youfor your attentionfor your attention